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A method for producing fatty acid alkyl esters and/or glycerin comprising a step of bringing a fat or oil into contact with an alcohol in the presence of a catalyst, wherein the catalyst is at least one catalyst selected from the group consisting of the following to: a metal oxide having an ilmenite structure and/or a slyrankite structure; an oxide containing a metallic element belonging to the Group 12 and a metallic element belonging to the Group 4; a mixed oxide containing a metallic element belonging to the Group 12 and a tetravalent transition metallic element; a metal oxide containing zirconium and at least one metallic element selected from the group consisting of metallic elements belonging to the Groups 4, 5 and 8; and a metal oxide containing anatase type titanium oxide and/or rutile type titanium oxide, and the metal oxide containing a sulfur component of 700 ppm or less.

脂肪酸烷基酯和/或甘油的制造方法包括在催化剂的存在下使脂肪或油与醇接触的步骤,其中,所述催化剂是选自由下列~所组成的组中的至少一种催化剂:具有钛铁矿结构和/或斯里兰卡石结构的金属氧化物;含有属于第12族的金属元素和属于第4族的金属元素的氧化物;含有属于第12族的金属元素和四价过渡金属元素的混合氧化物;含有锆和选自由属于第4、5和8族的金属元素所组成的组中的至少一种金属元素的金属氧化物;和含有锐钛矿型氧化钛和/或金红石型氧化钛的金属氧化物,并且所述金属氧化物含有的硫成分为700ppm以下。

In order to obtain versatile ulitity of host molecules, three new chiral calix [4] crown ethers containing aza, thio atoms bearing two chiral sites provided by -cysteine ester were synthesized by the condensation of calix [4] arene diacid dichloride with oligoethylene glycol bridged bis-amino acid methyl ester. All new compounds were characterized by NMR, MS and elemental analysis.

以-半胱氨酸为手性源,利用多甘醇二氯醚在碱性条件下对半胱氨酸巯基进行烷基化反应,成功地合成了多甘醇醚链桥联的半胱氨酸衍生物,醚化反应后,在高度稀释条件下与对叔丁基杯[4]芳烃二乙酰氯进行双功能基缩合反应成功地合成了新型的手性杯[4]含氮、硫杂冠醚,并利用〓H NMR、MS等谱图手段对其结构进行了表征。

The invention relates to a pipeline polyurea outer anticorrosive coating and the making method thereof, making heated prepolymerization reaction on dibenzo-methane diisocyanate, carbodiimide diisocyanate, polyether binary alcohol and polyether trihydric alcohol to prepare prepolymer solution A, and making end amino polyethylene oxide ether, dimethyl sulfur-based toluene diamine, diethyl diamine, iso-propyl titanate solution, polyacrylate, carbon black, titanium dioxide and lightweight calcium carbonate into solution B, and as using, respectively heating the solutions A and B to 65 deg.C and then mixing them, then quickly spraying and curing to form a coat.

本发明涉及一种管道用聚脲外防腐涂料及制造方法,由二苯基甲烷二异氰酸酯、碳化二亚胺化二异氰酸酯、聚醚二元醇和聚醚三元醇通过加热预聚反应制成预聚物的A液、由端氨基聚氧化乙烯醚、二甲硫基甲苯二胺、二乙基甲苯二胺、钛酸异丙酯溶液、聚丙烯酸酯溶液、碳黑、钛白粉和轻质碳酸钙配制而成的B液组成,使用时将A液和B液分别加热至65℃后混合,然后快速喷涂固化形成涂层。

A silver ion selective electrode was prepared and characterized with trimethylene bis (N-ethyl-N-phenyldithiocarbamate) as ionophore.

制备并考察了以双(N-乙基-N-苯基氨基二硫代甲酸)1,3-丙二醇酯为载体的银离子选择电极的性能。

The PrP of bastard halibut consists of 472 amino acid residues, weighing about 49.6kD. The deduced amino acid sequence is 71.9% similar to that of Japanese pufferfish and 66.4% similar to that of Atlantic salmon, and bears the structural signatures of PrPs including a signal sequence, tandem repeats, a hydrophobic region, two glycosylation sites, a disulphide bridge and a glycosyl phosphatidylinositol anchor site.

推测的牙鲆蛋白质感染因子蛋白由472个氨基酸组成,分子量约49.6kD,具有信号肽、短肽顺接重复、疏水区、糖基化位点、二硫键、糖基缩醛磷肌醇锚定位点等蛋白质感染因子蛋白特征结构域,与红鳍东方鲀和大西洋鲑蛋白质感染因子蛋白的相似性分别为71.9%和66.4%。

Plant volatiles as allyl isothiocyanate , Z-3-hexen-1-ol , and Z-3-hexenyl acetate can attract DBM effectively and they have enhanced effect on captures of sex lure.

同时研究了植物挥发物异硫氰酸丙烯酯、青叶醇(Z-3-hexen-1-ol)、乙酸顺-3-己烯酯(Z-3-hexenyl acetate)对小菜蛾的诱捕作用及对性信息素诱捕作用的影响。

This method had been applied to determination of the optical purity of the product from asymmetric ring opening of meso- epoxides.

方法已用于非手性环氧化合物不对称开环反应产物β-氨基醇及β-羟基硫醚类化合物的光学纯度鉴定。

Totally, 147 flavor compounds, which comprised of 17 acids, 12 alcohols, 16 aldehydes, 36 esters, 12 furans, 13 ketones, 14 miscellaneous compounds, 8 phenols, 6 pyrans, 4 pyrazines, 3 pyrroles, 6 sulfur-containing compounds, were identified.

共鉴定出147种风味化合物,其中酸类17种、醇类12种、醛类16种、酯类36种、呋喃12种、酮类13种、杂环化合物14种、酚类8种、吡喃6种、吡嗪类4种、吡咯3种、含硫化合物6种。

As far as these organic matters are concerned, there are as much sixteen kinds of low molecular weight organic acids and Aldehyde, Alcohol, Ketone, Carboxylic acid, Carboxylic acid, Furan, Pyrazine, Fat hydrocarbon, sulphide and so on. The results have also shown that the content of Aldehyde, Alcohol, Fat hydrocarbon, Carboxylic acid, Furan, Pyrazine, sulphide in composted production amended with NMF inoculants increased 6.5%、9.2%、5.7%、15.6%、9.8%、11.3% and 28.6%, respectively.

研究证实添加微生物腐熟菌剂的奶牛粪堆肥产品中醛类、醇类、酯类、羧酸类、呋喃类、吡啶类和含硫类等低分子有机化合物的相对含量比未添加NMF微生物腐熟菌剂分别增加6.5%、9.2%、5.7%、15.6%、9.8%、11.3%和28.6%,而酮类、脂肪族碳氢化合物的相对含量则分别减少11.4%和15.5%。

Among these, the most prevalent was endosulfan-diol, with an average concentration of 4.15 nanograms per gram of placenta.

在这些中最普遍的是二醇硫丹,它的平均浓度为每克胎盘组织中富集4.15毫微克,令人惊讶的是,668例孕妇样本中,一些患者的胎盘中甚至含有15~17 种杀虫剂。

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