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O-(1-Arylseleno-3-azido)isopropyl-O-2-(N3-tegafur)alkyl thiophosphate (3a~3f) were obtained via nu-cleophilic ring-opening of sodium azide to 2a~2f in dry DMF at room temperature, and their antitumor activities were tested.

以无水N,N-二甲基甲酰胺作溶剂,室温下,叠氮化钠中对2a~2f进行亲核开环,得到O-(1-芳硒基-3-叠氮基)异丙基-O-2-(N3-替加氟)乙基硫代磷酯。

The best application method is that 60% of silicon is used as based fertilizers, 40% of silicon as topdressing used in the eighth leaf.

现在硅肥已被国际土壤界列为继氮、磷、钾之后的第四大元素肥料,为全球农业及化肥业所重视[2]。

Adenosine was used as the raw material, dissolved in triethyl phosphate and then esterified with thiophosphoryl chloride under 0~5℃ for 8h without water and oxgen, in alkaline condition provided by 2,6-dimethylpyridine, introducing thiophosphoryl ester to adenosine.Then superfluous triethylamine was added and reacted under 5℃ for 1h to synthesize rough 5'-AMPS.The unpurified product was appled to a DEAE Sephadex A-25 column and eluted with triethylammonium bicarbonate.

用腺苷为起始原料,溶解于磷酸三乙脂中后,在无水无氧环境中及2,6-二甲基吡啶提供的碱性条件下与三氯硫磷以0~5℃下发生酯化反应8h,将硫代磷酸酯引入腺苷,然后再与过量三乙胺在5℃下反应1h,合成粗产品,再用碳酸氢三乙胺作洗脱液,过DEAE Sephadex A-25凝胶柱纯化。

Genistein promotes osteoid mineralization,reduces the loss of Ca, P and Mg in the bone and prevent the generation of osteoporosis in unsexed rats

染料木黄酮促进去势大鼠类骨质矿化,减少骨中钙、磷、镁丢失,预防骨质疏松的发生。

Study shows that,pH smallest coefficient of variation was 12.95%,coefficient of variation of soil available phosphorus was the largest,varia...

研究表明,pH的变异系数最小为12.95%,土壤有效磷的变异系数最大,变异值达到了122.18%;经克里金插值分析,研究区土壤养分的空间相关性减弱,朝均一化发展,这说明了红花套镇土地养分变化受人为因素影响较大,当地的土壤适合并已形成大面积的发展种养殖业,传统的稻、麦、棉种植数量和产量都与红花套镇的人平纯收负相关,对当地人平纯收贡献最大的是柑桔总产,相关系数分别为0.822,0.966,土地利用效率最大的是水产品养殖,相关系数分别为-0.760,0.870。

In this paper, the acetalization of benzylaldehyde and 1,3-propanediol in the presence of vanadium phosphorus oxide catalyst was studied.

研究了苯甲醛与1,3-丙二醇在钒磷氧催化剂作用下的缩醛化反应,考察了反应时间、醇醛比、催化剂用量、带水剂种类和用量等因素对苯甲醛1,3-丙二醇缩醛收率的影响。

KH12 could make its rhizosphere acider than XIN9005 so as to uptake more phosphorus.

KH12 的对根际土壤的酸化能力强于忻9005,增加了根系对磷素的吸收。

In this thesis, investigations focused on heteropoly acids-catalyzed C-C and C-N bond formation reactions and the synthesis of xanthenediones and acridinediones under thermal conditions are described.1.12-Phosphotungstic acid has been used as an efficient,eco-friendly,and air- and moisture-stable catalyst to promote the direct dehydrative substitution of the hydroxy group of benzylic and allylic alcohols with variousβ-dicarbonyl compounds.

本篇论文主要描述了杂多酸催化下的C-C和C-N键的生成,以及无溶剂直接加热下合成十氢氧杂蒽二酮和9-芳基十氢吖啶二酮。主要内容如下:1。在磷钨酸催化下,1,3-二羰基化合物与醇能够顺利偶合,脱除一分子的水,生成烷基化的1,3-二羰基化合物。反应在甲苯中进行时,二芳基甲醇能与各类1,3-二羰基化合物反应,成率很高;但对于1-苯乙醇,只能得到很低的产率。

A salt of bromic acid.To achieve such a miracle, the semiconductor industry has gone to extremes, using the world's most toxic substances like Arsine, Phosphine, Hydrofluoride, Hydrobromide and the like.Soon, even Synchroton will be used.

但是,为了这种&奇迹&,半导体技术也到了无所不用其极的地步,世上最剧毒的物质如砷烷(ah3)、磷烷(ph3)、氟化氢、溴化氢,等一长串毒品全都用上,很快连同步加速器也要用上去了。

The isopropyl chloracetate was synthesized by esterification of chloracetic acid with isopropyl alcohol using aluminium phosphotungstate as catalyst.

以氯乙酸和异丙醇为原料,磷钨酸铝作催化剂进行酯化反应,合成氯乙酸异丙酯。

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But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊!不用提了。提到肉,真是糟透了。

Tristan, I have nowhere to send this letter and no reason to believe you wish to receive it.

Tristan ,我不知道把这信寄到哪里,也不知道你是否想收到它。