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A method for chiral analysis of anatabine,nornicotine and anabasine in tobacco has been established.

建立了烟草中新烟草碱、降烟碱和假木贼碱的手性分析方法。

METHODS:3 levels from each of the amount of four factors-excipient calcium carbonate,tween-80,starch and emollient (magnesium stearate:french chalk) were subjected to the orthogonal design with the parameter of dissolution of the harmine in tablet as an index.

以辅料碳酸钙、吐温-80、淀粉及润滑剂用量为4因素,每因素取3水平,以总碱片中去氢骆驼蓬碱的体外溶出参数为指标进行正交试验。

From the point of view of geobotany, with the method of correlative factors of growth of plants, a countrywide theoretic ecological division was done for the introduction of Camptotheca acuminata and three kinds of areas of ecological preferent zone, ecological adaptive zone and ecological unadaptable zone were divided. With the theory of synecology, the characteristic on environment, constitution, life form spectrum, diversity, similarity of plots of communities were researched. Applying the method of species association, discrete distribution, indensity index, fractal geometry, etc. to research relations between the species of the communities, space distribution of Camptotheca acuminata, structure of age of Camptotheca acuminata, in different communities. Using the theories of autoecology, distibutons of seeds on land and growth of seedlings in vertical and horizontal directions, biomass of organ of Camptotheca acuminata were analyzed. On the opinions of conservation biology, the external and internal factors impressing Camptotheca acuminata were analyzed to research the mechanism of the endangered species, and with using of CTM Model, the future development direction of Camptotheca acuminata in different communities were forecasted, and. Standing on the position of resources ecology, discussing the regularity of camptothein in Camptotheca acuminata of different sites and seeding of different resources, also the the derive technics of camptothecin.

本文从地植物学的角度,运用植物生长相关因子法,对我国喜树资源的生态适宜区进行了划分,理论上确定了我国的喜树的引种栽培的最适生活区域、生态适宜区域和不适宜生活区域;从群落生态学的角度,对野生喜树所在的典型群落的群落环境、群落组成、群落生活型谱、群落的物种多样性特点、群落样地间相似性进行了研究;从种群生态学的角度,运用种间联结性、离散分布模型、聚集强度指数、分析几何等分析手段,对野生喜树所在典型群落间的种间关系、喜树的空间分布格局、年龄结构等进行了分析;从个体生态学的角度,对不同年龄组的喜树的种子的散落的垂直分布、水平分布、时间分布及种子发芽率和千里重等特点、不同种源的人工喜树苗期特点、喜树的高生长和茎生长特点、喜树的器官生物量特点进行了研究;从保护生物学的角度,对野生喜树的濒危的内部因素和外部因素进行了探讨,并运用CTM模型对不同群落中野生喜树的种群趋势进行了预测;从资源生态学的角度,对我国地理环境下喜树中喜树碱含量的地理分布规律、不同种源的喜树幼苗中喜树碱含量变化规律进行了研究,并对喜树碱的提取工艺进行了探讨。

Flushes is cool when should take down the jewelry, meets 碱 a kind of product by against jewelry, after specially contains the chlorine bleaching agent and the silver contact, can have the chlorination to respond, causes the silver personal ornament rapid nigrescence.

冲凉时应取下首饰,以防首饰遇到碱类产品,特别是含氯的漂白剂和银接触后,会起氯化反应,使银饰迅速变黑。

The method was used in analysis of papaverine hydrochloride concentration in rabbit vein blood after injecting papaverine hydrochloride injection.

测定了兔子静脉注射盐酸罂粟碱注射液后不同时间内血液中盐酸罂粟碱的含量,对其药时曲线进行了研究。

OBJECTIVE:To determine pilocarpine nitrate and its degradation products by HPLC,study the stability of pilocarpine nitrate eye-drops.

肖仰目的:建立以高效液相色谱法测定硝酸毛果芸香碱滴眼液中硝酸毛果芸香碱的含量及其降解产物,同时进行了其稳定性考察。

Based on this,a sensitive method has been developed for the quantitative determination of piperine in Mn-piperine-cetyltrimethylammonium bromide ternary system.

据此建立了在锰-胡椒碱-溴化十六烷基三甲基胺三元体系中测定胡椒碱的荧光分析新方法。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethyl malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effective base.

在这类催化反应中,碱的选择具有重要的影响:以K3PO4为碱, Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中,富电子溴代芳烃显示较好的活性; Pd2/L1催化的乙酰乙酸乙酯α-芳基化时,以 K2CO3为碱,催化体系显示较好的活性,这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯,而不是脱乙酰基的产物。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethy malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effectiv base.

在这类催化反应中,碱的选择具有重要的影响:以K3PO4为碱,Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中,富电子溴代芳烃显示较好的活性;Pd2/L1催化的乙酰乙酸乙酯α-芳基化时,以K2CO3为碱,催化体系显示较好的活性,这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯,而不是脱乙酰基的产物。

Employing high-dilute method and 5-fold excess amine prepared two new "two-armed" acyclic diamine intermediates I_a and I_b, which are also intermediates of synthesizing microcyclic compounds, and eight aromatic Schiff bases, II_, were synthesized from reaction of I_a or I_b condensing with different aromatic aldehydes. Their composition and structure were characterized by Elemental analysis, IR, UV-Vis, LIF,~1HNMR and MS. The hydrogen bond interactions and MS fragmental patterns were also discussed.3. Several novel transition metal complexes using II_a as ligand were synthesized and identified by Elemental analysis, IR, UV-Vis,~1HNMR and molar conductivity.

1,采用高度稀释及胺过量五倍的方法合成了两个具有吡啶双酰胺臂的非环二胺Ⅰ_a和Ⅰ_b,并以它们为中间体进一步合成了八个芳香席夫碱Ⅱ_a-Ⅱ_h,通过元素分析及各种波谱测试鉴定了它们的组成与结构,对化合物的UV-Vis、LIF、IR、~1HNMR及MS进行了较为详细的讨论,还探讨了席夫碱的氢键相互作用及质谱裂解方式; 2,以席夫碱Ⅱ_a为配体合成了几个新型的过渡金属配合物,并通过元素分析、UV-Vis、IR、~1HNMR、摩尔电导及DTA—TG对其进行了表征,讨论了化合物的配位情况及配体在配位中的脱质子行为。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。