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The two—step sulfomethy lation and the reaction with HOCH〓SO〓Na in sulfite cooking were illustrated in this paper. The optimum technological conditions were determined on the basis of suitable amount of HCHO in sulfite pulping. The differences of delignification and paper properties of wheat straw were also studied in SFP—AQ and alkaline sulfite and AQ cooking .

对麦草粉的两步法磺甲基化反应以及与羟甲基磺酸钠的反应进行了研究,解释了甲醛在亚硫酸盐蒸煮中脱木素作用机理,从理论上确定了甲醛在SFP—AQ蒸煮中的适宜用量,并据此提出了合理的蒸煮工艺和最佳工艺条件。

It showed that lyotropic liquid crystal phases had emerged in aqueous solution of sulfonated indanthrene at certain concentration and their textures appeared strip or band shapes.

采用氯磺酸磺化对蓝蒽酮进行改性处理,其水溶液在一定浓度下出现了溶致液晶相,织构呈带状和条状分布。

The result of the experiment showed that the qualitative medium - speed filter paper can be used as the material of the nitrite - detecting paper: color developing reagent A containing 4 - aminobenzene sulfonamide and N - 1 naphthyl ethylenediamine hydrochloride, and mixtures of 1 : 1 naphthylamine solution and sulfanilic acid solution as color developing reagent.

实验结果表明:定性中速滤纸可以作为亚硝酸根试纸的材料;含有4-氨基苯磺酰胺和N-1-萘基乙二胺盐酸盐的显色剂A及含有1:1的α-萘胺溶液和对氨基苯磺酸溶液的显色剂B,按1:1混合后可以作为显色剂;通过应用实验表明,亚硝酸根试纸具有体积小、便于携带、检测方便、成本低廉等特点。

In the sulfonation process,sulfonate groups were introduced on the phenyl groups of PS.

在磺化过程中,磺酸基被引入到聚苯乙烯的苯基上。

Taking toluene, chlorosulfonic acid and phosphoryl chloride as raw materials, p-toluenesulfonyl was synthesized.

以甲苯、氯磺酸、三氯氧磷为原料,氯化铵为催化剂合成对甲苯磺酰氯。

L-Amino-2-bromo-4-hydroxy- anthraquinone could be obtained by coordinated hydroxylation of l-amino-2- bromo- anthraquinone, boric acid and the initiator potassium iodide or bromide with 97.5%yield and 99% purity.

在用HPLC跟踪溴氨酸的合成过程研究中发现,1-氨基蒽醌-2,4二磺酸在溴化过程中可转化为产物溴氨酸。

A new method for synthesizing rosin allyl alcohol ester was studied. p-Toluenesulfonic acid allyl alcohol ester was first synthesized by O-acylation of allyl alcohol with p-toluene sulfonyl chloride, using NaOH as catalyst. Then rosin allyl alcohol ester was synthesized from sodium resinate and p-toluenesulfonic acid allyl alcohol ester.

探索了一种两步合成松香烯丙醇酯的新方法,即先以烯丙醇和时甲苯磺酰氯为原料,以NaOH为催化剂,通过O-酰化反应合成中间体对甲笨磺酸烯丙醇酯,再与松香钠皂发生亲核取代反应合成目标产物松香烯丙醇酯。

It is based on the facts that in the presence of sulfuric acid and sodium dodecyl benzene sulfonate, vanadium activated by vitamin C can catalyze potassium bromate to oxidize safranine O, the oxidation products of safranine O can emit intense and stable fluorescence on nitrocellulose membrane.

基于在硫酸介质和十二烷基苯磺酸钠存在下,抗坏血酸活化钒催化溴酸钾氧化番红花红O发射强而稳定的荧光的特性,建立了ⅤC活化溴酸钾氧化番红花红O催化荧光法测定痕量钒的新方法。

The charomatographic conditions of separation and direct dermination of benzophenone-4(MS40), salizyle acid sodium, salol, benzophenone-3(M40), octyl dimethyl PABA(6007), butyl methoxy dibenzoyl methane(1789), octyl methoxyl cinnamate and octyl salicylate(587) from u-Bondapak C18 Column were studied with methanol-water-THF as elution. A HPLC method for these compounds was founded.

研究了用甲醇-四氢呋喃-水作为流动相,从C18柱上分离和测定羟苯甲酮-5-磺酸(MS40)、水杨酸钠、水杨酸苯酯、羟苯甲酮(M40)、对-二甲酸氨基苯甲酸-2-乙基己酯(6007)、4-叔丁基-4-甲氧基二苯甲酸甲烷(1789)、对-甲氧基肉桂酸-2-乙基己酯、水氧酸-2-乙基己酯(587)等8种紫外线吸收剂的色谱条件,建立了用HPLC测定上述物质的方法。

By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料,经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸;并进一步改进和优化了合成工艺条件:即在催化剂三氯化铝过量50%并有三乙胺存在的条件下,中间体2-(4-十二烷基苯甲酰基)苯甲酸收率为72.45%;关环反应采用氯仿作溶剂,利用类似分水器的装置有效控制反应温度以减少碳化,2-十二烷基蒽醌的收率为68.1%。

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They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性,但我大喊,并在他们的方向扔石头让他们过的线索,远离我,以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。

Store this product in a sealed, lightproof, dry and cool place.

密封,遮光,置阴凉干燥处。