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The interference of reductant is eliminated by in direct iodimetry in the weak acidic medium and the content of potassium iodate is determined by direct iodimetry under acidic condition.

在弱酸性介质中,利用间接碘量法消除还原物的干扰,于酸性条件下采用直接碘量法测定碘酸钾含量。

A selective and mild PS-DIB/ionic-liquid immobilized 2, 2, 6, 6-tetramethyl-piperidin-4-ol-N-oxyl catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via the iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TeMPO catalyst, 4-(2, 2, 6, 6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from TeMPO and 1, 4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化,制得了负载型二乙酰氧碘苯作为氧化剂。2, 2, 6, 6-四甲基-N-氧自由基哌啶醇与1, 4-二溴丁烷反应生成4-溴丁氧基-2, 2, 6, 6-四甲基-哌啶-1-氧化物,再与N-甲基咪唑发生季铵化反应,生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2, 2, 6, 6-四甲基-N-氧自由基哌啶负载离子液体。

A selective and mild PS-DIB/ionic-liquid immobilized TEMPO catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via Iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TEMPO catalyst, 4-(2,2,6,6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from 2,2,6,6-tetramethyl-piperidin-4-ol-N-oxyl and 1,4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化,制得了负载型二乙酰氧碘苯(diacetoxyiodo polystyrene,PS-DIB)作为氧化剂。2,2,6,6-四甲基-N-氧自由基哌啶醇(2,2,6,6-tetramethyl-piperidin-4-ol-N-oxyl,TEMPO)与1,4-二溴丁烷反应生成4-溴丁氧基-2,2,6,6-四甲基-哌啶-1-氧化物,再与N-甲基咪唑发生季铵化反应,生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2,2,6,6-四甲基-N-氧自由基哌啶负载离子液体TEMPO-IL。

The radioactive methyl iodide method is one of the important ways to test iodine adsorbers.

引言放射性甲基碘法是碘吸附器的主要试验方法之一。

57 cases neonatal with omphalitis were divided randomly into two teams.29 cases in first team were treated with Dianfu and Yunnan Baiyao.28 cases in second team were treated only with Dianfu.

将2000年至2004年在我院确诊为新生儿脐炎的57例患者随机分成两组,治疗组采用碘伏与云南白药进行治疗;对照组采用碘伏进行治疗。

A spectrophotometric determination of iodine by oxidation decoloration reaction of pyrocatechol violet by iodatein a strong acid medium is reported in this paper.

本文提出了在强酸性条件下,根据碘酸根氧化邻苯二酚紫使其褪色吸光光谱法测定加碘食盐中碘含量的分析方法。

Thyroid neoplasms; Tumor cells, cultured; Sodium iodide symporter; Gene therapy; Iodine radioisotopes

甲状腺肿瘤肿瘤细胞,培养的钠碘转运体基因疗法碘放射性同位素 NIS基因甲状腺细胞腺相关病毒癌细胞系制备

Tsushima et al.(5), noted that the iodinated contrast agents used for computed tomography have pharmacokinetics similar to inulin and hypothesized that it could be used as a physiologic measure of renal indices, including clearance per unit renal volume and fractional vascular volume.

Tsushima等发现CT检查时碘化对比剂的药物代谢动力学与菊粉相似,于是假设碘化对比剂可用于测定肾脏指数包括单位肾容积清除率和血管容积分数。

Tsushima et al.(5), noted that the iodinated contrast agents used for computed tomography hae pharmacokinetics similar to inulin and hypothesized that it could be used as a physiologic measure of renal indices, including clearance per unit renal olume and fractional ascular olume.

Tsushima等发现CT检查时碘化对比剂的药物代谢动力学与菊粉相似,于是假设碘化对比剂可用于测定肾脏指数包括单位肾容积清除率和血管容积分数。

The incidence of anaphylactoid reaction is 1.28%.

低渗透压、非离子型碘造影剂目前已完全替代了以往的高渗透压、离子型碘造影剂,副反应明显减少[1,2]。

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