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A new method for the determination of vauqueline by using the flow injection chemiluminescence method is presented.

报道一种微量测定马钱子碱的新方法，该方法是基于高锰酸钾对马钱子碱的氧化作用，建立了微量马钱子碱的流动注射化学发光分析法。

The molecular structural formula of the rhodamine 6G hydrazide salicylal azomethine is shown on the right, and the present invention discloses the synthesization method of the rhodamine 6G hydrazide salicylal azomethine and rhodamine 6G hydrazide salicylal azomethine solution used for the content determination of a small amount of cupric ions in water sample: 0 percent to 98.99 percent of ethanol, 99.99 percent to 1 percent of acetic acid / sodium acetate buffer solution with the pH value of 5 to 9, in which the total concentration of acetic acid is 1 to 100 millimoles per litre, 0.01 percent of N, N-dimethylformamide and 1ppm to 100ppm of rhodamine 6G hydrazide salicylal azomethine, all measured in mass percentage.

罗丹明6G酰肼水杨醛希弗碱，分子结构式如右，本发明公开了罗丹明6G酰肼水杨醛希弗碱的合成方法及其用于水样中微量铜离子含量测定的溶液：0～98.99％乙醇，99.99～1％pH值5～9的醋酸/醋酸钠缓冲溶液，该缓冲溶液中醋酸总浓度为每升1～100毫摩尔，0.01％N，N-二甲基甲酰胺和1～100ppm罗丹明6G酰肼水杨醛希弗碱，均为质量百分含量。

The method is simple,rapid and suitable for the determination of three alkaloids in total alkaloids exfracted from L. plumule .

本法简单、快捷、适合于测定莲子心中莲心碱、异莲心碱、甲基莲心碱的含量。

The 1:1 mixtures of chaconine and solanine or solamargine and solasonine, produced markedly synergistic effects while the mixtures of unpaired glycoalkaloids from different plants did not have this effects.

卡茄碱与茄碱，澳洲茄边碱与澳洲茄碱的1：1的混合物产生了明显的协同作用，而来自于不同植物的不成对的糖苷生物碱则没有这种协同作用。

The results of the dissertation were concluded as follows:(1) It is essential to deposit a basic additive on the Mo-based catalysts for the synthesis of CH_3SH. The potassium-doped Mo-based catalysts exhibit the highest activity than that of the catalysts doped with the otherⅠA andⅡA group basic promoters. H_2-TPR and LRS characterizations suggest that the addition of a base leads to the transformation of octahedrally coordinated Mo to tetrahedrally coordinated Mo, thus leads to the split of low temperature reduction peaks. The interaction between the basic components and Mo lead to the formation of B-Mo interface phase, which are closely correlated with the formation of CH_3SH.(2) It has been found that Fe, Co, Ni and Te have evident promoting effects for the K-Mo/SiO_2 catalysts.

主要结果归纳如下：(1)在Mo基催化剂中，必须添加碱才具有可观的合成甲硫醇活性，在IA和IIA族元素中，K是最佳的碱促进剂，当K/Mo摩尔比为2，前驱体为K_2CO_3，采用共浸法制备的K-Mo催化剂活性最高。H_2-TPR和LRS表征显示，碱的加入导致表面八面体钼氧物种向四面体转化，催化剂的低温还原峰发生分裂，碱助剂与钼之间存在强相互作用形成了B-Mo"界面相"，该物种与合成甲硫醇密切相关。

The hydrolysates were elucidated as bebziylaconine,aconine and other two unknown compounds.

乌头碱的水解成分为乌头次碱，乌头原碱和另外2种未知产物。

Objective To investigate the adsorption function of macroporous adsorption resins for the separation and purification of the effective components in Plumula Nelumbinis.

目的研究大孔吸附树脂吸附分离莲子心中莲心碱、异莲心碱及甲基莲心碱的工艺条件及参数。

Results AKS-W Resin had a preferable adsorptive and separateive effect for the effective components in Plumula Nelumbinis. The products containing 10.2% liensinine, 6.7% isoliensinine, and 11.9% neferine could be obtained.

结果AKS-W树脂对莲子心中有效成分有较好的吸附分离效果，提取物中莲心碱、异莲心碱及甲基莲心碱的质量分数分别提高到10.2%、6.7%和11.9%。

With the content of the total alkaloids and mesaconitine as parameters, the optimum condition of absorption and elution were studied in the process of the purification with X-5 macroporous resin.

以川乌总碱和新乌头碱的含量为指标，考察X-5型大孔树脂分离纯化乌头总生物碱和新乌头碱的最佳吸附及洗脱条件。

PURPOSE: Establish the methods to detect and measure new aconitine, aconitine and hypoaconitine, which are the mostly toxic components of aconites.

目的 ：建立乌头类主要毒性成分新乌头碱、乌头碱、次乌头碱的检出方法和含量测定方法。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。