磷化

Benzyl acetate was synthesized from acetic acid and benzyl alcohol as raw materials with phosphotungstic acid as catalyst.

介绍了以冰乙酸和苯甲醇为原料，采用磷钨酸作催化剂合成乙酸苄酯的方法，考察了反应物醇酸摩尔比、催化剂用量、带水剂用量、反应时间、带水剂品种、催化剂重复使用对酯化率的影响。

A traditional acidification method incorporated with an ether extraction technique was used to prepare silicotungstic acid and phosphotungstic acid with Keggin structure.

采用盐酸酸化-乙醚萃取法制备了Keggin型硅钨酸、磷钨酸，并分别以活性炭和硅胶为载体，采用不同的制备方法制备出一系列负载型杂多酸。

Meanwhile, the hardening process of phosphorous slag cement was also determined by trimethylsilylation method and mercury porosimeter.

利用X射线衍射、扫描电镜及差热分析等测试手段，对少熟料磷渣水泥的水化产物进行了分析，并结合三甲基硅烷化法和压汞仪对该种水泥的水化硬化过程进行了研究

The method of the invention not only realizes the quantitative reduction, the stabilization and the resource utilization of the remained sludge and the urban putrescible organic waste, reduces the pollution of the remained sludge and the urban putrescible organic waste to environment, but also produces the organic acid which is beneficial for saprobe and the microbe which removes phosphor and nitrogen.

本发明不仅实现了剩余污泥和城市易腐有机废物的减量化、稳定化和资源化，减少了二者对环境的污染，同时产生了对污水生物除磷脱氮微生物有利的有机酸。

With sodium acetate as catalyst, inosine was esterified with acetic anhydride in the yield of 92% to give 2',3',5'-triacetyl inosine, which was treated with pyridine and phosphorus oxychloride to form a pyridinium solution, followed by performing an amination at 40℃ and 0.25~0.30 MPa to achieve adenosine in the yield of 67%.

肌苷在醋酸钠存在下与醋酸酐发生酯化反应以92%的收率得到2'，3'，5'-三乙酰肌苷，其化合物经吡啶和三氯氧磷处理形成吡啶盐溶液，未分离直接在40℃、0.25~0.30 MPa压力下进行氨解反应以67%产率制得腺苷。

Scenedesmus sp. isolated from sewage was entrapped in calcium alginate gel for tertiary treatment of the artificial wastewater.

利用固定化藻类的生物富积作用净化污水中的氮和磷，将栅藻包埋固定在褐藻酸钙凝胶胶球中，对人工污水进行深度净化。

In Eucalyptus forestland, soil organic carbon, total nitrogen, available potassium contents and soil PH decreased significantly; soil available phosphorus and exchangeable magnesium contents, net nitrogen mineralization rate and ammonification rate also decreased but showed no significant difference. In shrubland, soil exchangeable calcium content increased significantly, but the contents of other nutrients had no significant change.

结果表明：火烧3年后，桉林土壤有机碳、全氮、速效钾和pH含量明显降低，土壤有效磷、交换性镁、土壤净氮矿化速率和氨化速率降低，但不显著；火烧灌草坡除土壤交换性钙明显增加外，其他土壤养分均无显著变化。

The stereochemical effect of the chiral amino acid residues on the formation of penta-coordinate phosphorus intermolecular mixed carboxylic-phosphoric anhydride from N-phosphorylamino acids was studied with density functional theory calculations at B3LYP/6-311G level.

用密度泛函方法在B3LYP/6-311G水平上对N-磷酰化氨基酸生成五配位磷酸羧酸混酐反应中手性氨基酸残基侧链的立体化学效应进行了研究。

The results from the study on characters of phosphorus section distribution show that there are obviously ascending of phosphorus content in the surficial sediments and pore water.

以密云水库为例，研究了水库沈积物中有机质的含量与有机磷的关系，表明表层沈积物中的总有机碳和有机磷的含量都明显高於底层，是由於一些以磷为营养素的富营养化指示藻类在水体中逐年增加，它们死亡后的残骸经分解－矿化后在底积物中累积的结果。

Keywords triethyl phosphate;esterification reaction;phosphate oxychloride;synthesis

磷酸三乙酯；酯化反应；三氯氧磷；合成

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。