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Results and Discussion Flavin 2 was synthesized from 3,4-diaminobenzoic acid (3) and alloxane monohydrate (4) in good yield according to standard procedures (Scheme 1).9 The first step afforded flavin 5 in quantitative yield, in 1:1 ratio of the 7- and 8-hydroxycarbonyl regioisomers, and was subsequently methylated by methyl iodide to form flavin 6 in 86% yield, in a 3:2 ratio of the 7- and 8-regioisomers.

结果与讨论黄素二是合成3,4 -二氨基安息香的酸( 3 )和氧嘧啶水合物( 4 )在良好的收益率根据标准程序(计划1) 0.9的第一步,给予黄素五,在定量产量,在1:1的比例, 7 -8 -羟基羰基 regioisomers ,并随后甲基甲基碘形成黄素6月在86 %的产量,在一个3:2的比例, 7 -和8 regioisomers 。

Results Comparing with normal epithelium and dysplasia tissue, DNA content and heteroploid cells increased significantly in esophageal carcinoma.

应用碘化丙啶染色和间接免疫荧光标记方法,采用流式细胞仪对30例食管癌组织及相应的癌旁组织进行定量检测。

In order to compare the properties of 2 stable chlorine dioxide disinfectants using different activators, malonic acid iodometry method and quantitative germicidal test were used for laboratory obser-vation.

为了比较用不同活化剂的两种稳定性二氧化氯消毒剂的性能,用丙二酸碘量法和定量杀菌试验在实验室进行了观察。

The analytical method for sodium methyl mercaptide was established based on the reaction in quantity between methyl mercaptan and iodine at the base condition.

采用甲硫醇与碘在碱性条件下定量反应生成双硫醚的反应原理,建立了甲硫醇钠的定量分析方法。

METHODS: The concentration of ozone that was transmitted by ozone generator at different time was determined by using iodine titrimetric method. According to the bactericidal assay of quantitative vehicle, the bacteria on the ozonized vehicles and unozonized vehicles was washed, 50μl eluant was seeded on the TSA plates. The TSA plates were put into the anaerobiotic incubator (90% N2, 10% CO2, 37℃). After 24 to 48 hours, the CFU on the plate was counted.

用碘滴定法测定打开臭氧发生器不同机组及不同时间时的臭氧浓度,按载体定量杀菌试验,将经臭氧作用的载体与相同环境下未经臭氧作用的载体上的细菌洗下,各取洗脱液50μl,接种于TSA平板并置厌氧箱(90%N2, 10%CO2, 37℃)培养24~48h后,进行活菌菌落计数。

After ethanol extracted hepaticglycogen, it was identified by indic colorific mensuration and quantified with anthrone mensuration. Finally, experimentative design was bringed forward.

采用三氯醋酸沉淀组织蛋白质,乙醇提取肝糖原后,以碘呈色法对其鉴定,再以蒽酮法进行定量,最后提出对相关物质检测的实验设计要求。

The results showed that under 200 W power, in the present of various alkalis, e.g. Na2CO3, NaF, KF, NaHCO3, and DMF-H2O (V∶V=5∶3) used as solvent, PVC-TETA-Pd could catalyze sodium tetraphenylborate to react quantificationally with iodobenzene in 20 min without inert gas protection, and all the phenyl g...

实验发现:在微波功率为200W时,在Na2CO3,NaF,KF,NaHCO3等多种碱的存在下,以DMF的水溶液(V∶V=5∶3)为溶剂,在无惰性气体保护下,PVC-TETA-Pd催化四苯硼钠与碘代苯在20min内即可定量反应,与常规加热方式相比,节省了大量时间;同时也证明了四苯硼钠的四个苯基均可参与Suzuki偶联反应;该催化剂回收再利用3次后,仍具有较高的催化活性。

The expression changes of ICAM-1 and p65 mRNA level were detected by reverse transcription-polymerase chain reaction and the expression of p65 protein in AR42J cell lines were detected with Stept Avidin-Biotin complex respectively, and the changes of amylase in culture medium with chromatometry.

逆转录-多聚酶链反应半定量法观察细胞间黏附分子(ICAM-1)和p65亚单位mRNA表达的变化;链酶亲和素-生物素-过氧化物酶复合物法检测p65蛋白在AR42J细胞中的表达;人工碘比色法观察培养液上清中淀粉酶的活性改变。

Principle— The titrimetric determination of water is based upon the quantitative reaction of water with an anhydrous solution of sulfur dioxide and iodine in the presence of a buffer that reacts with hydrogen ions.

原理---水分滴定测定法是基于水与二氧化硫和碘的无水溶液,在能与氢离子反应的缓冲溶液下发生的定量反应。

According to the bactericidal assay of quantitative vehicle, the bacteria on the ozonized vehicles and unozonized vehicles was washed, 50μl eluant was seeded on the TSA plates.

用碘滴定法测定打开臭氧发生器不同机组及不同时间时的臭氧浓度,按载体定量杀菌试验,将经臭氧作用的载体与相同环境下未经臭氧作用的载体上的细菌洗下,各取洗脱液50μl,接种于TSA平板并置厌氧箱(90%N2,10%CO2,37℃)培养24-48h后,进行活菌菌落计数。

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