碳化的

The direct incorporation of U-13C glucose was estimated by the intensity increase of m/z to F(F was parent fragment, and n was the carbon number in the fragment), while the total isotope incorporation from the added 13C could be calculated according to the abundance ratio increment summation from m/z (Fa+1) through (Fa was the fragment containing all original skeleton carbons, and T was the carbon number in the amino acid molecule). The 13C enrichment in the target compound was expressed as atom percentage excess, and that of D-amino acid needed to be corrected by the coefficient of hydrolysis-induced racemization. The 13C enrichment reflected the carbon turnover velocity of individual amino acid enantiomers, and was powerful to investigate the dynamics of soil amino acids.

外加葡萄糖直接合成氨基酸的比例可利用质谱碎片的相对强度变化来评价（n为质谱碎片F中含有的碳原子数目）；而源于葡萄糖的13C同位素在氨基酸分子中的富集程度是所有同位素峰相对强度变化的总和。13C在目标化合物中的富集比例用原子百分超评价，D氨－基酸的APE还需进一步利用水解诱导的外消旋化系数校正。13C在目标化合物中的富集程度可反映各氨基酸手性异构体的碳循环速率大小，是研究土壤氨基酸动态变化的有力工具。

In summary, the alkylation performances of isobutane with butene over bothheteropoly acid and zeolite catalysts have been investigated in this thesis, and theresults are helpful for further development of the solid acid catalysts for this process.

通过本论文的研究，对杂多酸和分子筛催化剂的烷基化性能有了进一步认识，能对今后开发固体酸的碳四烷基化催化剂有所帮助和借鉴。

At this stage, the solid pyrolyzed products of polysiloxane and polycarbosilane were amorphous silicon oxycarbide and nonstoichiometric silicon carbide containing excess carbon, respectively At higher temperature, structure of the amorphous pyrolyzed products started to rearrange and experienced a disorder →order transformation, even crystallized Cristobalite crystallized from SiO〓C〓, and β-SiC also crystallized from SiO〓C〓 provided carbon content of the starting polysiloxane was high enough, while β-SiC crystallized from SiC〓.

当热解温度达1000℃时，聚合物先驱体的无机化过程已基本完成，其陶瓷转化率值趋于稳定，此时聚硅氧烷的热解产物为非晶态的氧碳化硅，聚碳硅烷的热解产物则为含过量碳的非化学计量比的非晶态碳化硅；随着热解温度的升高，非晶态热解产物的结构逐步调整，发生无序→有序的相变，以至析晶。

This paper studied the synthesis and models about the etherification reaction from isoamylene to the tert-amyl methyl ether synthesis.

分析了异戊烯醚化生成甲基叔戊基醚的反应机理及相关的反应动力学模型，以甲醇和乙烯裂解碳五为原料进行醚化反应，分别求得R-E模型、L-H模型的动力学参数。

In an identical plant, the graphitization and carbonization of both fiber surface and inside are carried out simultaneously.

本发明具有在一套设备内同时实现石墨化和纤维表面及内部的渗碳，工艺简单，得到高强度和高模量的石墨化碳纤维的优点。

Three immobilization modes of antigen to the polymers in the pH-sensitive phase separation immunoassay were investigated and compared. The results showed that the immobilization mode in the presence of N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride rendered the most desirable results. The immobilization efficiencies and immunological reaction activities of immobilized antigen of this mode were improved over the other two modes.

本文研究并比较了pH敏感相分离免疫分析中抗原在高分子上的三种固定化模式，结果显示由碳二亚胺偶联的固定模式效果最好，固定化效率、固定抗原的免疫反应活性较之另外两种模式均得到了提高。

The formation mechanism of titanium nitride powders by reduction of carbon and nitridation was researched by method of continuous weighing.

用连续称重法研究了钛白粉被活性碳还原氮化合成氮化钛粉末的还原氮化反应机理，并进行了反应的热力学、反应产物的显微结构以及X-ray衍射分析。

Results show that microbial biomass carbon and microbial biomass nitrogen in fertilized soil peak in the first several days, and then decline. Incubating both sweet maize straw and white clover have the highest yield, maxima of 529.57 mgkg^(-1) and 75.50 mgkg^(-1) respectively. They also release respired CO2 the most among all treated soils. The best mineral nitrogen release is in white clover incubating, with a maximum of 29.81 mgkg^(-1) under a 26-day culture, and then keeping 1.60 times the control and reaching 2.48 times at 80-day culture. Sweet maize incubating has the least mineral nitrogen release. It is 13%~53% of the control under a 26-day culture, with a maximum of 7.51 mg kg^(-1). Soil nitrogen mineralization is insignificant under sweet maize incubating with urea in short-term.

研究发现，各施肥处理的土壤微生物量碳、微生物量氮均在培养前期出现峰值，后期平稳降低；甜玉米桔秆和白三叶草绿肥同时还田的土壤微生物量碳、微生物量氮在各培养时期均最大，峰值分别达529.57 mgkg^(-1)，和75.50 mgkg^(-1)，土壤呼吸产生的CO2最多；白三叶草绿肥单独还田有利于土壤无机氮的释放，培养第26d无机氮达到最大值，为29.81 mgkg^(-1)，之后一直在对照处理的1.60倍以上，第80d达到2.48倍；甜玉米秸秆单独还田不利于土壤无机氮的释放，培养的第26d至结束，甜玉米秸秆处理的无机氮为对照的13%~53%，最大为751 mgkg^(-1)；甜玉米秸秆配施尿素，短期内不利于土壤无机氮矿化。

Results show that microbial biomass carbon and microbial biomass nitrogen in fertilized soil peak in the first several days, and then decline. Intercropping Incubating both sweet maize straw and white clover have the highest yield, maxima of 529.57 mg·kg-1 and 75.50 mg·kg-1 respectively. They also release the most respired CO2 the most among all treated soils. The best mineral nitrogen release is in white clover intercroppingincubating, with a maximum of 29.81 mg·kg-1 under a 26-day culture, and then keeping 1.60 times the control and reaching 2.48 times at 80-day culture. Sweet maize incubatingintercropping has the least mineral nitrogen release. It is 13%~53% of the control under a 26-day culture, with a maximum of 7.51 mg·kg-1. Soil nitrogen mineralizatiomineralization is insignificant under sweet maize incubatingintercropping with urea in short-term.

研究发现，各施肥处理的土壤微生物量碳、微生物量氮均在培养前期出现峰值，后期平稳降低；甜玉米秸秆和白三叶草绿肥同时还田的土壤微生物量碳、微生物量氮在各培养时期均最大，峰值分别达529.57 mg·kg-1和75.50 mg·kg-1，土壤呼吸产生的CO2最多；白三叶草绿肥单独还田有利于土壤无机氮的释放，培养第26 d 无机氮达到最大值，为29.81 mg·kg-1，之后一直在对照处理的1.60倍以上，第80 d达到2.48倍；甜玉米秸秆单独还田不利于土壤无机氮的释放，培养的第26 d至结束，甜玉米秸秆处理的无机氮为对照的13%～53%，最大为7.51 mg·kg-1；甜玉米秸秆配施尿素，短期内不利于土壤无机氮矿化。

The results show that a surface layer of stable cobalt borides of CoB, CoW2 B2 and CoW3B3 formed at 950 ℃ can effectively reduce tKey words: diamond films; cemented carbide; boronizing pretreatment; adhesion

结果表明，基体经硼化预处理后表面形成CoB、CoW2B2、CoW3B3相；当沉积温度为750～800℃，碳源浓度为3.3%时，薄膜表面形貌和生长织构随着沉积气压改变有明显的变化；硼化预处理后所得样品在1500N载荷下压痕表现出良好的附着性能，较二步法预处理更加有效地改善了膜-基附着性能。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。