碱量法

With methanol as solvent and NaOH as catalyst,the influence of the concentration of NaOH ,reaction temperature and reaction time to the alcoholysis of polyvinyl acetate is studied by the homogeneous design procedure.

使用均匀设计法研究了甲醇作为溶剂，氢氧化钠作为催化剂时，聚醋酸乙烯酯醇解反应中碱的物质的量比、反应温度和反应时间对聚乙烯醇醇解度的影响。

The extracting coenzyme Q_(10) from Blakeslea trispora using saponific ation was also studied by orthogonal test. And the optimum extracting conditions were obtained as follows: Wet culture was distilled at 70℃for 60min, added caustic potash up to 1.9 times of dry culture, pyrogallol up to 1/2 dry culture, and the concentration of alkali-methanol was 10%.The average recovery of CoQ_(10) was 81.5%.

采用正交实验，对醇碱皂化法提取三孢布拉氏霉菌体中辅酶Q_(10)的各工艺条件进行了研究，确定最佳的工艺条件为： KOH加量为干菌体质量的1.9倍，醇碱浓度为10%，焦性没食子酸添加量为干菌体质量的1/2，在70℃下皂化60min，其平均提取收率达81.5%。

The performances of leadless and cadmiumless fluxing agents for overglaze colors were studied based on alkali-boron-silicon fluxing agent system.

用正交实验法研究了在碱-硼-硅系统基础熔剂中，外加助熔助色成分MgO、CaO、SrO、BaO四种碱土金属氧化物的添加量及R2O：RO、SrO：CaO、RO：SiO2对无铅无镉釉上彩熔剂性能的影响规律。

In this paper,the effects of pH,concentration of buffer and triethylamine in mobile phase on chromatographic behavior of oxymatrine,sophoridine and matrine were studied by using ion exchange chromatography and their mechanisms were discussed.

采用离子交换色谱法，以氧化苦参碱、槐定碱、苦参碱3种生物碱为对象，研究了流动相pH、缓冲液浓度及三乙胺加入量等色谱条件对生物碱色谱行为的影响，并探讨了其作用机制。

Orthogonality L9(34) methods on the basis of the concentrations of caladium alkali was used to optimize the preparation technology. The final technology was determined as follow:12 times water soaking herbs, volatility oil distilled by vapor 2h, decoction 2 times every 1.5h and 85% alcohol forming granules.

经正交实验四因素三水平L9(34)方法，以西贝碱的含量为检测结果，优选了最佳的提取工艺，确定了用12倍量水浸泡4h，以水蒸汽蒸馏法收集挥发油2h，煎煮1.5h，干膏用85%乙醇制粒的科学工艺。

HepG2 cells were exposured to oxymatrine, final concentrations of which were 0.1, 0.2, 0.3, 0.4, 0.5, 0.8, 1, 2, 5, 8, 10, 15 g.L-1 respectively, MTT method was used to determine the inhibiting effects of oxymatrine on HepG2 cells proliferation, followed by Haematoxylin and Eosin staining to observe the cell morphology.

以0.1，0.2，0.3，0.4，0.5，0.8，1，2，5，8，10，15 g.L-1的氧化苦参碱处理HepG2细胞，四噻唑蓝法检测其对细胞增殖的影响；苏木精-伊红染色比较细胞形态差异；免疫组化染色进一步检测HepG2细胞肿瘤相关蛋白表达量的变化。

According to the Box-Benhnken design principle,the method of response surface method with 3 factors and 3 levels was used. The factors influencing the technological parameters were determined by means of regression analysis. Response surfaces were finally graphed with the yield as the response value. The synthesis conditions were optimized as follows:reaction reagent was NBS,stoichiometric proportion between NBS and anhydrovinblastine was 1.07; the dosage of TFA was 22 mL/L; reaction temperature was －68 ℃ and duration was 90 min.

在单因素实验基础上，根据Box-Benhnken实验设计原理，采用三因素三水平的响应面分析法，研究了各个因素及其交互作用后，得到了合成7′-Br-脱水长春碱的最佳工艺条件：以二氯甲烷为溶剂，采用NBS为溴代剂，其用量与底物的物质的量比为1.07∶1，TFA的加入量22 mL/L，在－68 ℃下反应90 min，终止反应后，得到卤代产物。

The result shows that to improve the anodic current efficiency, we should decrease the reactions in the anodic solution between dissolving chlorine and transferring sodium hydrate and reduce a series of the reactions between the anode and the cathode.

本论文首先阐述了氯碱工业生产技术发展历史，并介绍离子膜法电解产生、发展过程以及其发展方向，考察了影响电流效率的各种因素，并提出提高电流效率的措施，得出要提高阳极电流效率，就要尽量减少在阳极液中产生的溶解氯与迁移烧碱之间发生的副反应，减少阳极上氧的析出量；要提高碱的电流效率，就要尽量减少氢氧根离子向阳极室的反渗。

Chromium ore samples were fused by alkali and then leached out by hydrochloric acid. After the analytical lines of the elements were selected, the conditions of sample uptake, carrier gas flow, cooling gas flow and RF power were optimized with the system of SeaSpray nebulizer and cyclone spray chamber, based on the principle of best signal stability. The determination of chromium, aluminum, iron, magnesium and silicon in chromium ores was fulfilled.

铬矿石样品经碱熔融和盐酸浸取后，选用SeaSpray雾化器和旋流雾室，选定了待测元素的分析线，以信号的稳定性为原则，优化了样品提升量、载气流量、冷却气流量和入射功率，实现了电感耦合等离子体原子发射光谱法对铬矿石中铬、铝、铁、镁和硅等主量成分的测定。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。