碘化

Chapter three focuses on the application of the Baylis-Hillman adduct in organic synthesis and some new exploration was made.

第一章对钐试剂促进的有机反应和Baylis-Hillman反应在有机合成中的应用作了简要介绍；第二章研究了二碘化钐促进的还原消除反应；第三章研究了Baylis-Hillman加成物参与的立体选择性的转化反应。

A highly explosive mixture of ammonium nitrate and trinitrotoluene.

一种无色或黄色的碘化氢水溶液。

Methods: Mesenchymal stem cells were isolated from human term placenta by digestion of collagenase Ⅱ and their unique growth characteristic of attaching to the wall of cell culture flask. The proliferation ability was detected by living cell number counting and propidium iodide staining. Their surface markers were detected by flow cytometry. The cells were induced to osteoblast with dexamethasone, antiscorbutic acid and β-sodium glycerophosphate. And they also were induced to adipocytes with dexamethasone and insulin. After induction, the cells were observed by Von Kossa staining and oil red O staining.

将人足月胎盘组织经胶原酶Ⅱ消化和贴壁培养法获取间充质干细胞，运用活细胞计数和碘化丙吮检测其增殖能力；采用流式细胞术检测其细胞表面标志的表达；用地塞米松、抗坏血酸及β-磷酸甘油诱导其向成骨细胞分化，并用Von Kossa染色进行鉴定；用地塞米松与胰岛素诱导其向脂肪细胞分化，并以油红O染色进行鉴定。

Starting from 3-benzoyl-5-formyl-indolizine, 3-benzoyl-5-(2'2'-diacetylethenyl)-indolizines and analogs were obtained by the 〓mediated aldol condensation or Wittig reaction. These compounds,promoted by low-valent titanium, gave highly functionlizedcycl[3,2,2]azine derivatives. The coupling reaction proceeded betweenthe carbonyl group and the carbon-carbon double bond, a rare example inMcMurry reaction.

我们以3-苯甲酰基-5-甲酰基中氮茚为原料，通过三碘化钐促进的aldol反应和Wittig反应制备了3-羰基-5-羰基乙烯基中氮茚，随后经低价钛还原偶联，没有生成正常的分子内羰基-羰基偶联产物，而是得到反常的羰基与α，β-不饱羰基的双键偶联产物，较高收率地得到了含多官能团的CycI[3，2，2]azine衍生物。

The polymerization of butadiene in benzene in the presence of titanium tetraiodide triisobutyl aluminium catalyst has been studied.

研究了丁二烯在苯中有四碘化钛-三异丁基铝催化剂的存在下的聚合。

Pentek filter systems offer multistage, reverse osmosis, in-line, countertop, shower and faucet filter options, while Pentek specialty products and processes such as ultraviolet, bromination, iodination, and radial flow iron reduction increase our ability to meet specialized needs.

pentek过滤系统提供了多级，反渗透，在网上， countertop ，淋浴和水龙头过滤选项，而pentek特种产品和新工艺，如紫外线，溴化，碘化，并径向流还原铁增加我们的能力，以满足特殊需求。

Although itsapplication in organic synthesis has extented rapidly, a survey of literature showsthat CuCN·2LiCl is almost the only copper salt for the Michael addition reaction offunctionalized organozinc halides, and the amount of CuCN·2LiCl used isstoichiometric. Because of the toxity of CN〓, we try to carry out the reaction inother way instead of CuCN.

但在带官能团的有机卤化锌的Michael加成反应中，到目前为止基本上都是使用毒性较大的铜盐CuCN-2LiCl，为了寻找更好的方法，并使其成为催化反应，我们以带官能团的有机碘化锌的Michael加成反应为目标反应，对FG-R-ZnI在有机合成中的应用进行了考察，得到了较好的结果。

That 1,4-addition reactions of Grignard agent made from 1-bromo-3-triphenylmethoxyl-1-octene and organozinc agent made from 1-iodo-3-trimethysiloxy-1-octene with 2-(6-methoxylcarbonylhexyl)-4-(2- tetrahydro-pyranyloxy)-2-cyclopentenone both gave prostaglandin 〓 methyl ester statethat prostaglandin E compounds can be prepared by 1,4-addition reaction oforganozinc agent.

最后，研究了溴化-3-三苯甲氧基-1-辛烯基镁和碘化-3-三甲硅氧基-1-辛烯基锌与2-(6-甲氧羰己基)-4-(2-四氢吡喃氧基)-2-环戊烯酮通过1，4-加成反应合成〓甲酯的方法，结果表明，用有机锌试剂通过1，4-加成反应来合成PGE类化合物是可行的。

A series of test condition for determining the solubility product of PbI2 in the micro experiment was studied and a good result was obtained.

探索碘化铅溶度积测定实验微型化的最佳条件，介绍了该微型实验的方法。

CoCl2 (a chemical hypoxia-mimetic agent) was used to establish the chemical hypoxia-induced PC12 cell injuries model. Sodium hydrosulfide was used as a H2S donor. The viability of PC12 cells was measured by CCK-8 assay. The percentage of apoptotic cells was assessed by propidium iodide stain flow cytometry. The morphological change of apoptotic cells was tested by using the chromatin dye Hoechst 33258. The mitochondrial membrane potential was analyzed by rhodamine 123 staining and photofluorography. The level of reactive oxygen species in PC12 cells was measured by DCFH-DA staining and photofluorography.

应用化学性缺氧模拟剂CoCl2在PC12细胞建立化学性缺氧损伤模型；以硫氢化钠作为H2S的供体；应用CCK-8比色法检测细胞存活率；碘化丙啶染色流式细胞技术检测细胞凋亡率；Hoechst33258染色检测细胞凋亡的形态学变化；罗丹明123(Rh123)染色荧光显微镜照相检测细胞线粒体膜电位；2'，7'-二氯荧光黄双乙酸盐染色荧光显微镜照相检测细胞内的活性氧水平。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。