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By identifying the obtained components by TLC, three alkaloids components were detected, among which one was nuciferine. The other two were N-Nornucirerine and O- Nornucirerine, identified by Nuclear Magnetic Resonance and Mass Spectrum.6、In order to exploit natural bacteriostat of lotus leaves, optimal extraction process and antibacterial characteristics were studied.

两者得到的化合物分别经TLC鉴别,得到3个生物碱成分,其中1个为荷叶碱,其余两个应用核磁共振和质谱等技术鉴定为N-去甲荷叶碱和0-去甲荷叶碱。6、从荷叶天然食品抑菌剂开发的角度,研究了荷叶抑菌有效成分的提取优化工艺及抑菌特性。

Is for the airplane, above the clouds so high sowing and sing, like a big bird in sky B is for a bunny, but it doesn't cut his tail, he goes cipety hup hup hup, a longer bunny trail.

是上述的云雾,使飞机,播种和唱歌,像一个大鸟在天空 B是一个兔子,但它不切断了他的尾巴,他就会cipety石杉碱甲石杉碱甲石杉碱甲,较长的兔子痕迹。

Eight hydrazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, 2-hydroxy-1-naphthaldehyde with nicotinic or isonicotinoyl hydrazide in anhydrous ethanol respectively; Three thiosemicarbazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, o–hydroxyacetophenon with thiosemicarbazide in hydrous-ethanol respectively.

主要包括以下五部分的工作: 1、以水杨醛、邻香草醛、邻羟基萘甲醛、邻羟基苯乙酮分别与烟酰肼和异烟酰肼按1:1的比例在无水乙醇中反应,制备了八种酰腙类Schiff碱;以水杨醛、邻香草醛、邻羟基苯乙酮与氨基硫脲在水-乙醇混合溶剂中反应,合成了三种Schiff碱配体,并对Schiff碱配体的结构进行了表征。

The ethanol extract was dissolved with HCl, the acidic extract was basified to pH9-10 with NH_3-water and extracted with CHCl_3 to give total alkaloids. five alkaloids were isolated with column chromatography and preparative thin-layer chromatography, and three of them were identified as dehydrocorydaline、 corynoline and dihydrosanguinarine on the basis of spectral analysis MS,~1H-NMR,~(13C-NMR and physicochemical properties. All of them were found for the first time from this plant.

为研究灰绿黄堇的化学成分,本文将灰绿黄堇乙醇提取物采取酸提取、碱游离后萃取的方法得到总生物碱,然后利用柱色谱、制备薄层色谱等方法分离、纯化了灰绿黄堇中5种生物碱,并利用IR、MS、~1H-NMR、~(13)C-NMR等方法鉴定了其中的3种,分别为去氢紫堇碱、紫堇灵、二氢血根碱,均为首次在此植物中发现。

The results showed that germinative energy was more sensitive to alkaline stress than germination rate,RL was more sensitive to alkaline stress than SH and RN,early seedling stage was more sensitive to alkaline stress than germination period.

结果表明,水稻发芽势对碱胁迫的反应较发芽率更为敏感;根长对碱胁迫的反应较苗高和根数更为敏感;幼苗前期对碱胁迫的反应较发芽期更为敏感。

Moreover, the water extract and the alkaloids of Rhizoma Coptidis, as well as berberine, palmatine and jatrorrhizine could increase the EFSinduced contraction.

为了验证我们的这种推测,本文研究黄连水提物、黄连总生物碱以及黄连中的主要化学成分小檗碱、巴马丁碱和药根碱对豚鼠胃窦环行肌收缩的影响。

The survival rates of CEM cells cultured with cis-diamminedichicloroplatinum added 24 h later were higher than that cultured with hTERT ASODN and DDP added 24 h later. The survival rates of CEM cells cultured with DDP were similar with that cultured with hTERT SOND and DDP. In morphological observation of apoptotic cells using Giemsa staining, cells treated with DDP or DDP combined with hTERT ASODN ro SODN at 48 h, displayed classic apoptotic changes. Apoptosis rates of CEM cells treated with DDP for 48 h after 24 h of exposure to ASODN significantly increased. There was significant difference in the percentage of apoptotic cells of CEM cells between hTERT ASODN plus DDP and SODN plus DDP or DDP alone, respectively.

结果: hTERT ASODN作用于CEM细胞24 h再加入柔红霉素、长春新碱、足叶乙甙,对细胞生长的抑制分别与单用柔红霉素、长春新碱、足叶乙甙及hTERT正义寡核苷酸联合柔红霉素、长春新碱、足叶乙甙组相比,统计学上无显著差异(P>0.05)。hTERT反义核酸作用于CEM细胞24 h加入顺铂,再共同作用48 h,CEM活细胞均数为2.318×108 cells/L,与单用顺铂组(3.250×108 cells/L)及hTERT正义核酸联用顺铂组(3.175×108 cells/L)相比,对细胞抑制明显增强(P<0.05)。hTERT ASODN作用于CEM细胞24 h再加入顺铂作用48 h,细胞出现典型的凋亡形态学改变。hTERT ASODN与2.5 μmol/L顺铂联合作用于CEM细胞48 h的凋亡细胞百分率(19.47%)分别同SODN与顺铂联合作用组(6.97%)、单用顺铂作用组(6.02%)进行比较有显著差异(P<0.01)。

METHODS:Based on the model of human umbilical vein endothelial cell, this study adopted Rose Bengal Stain, cell ELISA, immunocyto-chemical techniques to investigate the effect of berberine on PMN-endothelium adhesion and the expression of cell adhesion molecules.

以小檗碱加IL-1、TNF处理人PMN或人脐静脉内皮细胞后,用蛋白染料染色法研究小檗碱对PMN与HUVEC粘附的作用,用细胞ELISA、APAAP法研究小檗碱对细胞表面粘附分子表达的影响。

By alkaline fusion of hydroxycaproic acid and its derivatives with sodium hydrate.

用氢氧化钠碱熔处理废碱液中的羟基己酸及其聚合物,可使废碱液中己二酸的质量分数由 3。

By alkaline fusion of hydroxycaproic acid and its derivatives with sodium hydrate.

用氢氧化钠碱熔处理废碱液中的羟基己酸及其聚合物,可使废碱液中己二酸的质量分数由 3.18%提高到8.74 %,且环境效益和经济效益显

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The X-ray diffract was used to analyze the crystal structure of the composite. Results show that after the talc was treated with blend coupling agent, the crystal structure of talc changed, and effect Intercalation phenomenon.

通过X射线衍射分析可知,用混合偶联剂对滑石粉进行预处理后,滑石粉晶体结构发生改变,产生了插层现象,使PP/滑石粉复合材料为纳米复合材料。

An authentic Maui wedding might require the services of a 'kahu', which is a Hawaiian minister.

毛伊可能需要一个真实婚礼服务'kahu',这是夏威夷部长。

Funds involving such cases are limited and there is no huge capital flight.

与此有关的资金数额是相对少数的,并没有引发资本外逃现象。