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When diethyl carbonate was used as transesterification reagent,the convertion of phenol and the yield of DPC had improved,but the extant was small.

碳酸二乙酯为酯交换试剂,苯酚的转化率和DPC的产率都有所提高,但提高的幅度不大。

When all the sodium has dissolved, a mixture of 164 parts of ethyl phenylacetateand 118 parts of diethyl carbonate is added during 5 minutes and the mixture is maintained at the boil for a further hour.

当所有的纳都溶解后,然后在五分钟内添加164份乙基乙酸苯酯和118份二乙基碳酸酯的混合物,混合物再另外维持一个小时的沸腾状态。

This invention provides a polymerizer and polymerization equipment for producing an aromatic polycarbonate by melt transesterification from a molten prepolymer, of the aromatic polycarbonate, produced from an aromatic dihydroxy compound and a diaryl carbonate.

本发明提供了一种用于通过熔融酯交换由芳族聚碳酸酯的熔融预聚物生产芳族聚碳酸酯的聚合器和聚合设备,其中芳族聚碳酸酯的熔融预聚物由芳族二羟基化合物和碳酸二芳基酯生产。

Ytterbium metal, ytterbium diiodide, samarium diiodide promoted organic reaction and their applications in organic synthesis;;bis carbonate in organic synthesis

中文题名金属镱,二碘化镱和二碘化钐促进的有机反应在有机合成中的应用;双碳酸酯在有机合成中的应用

Much attention has been paid to the synthesis and application of dimethyl carbonate because o...

作为一种低毒性和有多种反应活性的化学试剂,碳酸二甲酯(DimethylCarbonate简称DMC)的合成与应用近年来受到了广泛的重视。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料,先将二酚与碳酸钾成盐,甲苯带水回流反应,然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体;再以二硝基单体,铁粉,HCl为原料,乙醇和水做溶剂,回流反应、乙醇重结晶,得到含氟芳香二胺基单体。

The recent advances in the main clean processes to synthesize diphenylmethane diisocyanates are reviewed, such as BTC method, condensation of aniline, reductive carbonylation of nitrobenzene, oxidative carbonylation of aniline, methoxycarbonylation of aniline, alcoholysis of N,N'-diphenyl urea and the coupling process.

回顾了清洁合成二苯甲烷二异氰酸酯的几种主要方法,如BTC法、苯胺缩和法、硝基苯还原羰基化法、苯胺氧化羰基化法、碳酸酯法、二苯基脲法和反应耦合法等合成路线。

Results:Biochemical indicators: the concentrations of K+, Na+ and Cl- in the serum after the infusion are different with those before the infusion; other indicators don't have the significant difference. The mean infusion time of group A is longer than that of group B (p=0.006), while the dosis letalis of KCl doesn't have significant difference between groups (p=0.062); the concentrations of K+ in blood, Na+, Mg2+ and Cl- in serum have the significant difference between groups; the urine volume and the concentrations of all the urine electrolyte indicators don't have the statistical significant difference between groups.

结果:生化指标:输入钾前后,家兔血清钾离子浓度升高,钠、钙及氯离子浓度降低,具有统计学显著性差异,p=0.000;全血钾及血清其他离子浓度变化,以p=0.05为标准,不具有统计学显著性差异。A、B两组间比较结果:A组输液致死时间长于B组(p=0.006),致死输钾量无统计学显著性差异(p=0.062);全血钾、血清钠、镁及氯离子浓度变化值具有显著差异,血清钾、钙、碳酸氢根离子浓度变化值无明显的差异;尿量和尿液各电解质浓度指标无统计学显著性差异。

Application to the Eopalaeozoic buried hill in the Z oilfield shows that the two types of azimuthal attributes, attenuation gradient and frequency at 85% energy ratio, are closely related to fracture characteristics of carbonate reservoir.

对Z区下古生界潜山碳酸岩储层进行的裂缝预测表明,由衰减梯度和85%能量比频率两种属性导出的裂缝发育密度具有很好的相关性,且与实际情况符合。

The invention relates to a mixed additive used in lithium secondary battery electrolyte, which is characterized in that: its components comprises that biphenyl at 0.5-95.4%, phenylcyclohexyl at 1.1-93.8%, vinylene carbonate at 0.4-93.2%, tertiary carbon alkyl benzene at 0.5-96.5%; and ethenyl sulfonyl benzene at

本发明公开了一种锂离子二次电池电解液用混合添加剂,其特征在于:组分与重量%分别是:联苯类0.5%~95.4%;环己基苯类1.1%~93.8%;碳酸亚乙烯酯0.4%~93.2%;叔碳烷基苯0.5%~96.5%;乙烯基硫酰苯0.5%~95.8%。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

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