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MethodsBy high perfomance liquid chromatography method, mobile phase was acetamide plus water solution of sodium heptansulfonic acid and sodium phosphate.

方法采用高效液相色谱法,用乙腈与庚烷磺酸钠磷酸钠的水溶液为流动相,流速 1 。0ml/min ,柱温 4 0℃,检测波长为 2 80nm ,进样量为 2 0 μl。

Methods Enamel surface specimens were randomly allocated into 3 groups: 1 450 mg/L sodium fluoride dentifrice group, 1 450 mg/L sodium monofluorophosphate dentifrice group and non-fluoride dentifrice control group. Sound enamel surfaces were dematerialized in bacteria model in vitro. QLF was used to analyze the area of lesionsArea, the loss of fluorescenceΔF and ΔQArea×ΔF on enamel surfaces after demineralization.

将30个牙釉质块开窗后分为3组,分别使用氟含量1 450 mg/L的氟化钠牙膏、单氟磷酸钠牙膏和无氟牙膏的处理液处理,并在体外恒化器龋病模型中进行脱矿循环,定量光导荧光技术QLF分析病损脱矿后的面积、荧光损失和总荧光损失量,激光扫描共聚焦显微镜CLSM分析脱矿后矿物质含量变化。

Methods Enamel surface specimens were randomly allocated into 3 groups: 1 450 mg/L sodium fluoride dentifrice group, 1 450 mg/L sodium monofluorophosphate dentifrice group and non-fluoride dentifrice control group. Sound enamel surfaces were dematerialized in bacteria model in vitro. QLF was used to analyze the area of lesions, the loss of fluorescence and ΔQ on enamel surfaces after demineralization.

将30个牙釉质块开窗后分为3组,分别使用氟含量1 450 mg/L的氟化钠牙膏、单氟磷酸钠牙膏和无氟牙膏的处理液处理,并在体外恒化器龋病模型中进行脱矿循环,定量光导荧光技术分析病损脱矿后的面积、荧光损失和总荧光损失量,激光扫描共聚焦显微镜分析脱矿后矿物质含量变化。

Enamel surface ecime were randomly allocated into 3 grou : 1 450 mg/L sodium fluoride dentifrice group, 1 450 mg/L sodium monofluoropho hate dentifrice group and non-fluoride dentifrice control group. Sound enamel surfaces were dematerialized in bacteria model in vitro. QLF was used to analyze the area of lesio, the lo of fluorescence and ΔQ on enamel surfaces after demineralization.

将30个牙釉质块开窗后分为3组,分别使用氟含量1 450 mg/L的氟化钠牙膏、单氟磷酸钠牙膏和无氟牙膏的处理液处理,并在体外恒化器龋病模型中进行脱矿循环,定量光导荧光技术分析病损脱矿后的面积、荧光损失和总荧光损失量,激光扫描共聚焦显微镜分析脱矿后矿物质含量变化。

The questing for long service electroless Nickel technology leads to the preferable formula and operation conditions as follows: Nickel Sulphate 25g/L, Sodium Hypophosphate 30g/L, Lactic Acid 20~ 25ml/L, Citric Acid 5g/L, Sodium Acetate 15g/L, Thiourea l~3mg/L, Stabilizer E Img/L.

研究得出的最佳长寿命镀镍工艺为;硫酸镍25g/L,次亚磷酸钠30g/L,乳酸20ml/L,柠檬酸5g/L,乙酸钠15g/L,硫脲1~3mg/L,稳定剂E1mg/L镀液pH值5.0~5.1,施镀温度90±2℃,装载量1dm~2/L;每60min测量镀液中消耗的有效成分和补加浓缩液。

The questing for acidic middle-temperature electroless Nickel technology leads to the preferable prescription as follows:Proportion of Nickel Sulphate and Sodium Hypophosphate 0.36; Sodium Acetate 15g/L; Stabilizer A lmg/L(Stabilizer B Img/L for continual experiment); Composite complexing agent Lactic Acid 10ml/L and acetic acid 10 ml/L; Accelerator organic acid G 6g/L; pH value 5.0; Loading Capacity ldm2/L; Temperature 70C (Temperature 75C for continual experiment); Proportion of supplement for Nickel Sulphate and Sodium Hypophosphate 1:1.2; Testing the consumed ion of Nickel solution and supplement inspissations solution every 60min by the proportion of 15% fresh solution.

最后,通过研究得出最佳工艺配方为:硫酸镍与次亚磷酸钠的摩尔比为0.36;乙酸钠15g/L:稳定剂Almg/L(周期实验加稳定剂B10mg/L);复合络合剂组合为乳酸10ml/L+冰乙酸10ml/L:促进剂为有机酸G6g/L;pH值为5.0;装载量为1.0dm~2/L;施镀温度为70℃(周期实验为75℃):主盐与还原剂的添加比例1:1.2;每60分钟对镀后液进行镍离子浓度的测定并按镍离子的消耗量添加浓缩液,添加比例按开缸液的15%。

6 Buffer comprised 6 mmol/L sodium phosphate, 10 mmol/L sodium borate, 25 mmol/L sodium dodecyl sulphate is used as runing solution, and UV detection wavelength is at 227 nm to determining disperse blue 2BLN in dyeing wastewater.

6mmol/L磷酸钠、10mmol/L硼砂、25mmol/L十二烷基磺酸钠组成的pH9 6的缓冲溶液作电泳液,UV检测波长227nm,测定了印染废水中分散蓝2BLN 的含量。

The dispersion mechanism of the dispersants was analyzed by testing the Zeta potential of the dispersion phase in the dispersion medium. It was shown that Ⅰ and Ⅱ raised obviously the absolute values of surface Zeta potential of titania particles, and NK-1 formed good solvate layers of the particles so that the nano-titania particles were stably dispersed in the water solns.

通过测定分散相在分散递质中的Zeta电位,分析了分散剂的分散机理,说明六偏磷酸钠和硅酸钠可显著提高整理液中二氧化钛颗粒表面Zeta电位的绝对值,NK-1在纳米二氧化钛颗粒表面形成良好的溶剂化层,使纳米二氧化钛颗粒在水溶液中获得优良的分散稳定性。

Fluoride with sodium fluoride, potassium fluoride, stannous fluoride and sodium monofluorophosphate.

氟化物有氟化钠,氟化钾,氟化亚锡及单氟磷酸钠

The proper synthetic technology are as follows: molar ratio of P-aminobenzene sulfonic acid/phenol/formaldehyde is 1∶2∶9, concentration of P-aminobenzene sulfonic acid is 0.4mol·L~-1 , pH of reaction system is 8.0, reaction temperature is 95℃ and reaction time is 3.5h. aminobenzene sulfonate ; dispersant ; ceramic grind additives

国外在磨矿行业已大量使用高效减水剂助磨并取得了显著效果,国内关于这方面的研究起步较晚,主要采用如碳酸钠、硅酸钠、磷酸钠等无机盐,而且也主要是用于有色金属选矿方面,在硅酸盐工业原料加工中有部分采

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