碘定量的

To determine the condition of chromogenic reaction between iodine and amylum quantitatively, the author studied the law in the course of chromogenic reaction between iodine and amylum with the aid of spectrophotometer quantitatively, and found that maximum absorption wavelength is 610 nm, and the absorbance in the course of chromogenic reaction between iodine and amylum has not changed within 7 hours.

为了确定碘和淀粉反应的定量关系，本文利用分光光度计定量地研究了碘和淀粉显色反应过程中吸光度的变化规律，发现碘和淀粉显色反应的最大吸收波长为610 nm，碘和淀粉显色反应的吸光度在七小时内基本不变，可以进行比色分析。

In the medium of H2SO4 with KBr as the catalyst, the color of Cresol Red oxidized by iodate can be faded, and the degree of color fading is proportional to the concentration of iodine and the linear range of determination is 20 μg/25 mL~50 μg/25 mL.

在硫酸介质中、在溴化钾催化条件下，碘酸根对甲酚红有褪色作用，且褪色的程度与碘酸根的量有关，碘定量测定的线性范围为20μg/25mL～50μg/25mL，检出限为6。

This is a easy and rapid method for quantitative determination of urinary iodine in field survey.

提出了一个简易、快速，现场定量测定尿碘的方法。

PH of filtrate is kept below 0.65 in order to avoid the reaction between sodium formate and iodine bromide. Then iodine bromide halogenation method is used to determine quantitatively the content of the third monomer, i.

控制滤液pH在0.65以下，以防止甲酸钠和溴化碘起反应，然后用溴化碘卤化法定量测定滤液中的第三单体甲基丙烯磺酸钠的含量。

Result: 1. The method of arc-needle injection with 131I-iodinated oil step-by-step sector-shapely improved obviously the drug distribution, comparing with routine linearity injection. 2. SPECT image reconstruction detect 131I-iodinated oil three-dimensional distribution quantitatively. 131I-iodinated oil metabolism equation may obtained by continuous measurements, in order to calculate absorption dose of p particle at target. 3. ZT glue lengthens obviously 131I-iodinated oil retention in mouse local subcutis and rabbit liver which can rise local radiation effect, decrease injury at normal tissue.

结果：1、弧形针分段扇形注射~(131)I-碘化油，比常规使用的线性注射明显改善药物弥散均匀度。2、SPECT断层扫描定量检测~(131)I-碘化油的三维分布，连续测量建立~(131)I-碘化油的代谢方程，并计算~(131)I对靶区的β辐射贡献的吸收剂量。3、ZT胶明显延长~(131)I-碘化油在大鼠皮下、兔肝脏内的滞留。

I-iodinated oil metabolism equation may obtained by continuous measurements, in order to calculate absorption dose of β particle at target. 3. ZT glue lengthens obviously 〓I-iodinated oil retention in mouse local subcutis and rabbit liver which can rise local radiation effect, decrease injury at normal tissue.

结果：1、弧形针分段扇形注射〓I-碘化油，比常规使用的线性注射明显改善药物弥散均匀度。2、SPECT断层扫描定量检测〓I-碘化油的三维分布，连续测量建立〓I-碘化油的代谢方程，并计算〓I对靶区的β辐射贡献的吸收剂量。3、ZT胶明显延长〓I-碘化油在大鼠皮下、兔肝脏内的滞留。

The results show that in the presence of NaHCO3 as base and DMF-H2O (volume ratio 2∶1) as solvent, the complex could catalyze not only iodobenzene but also non-activated bromobenzene quantitatively at 90 ℃ without the inert gas protection, and furthermore the catalyst could be recovered and reused more than eight times.

结果表明，在没有惰性气体保护的情况下，以NaHCO3作碱，以DMF水溶液(体积比为2∶1)作溶剂，在90 ℃时，该配合物不仅对活性较高的碘代苯能够定量地催化，对未活化的溴代苯也能定量地催化，并且催化剂能够回收再利用8次以上。

Analysis on main points for determination of chlorine dioxide by iodometric method ;2. The experiment results show: To measure sulfide in wastewater by iodometric method may have errors because the interferent can not be removed.

用碘量法测定废水中的硫化物，可能因无法消除干扰而使测定结果存在较大误差；对于同一废水样品，当碘量法和亚甲基蓝分光光度法的测定结果存在显著性差异时，可用Pb2半定量法进行判定；对于某些化纤企业的废水，用氢氧化钾-乙醇溶液洗涤沉淀，可消除碘量法测定的干扰。

Methods: Eleven B-CLL patients were studied. Leukemic lymphocytes with (n=8) or without (n=3) P2z receptors were exposed in vitro to ATP, benzoylbenzoic-ATP, 2-methylthio-ATP(2MeSATP), adenosine-5′-［γ-thio］ triphosphate, and other nucleosides for 8h. Apoptosis was detected by electron microscopy, agarose gel electrophoresis, and quantitative TdT assay. Results:Apoptosis was detected only in leukemic lymphocytes with P2z receptors. By using the quantitative assay, ATP-inducing DNA strand breaks were found to occur specifically for BzATP, ATP and 2MeSATP, but not for ATP-γS and other nucleosides.

将表达P2z受体［P2z］与不含P2z受体［P2z］的两组CLL细胞分别同1.0mmol/L三磷酸腺苷体外培养8小时，以电镜、DNA凝胶电泳和定量DNA 3′端TdT法检测细胞凋亡；并对ATP、苯甲酰苯甲酸ATP、2-甲基硫ATP(2MeSATP)、γ-硫代ATP及其它核苷的诱导效应和氧化型ATP、1-［N，O-二(5-异喹啉碘酰基)N-甲基-L-酪氨酰］-4-苯哌嗪KN-62）的抑制效应做定量研究。

In the medium of H2SO4 with KBr as the catalyst, the color of Cresol Red oxidized by iodate can be faded, and the degree of color fading is proportional to the concentration of iodine and the linear range of determination is 20 μg/25 mL~50 μg/25 mL.

在硫酸介质中、在溴化钾催化条件下，碘酸根对甲酚红有褪色作用，且褪色的程度与碘酸根的量有关，碘定量测定的线性范围为20μg/25mL～50μg/25mL，检出限为6.57×10-1μg/25mL，回收率为98.1%～104.2%。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了