磺酸

In the third part of this paper, a facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

对肼基苯磺酸是由对氨基苯磺酸经亚硝酸钠重氮化得到的重氮盐用亚硫酸氢钠还原、水解、硫酸酸化制得，本文经多次实验确定了反应原料、用量及反应条件，得到的产品纯度好，产率高。

Based on reviewing of functionalization of saturated carbon by catalytic oxidation with metalloporphyrins and metal phthalocyanines as a mimic of the enzyme cytochrome P-450, two reaction systems of which one was the preparation of 4, 4'-dinitrostilbene-2, 2'-disulfonic acid from 4-nitrotoluene2-sulfonic acid and the other was the preparation of 4, 4'-bis (dimethylamino -diphenyl) phenylmethanol from 4, 4'-bis (dimethylamino-diphenyl) phenyl methane , were specifically studied as carfunctionalization and oxyfunctionalization of saturated carbon.

本文在全面综述金属卟啉和金属酞菁类模拟细胞色素P-450酶催化剂催化氧化饱和碳原子功能化的基础上，选择由4-硝基甲苯-2-磺酸制取4，4'-二硝基二苯乙烯-2，2'-二磺酸和由4，4'-二苯基甲烷制取4，4'-二苯基甲醇两个反应体系进行饱和碳原子碳功能化和氧功能化的具体研究。

The surface action mechanism of sodium polydithio dipropyl sulfonate in acidic Cu plating bath indicates that the surface complex produced by adsorbed sodium polydithio dipropyl sulfonate and Cu + resists copper ions' electrodeposition.

酸性镀铜溶液中表面活性剂聚二硫二丙烷磺酸钠的表面作用机理表现为：吸附态的聚二硫二丙烷磺酸钠与Cu＋形成表面络合物阻化铜离子的电沉积。

The results showed that 1,5-naphthalene disulfonic acid could be degradated effectively by the catalytic supercritical wa...

结果表明，催化超临界水氧化技术能有效地降解1，5-萘二磺酸，COD去除率可达98%以上；随着反应温度的升高，停留时间的延长，COD去除率也提高；1，5-萘二磺酸在超临界水中催化氧化降解反应的级数对COD和氧气分别为0.89和0.28，活化能为56.8 kJ/mol。

Based on the study of the adsorption mechnism between the macroporous weak base anion-exchange resins and the aromatic sulfonic acid, a pretreatment method for the wastewater from 4, 4'-diaminostilibene-2, 2'-disulfonic acid manufacturing process, a refractory dye intermediate wastewater, was developed.

在对芳香磺酸化合物吸附机理研究的基础上，开发了大孔弱碱性阴离子交换树脂吸附法处理4，4'-二氨基二苯乙烯-2，2'-二磺酸氧化工序生产废水的新技术，并得到了工业化应用。

Methods: According to the degree of color change, the ozone in the ambient air causes the indigo disulfonic acid sodium discoloration response a new colorless production.

空气中的臭氧使吸收液中蓝色的靛蓝二磺酸钠褪色，生成无色靛红二磺酸钠，根据颜色减弱程度比色定量。

A modified analysis method based on the determination of ozone—indigo disulphonate spectrophotometer(GB/T 15437-1995) in gas phase has been developed to detect the concentration of ozone in liquid phase. An analytical condition of λmax=612～615 nm,ε=20 000 L/, pH 2 is obtained by the titration of indigo disulphonate. Compared with potassium iodide method,it shows a higher precision and accuracy,CV＜3.0%. The results also prove that blank experiment will bring about 5.0%systematic error.

在气相臭氧浓度的靛蓝二磺酸钠分光光度法(GB/T15437-1995)基础上提出了液相臭氧浓度的测定方法，采用靛蓝二磺酸钠标准曲线法代替采用易分解的臭氧标准曲线法，得出测定条件λmax=612～615 nm、ε=20 000 L/、pH为2，通过碘量法比较实验，说明新的测定方法具有较高的精度和准确度，相对标准偏差小于3.0%；比较结果表明忽略空白实验将引入5.0%的系统误差。

The preparation method comprises the steps as follows: houghite ZnAl-NO3-LDHs is taken as the precursor, ion exchange method is adopted to insert the 2- naphthylamine-1, 5-disulfonic acid to the interlayer of ZnAl-NO3-LDHs, thereby assembling and acquiring the ZnAl-NADA-LDHs of good crystalling phase structure and splendid performance.

超分子结构2-萘胺-1，5-二磺酸插层材料，简写为ZnAl-NADA-LDHs，其分子式为：[Zn 2 1-x Al 3 x 2 ](C 10 H 7 NO 6 S 2 ) 2- x/2 mH 2 O，是以水滑石ZnAl-NO 3 -LDHs为前体，采用离子交换法将2-萘胺-1，5-二磺酸插入到ZnAl-NO 3 -LDHs层间，组装得到晶相结构良好、性能优异的ZnAl-NADA-LDHs。

Methods sixty patients scheduled for the operation on hypogastric zone were divided randomly into two groups.

60例选择性下腹部手术患者，随机分为两组：甲磺酸罗哌卡因复合芬太尼组(研究组，n=32)和甲磺酸罗哌卡因组(对照组，n=28)。

Firstly, polyacrylamide with 26 million molecular weight was compounded in lab through establishing optimum compounding initiator proportionality of 1:1. 3 and mass concentration of 170 mgL^(-1), temperature of 10 ℃, acrylamide mass percentage of 25%, electrical conductivity of 3.6 μSm^(-1) and pH value of 6.57. The salt-resistance, thermal endurance and shear-resistance of polyacrylamide could be enhanced b introducing sulfonic acid group or styrene sulfonate group or drawing the two groups above at the same time. Secondly, chelator HEDP, bactericide isoquinoline ketone and oxygen scavenger thiourea were optimized to improve the compatibility of polyacrylamide and formation water.

在由室内试验确定了复合引发剂最佳比值1：1.3和质量浓度170 mgL^(-1)、合成最佳温度10℃、丙烯酰胺单体质量分数25%、电导率3.6μSm^(-1)和pH值6.57后，合成出相对分子质量高于2.6×10^7的聚丙烯酰胺，同时通过丙烯酰胺单体复配引入磺酸基团、苯乙烯磺酸基团或同时引入此两种基团，提高了聚合物的抗盐、抗温、抗剪切性能；后针对聚丙烯酰胺与地层水配伍性差的问题，优选出HEDP螯合剂、异噻唑烷酮杀菌剂和除氧剂硫脲，对聚合物稳定效果明显。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。