碳化的

The fixed carbon content in the sample can be calculated from the difference between two weightings.

在600℃灰化滤纸并纯化固定碳90 min，称重，然后在1000℃灼烧至恒重，前后两次重量之差值为固定碳的结果。

Then esterification of 3, 7-dimethyl-2-pentadecanol with acetic anhydride, the active component of sex pheromone of pine sawfly, 3, 7-dimethyl2-pentadecanyl acetate was obtained in 83. 4％ yield.

最后，用乙酸酐对3，7-二甲基-2-十五碳醇进行酯化，得到松叶蜂性信息素的活性组分--3，7-二甲基-2-十五碳醇乙酸酯，收率为83.4％。

After active carbon powder and alloy steel powder are added to the thermit, the self-propagating high-temperature synthesis reaction starts.

本文研究了合金化自蔓延陶瓷内衬复合钢管制造技术，即在铝热剂中加入活性碳粉或合金钢粉末，进行自蔓延高温合成反应，分析了碳和合金元素对复合钢管过渡层的影响。

By developing the spV tight-binding model, we study the band spectrum feature of the cagelike structure such as carbon clusters, carbon nanotubes, BN nanotubes in this thesis.

本论文发展sp~3s~*紧束缚模型，着重研究笼状纳米结构如碳巴基球、碳纳米管、纳米氮化硼管的能谱特征。

We prepared the ordered porous alumina membrane by a two-step anodization method in oxalic or sulfuric acids, which is a self-ordered hexagonal array of cells with an adjustable pore diameter of 20-150nm and a different pore structures (i.e. Y-branched, dendriform, toothed and torous ones). Furthermore, the template-electrodeposition, vapor-catalytic growth, and controlled chemical etching were developed for well-aligned carbon nanotubes and oxide nanopillars with adjustable diameter, Al2O3-AlN one-dimensional heterojunction, Y-junction and dendriform metal nanowires, as well as Y-junction, and torous carbon nanotubes. The resultant one-dimensional junctions were characterized by XRD, SEM, TEM,HRTEM, and STM, and the field emission of the well-aligned carbon nanotubes and the luminescence of ZnO nanopillar array have also been mearsured.

完善和发展了阳极腐蚀法制备多孔氧化铝膜的方法，制备出了孔径在20-150nm之间可调和具有不同孔结构（如Y形、树枝状、锯齿状）的系列多孔氧化铝模板，在此基础上，利用电化学沉积、气相催化生长和化学控制腐蚀等方法，成功地生长出具有可调直径的碳纳米管和氧化物纳米柱有序阵列、Al2O3-AlN异质结纳米线、Y形和树枝状的金属纳米线以及Y形、藕节形和锯齿形的碳纳米管等多种一维结纳米材料及其阵列体系，探索了基于模板孔壁内沿生长一维结纳米材料的机制，较系统的研究了碳纳米管阵列的场发射性能和氧化锌纳米柱的发光性能，为低维纳米材料器件化提供了实验基础。

Through a series of quenching, tempering, tensile testing, low-temperature impact test and metallographic analysis, we ultimately came to the following conclusions:(1) low-carbon alloyed steel 20CrMn2NiMoV quenching at 870℃ and tempering at 200℃, whose structure contains tempered dislocation lath martensite and few small bainite under mixed, has the best obdurability;(2) Carbon Steel 45CrMn2NiMoV quenching at 850℃ and tempering at 620℃, whose structure is sorbitic, has a performance less than that of low-carbon Alloyed steel, but it can also meet the basic design requirements.(3) Mn can substitute for the role of Ni within limited extent.

通过一系列淬火、回火、拉伸试验、低温冲击试验以及金相分析，最终得出以下主要结论：（1）低碳合金钢20CrMn2NiMoV经870℃淬火+200℃回火，得到回火位错型板条马氏体+少量细小下贝氏体的混合组织，具有最佳的强韧性配合；（2）中碳合金钢45CrMn2NiMoV经850℃淬火+620℃回火，得到回火索氏体组织，综合性能虽然不及低碳合金钢，但也能基本满足设计要求；（3）Mn在一定程度上能够替代Ni的作用，适量的Mn和Ni相互配合可以得到最佳的低温韧性，因此&以Mn代Ni&是低温钢材料研究开发中一条可行的适合我国资源状况的合金化思路。

A process for continuously preparing nm carbon tubes on fluidized bed include such steps as carrying the transition metal oxide catalyst on carrier, putting it in catalyst-activating reactor, reduction reaction by introducing the gas mixture of nitrogen gas and hydrogen or CO gas to the reactor, loading the catalyst into fluidized bed, and introducing mixed reaction gas to its to grow said nm carbon tubes on the catalyst by chemical gas-phase deposition.

本发明涉及一种流化床连续化制备碳纳米管的方法，首先将过渡金属的氧化物催化剂载于担体上，然后将其放在催化剂活化反应器内，通入流动的氢气或一氧化碳与氮气的混合气体进行还原反应，最后将催化剂送至流化床中，通入反应混合气体，流化床的下部则得到碳纳米管。本发明的方法和装置，在流化床中经过化学气相沉积，在催化剂载体上生长出碳纳米管。

Alkylbenzene, normal alkanes and alkylcyclohexane on the pyrolysates of P. Boryanum at 300℃ had uniform distribution and the relative content of them was similar, indicating that they originated from same precursors. Fatty acids, alcohol and ketone in algal cell are the possible precursors. For example, the precursor of relatively abundant C〓 alkylbenzene and alkylbenzene with C〓 side chain perhaps related with palmitic acid. N-alkylnaphthalene in pyrolysates at 300℃ probably derived from alkylation of cleavage products of aromatic steranes and terpanes.

在盘星藻300℃热解产物中，烷基苯、正烷烃和烷基环己烷碳数分布一致、各化合物的相对含量接近，表明它们有相同的来源，藻类体内的脂肪酸、醇和酮及细胞壁等物质可能是其母质，相对含量较高的碳数为16及侧链碳数为16的烷基苯类化合物，其前身物可能与软脂酸有关。300℃热解产物中的正烷基萘类化合物，可能由芳香甾、萜类的降解产物与直链烃类加成烷基化而形成。

The results of FT-IR 1H-NMR indicate the structure of polyester, and the 13C-NMR analysis of three quaternary carbon showed the existing of hyperbranched struscture, MALDI-TOF MS showed the hyperbranched polyester structure, the degree of branching of the polyesters determined by 13C-NMR being 0.408. The esterification reaction kinetics followed a second-order equation and the reaction rate was controled by the concemtration of carboxyl group and hydroxyl group,-d/dt=K.

以IR、1H-NMR证实了聚酯结构的存在，13C-NMR谱图上3种季碳的特征峰有力证实了超支化分子结构的存在，MALDI-TOF MS证明了超支化聚酯的成功合成，并计算超支化聚酯的支化度为0.408；探讨并建立了超支化聚酯的缩聚反应动力学方程－d/dt=K，该缩聚反应属于二级反应，反应速率由羟基浓度和羟基浓度共同决定。

The lipid may divide into the animal fat and the vegetable oil according to its origin, and the saponification value affected by the carbon chain length of fatty acids. The types of lipid determine the properties of saponification products. Besides, it takes different time to accomplish the reactions of saponification by the different lipid.

油脂依其来源可分为动物性油脂与植物性油脂，油脂皂化价受油脂脂肪酸碳链长度影响，因此油脂种类决定皂化产物之特性与质感，不同的油脂达成皂化反应所需时间也各有差异。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新