硫酸化

Aniline compounds are used as raw material and reacted with anthranilic acid and then phenyl iodide as alkylating agents to give alkylating products followed by cyclizing with concentrated sulphuric acid to give a N-phenyl-acridone(or 3-ethoxyl-N-phenylacridone).The structure of intermediate and target compound are determined by IR and MS.

以苯胺类化合物为原料，先后以邻氯苯甲酸和碘苯为烷基化试剂进行了N 烷基化反应，再用浓硫酸使其环化制得N-苯基吖啶酮和3-乙氧基-N-苯基吖啶酮，并用红外光谱及质谱仪检测了各中间体及目标产物的结构。

Potassium bromide produced in the elimination step was cleaned with steam treatment, then used to bromize tert-Butyl alcohol, producing tert-butyl bromide.

为了回收中间元素澳，用水蒸汽蒸馏方法除去脱漠化氢后生成演化钾盐中的杂质，通过添加硫酸以再生漠化钾用于叙丁醇漠化制漠代叔丁烷。

Cellulose acetate butyrate with high or low degree of butyryl substitution was synthesized in heterogeneous system(butyric acid/ acetic acid/ butyric anhydride/ sulfuric acid) using the "free solvent" method. The effect of activation time, esterification time, the molecular weight of cellulose and the content of the organic acid or anhydride on the degree of acetyl and butyryl substitution of cellulose was discussed.

在非均相体系中进行酯化反应，采用&反应性溶剂&，以硫酸作为催化剂合成出从高丁酯含量到低丁酯含量的纤维素醋酸丁酸酯，研究有机酸以及酸酐的添加量、活化时间、酯化反应时间以及原料纤维素的分子量对酯化产物纤维素醋酸丁酸酯的影响。

Experimental results show that esterification reaction proceeds effectively at 200℃ with ferric sulfate as catalyst.

论文研究选用硫酸铁作酯化反应的催化剂，在醇酸摩尔比10：1.0，酯化温度200℃，酯化时间2小时。

The results show that the optimal parameters of esterification are as follows: 4% of SO42-/ZrO2, molar ratio of methanol to litsea cubeba kernel oil 101, 68 ℃ of reaction temperature and 4 h of reaction time, the acid value decreases to 2.52 mg/g. Compared with the traditional acidic-catalyzed method, this method has the advantages of no acid proof equipment, easy to recycle catalyst and no acidic waste water emission. The optimal parameters of transesterification are as follows: 25 ℃ of reaction temperature, 0.5% of hexadecyl-trimethyl-ammonium bromide, 1% of NaOH, molar ratio of methanol to the oil 61 and 15 min of reaction time. The ester exchanging rate is 97.6%. This method adopts phase transfer catalyst and produces industry prospect, which has many advantages such as energy-saving and time-saving under room temperature.

研究结果表明，固体酸SO42-/ZrO2催化酯化反应的最佳条件为：油重4%的SO42-/ZrO2，醇油摩尔比为101，温度为68 ℃，反应时间为4 h，原油酸值降到2.52 mg/g；该法相对浓硫酸催化酯化法具有不需耐酸设备、催化剂易回收、无废水排放等优点；相转移催化酯交换反应的最佳条件为：温度为 25 ℃，0.5%的十六烷基三甲基溴化铵，油重1%的NaOH，醇油摩尔比为61，反应15 min，原油酯交换率达到97.6%；采用相转移催化技术，反应在常温下进行，大大减少了能耗，缩短了反应时间，具有的产业化前景。

After coupling diazotized p-chloroaniline with imidazole, the resulting monoazo dye is quaternized with dimethyl sulfate. Upon dimethylamination, the ...

对-氯苯胺重氮化后，与咪唑偶合，生成单偶氮染料，与硫酸二甲酯季铵化，所得季铵化合物再经二甲胺基化即为题示染料。

In this thesis,MWNTs were modified firstly using concentrated acid of H_2SO_4 and HNO_3,and then octadecyl isocyanate was grafted onto the surface of the MWNTs to improve the dispersion and the interaction between the filler and the matrix.

第一步，用浓硫酸和浓硝酸的混合液对MWNTs进行酸化处理，第二步，用廉价的十八烷基异氰酸酯对酸化过的MWNTs进行烷基化处理。

Passivation process also has some drawbacks, including hard buck coke catalyst bed treatment、polythionic acid stress corrosion cracking prevent for sensitively materials, meanwhile passivation process must be coordination between skillful local workers with knowledgeable company.

钝化法也有一些潜在的缺点必须注意，同时也是需要厂商负责保证，主要包括大块结焦废触媒的处理、钝化剂化学成分是否会对设备材质造成潜在伤害的确认及设备因敏化而产生聚硫酸应力腐蚀的预防等。

A series of sulphonated SBS were achieved by reacting SBS blockcopolymer with sulphuric acid, meanwhile, the blends of PVC andsulphonated SBS were studied. By means of strength capabilityexamination and DSC analysis, it was found the miscibility wasincreased after SBS was sulphonated.2 The chemical grafting of styrene and PVC membrane2.1 The reaction condition of graftingBy means of the swelling and seepage of Styrene to PVC film,St was grafted onto PVC film by the initiation of BPO .

采用硫酸对热塑性弹性体SBS进行磺化，得到不同磺化度的产物，并对其与PVC的物理共混进行了研究；通过力学性能及DSC测试，发现SBS磺化后增加了与PVC的相容性(来源：Af2a2a2BC论文网www.abclunwen.com)。2 苯乙烯与聚氯乙烯膜的化学接枝2.1 苯乙烯与聚氯乙烯膜接枝条件利用苯乙烯对PVC的溶胀渗透，在过氧化苯甲酚的引发下发生接枝共聚反应。

The existence of titanium dioxide and titanyl sulfate reduces the corrosion of zinc deposits.

结果发现：钛的加入能明显提高钝化膜的耐蚀性，这是由于钝化膜中形成二氧化钛和硫酸氧钛，它们掺杂在钝化膜及其腐蚀产物中，有效抑制了锌镀层的腐蚀。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。