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硫酸化

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With increasing number of hot-wall hydroprocessing reactors and extension of service time, the occurrence of polythionic acid corrosion, hydrogen induced spalling of weld overlay, temper embrittlement of base metal, hydrogen embrittlement and surface cracking etc.

随着国产热壁加氢反应器的数量不断增加和服役时间的延长,连多硫酸腐蚀、堆焊层氢致剥离、母材回火脆化、氢脆、表面开裂等时效损伤出现的情况越来越多。

Iron grade is 35%~60%.Utilization of pyritic slag, the study on production of DR process metallization nodule with pyritic humidifying granding and forming was proposed.

利用硫酸烧渣,进行了煤基直接还原生产金属化团块的研究,提出了润磨造球-预热焙烧-磁选-冷固结成型的新工艺流程。

The compositions by weight percentage of the passivation solution are: 3.12 to 4.74 percent of EDTA, 2.60 to 3.95 percent of hydroxylamine sulfate, 0.52 to 2.37 percent of citric acids, 1.04 to 2.77 percent of sodium pyroborate, the balance being water.

本发明钝化液由重量百分比为:3.12%~4.74%的EDTA、2.60%~3.95%的硫酸羟胺、0.52%~2.37%的柠檬酸、1.04%~2.77%的四硼酸钠和余量的水组成。

Accordingly a further feature of the invention is a combined process wherein a dialkyl phenylethylmalonate is made from an alkyl phenylacetate and a dialkyl carbonate by a process comprising adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C, at least a chemically equivalent proportion of a lower aliphatic alcohol, subsequently adding an approximately equivalent proportion of a dialkyl carbonate and of an alkyl phenylacetate, heating the mixture to induce reaction and continuously distilling out the alcohol formed from the reaction zone and finally causing the sodio diethyl phenylmalonate so obtained to interact with an ethylating agent, such as ethyl halide, diethyl sulphate of ethyl p-toluene-sulphonate.

因此,本发明的另一个应用是一个组合工艺过程:二烷基苯基乙基丙二酸酯由烷基乙酸苯酯和二烷基碳酸酯得到,具体工艺过程是:向覆盖有沸点超过一百摄氏度的团庆化合物溶剂的金属钠中添加至少化学平衡的低级脂肪族醇,然后加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯,加热混合物引导反应进行,持续蒸馏把形成的醇类从反应区域移出,最后使获得的二乙基苯基丙二酸酯和乙基化试剂如卤代乙烷,二乙基硫酸酯形成乙基p-甲苯磺酸酯。

A novel naphthenic petroleum sulphonate was prepared in laboratory with the naphthenic oil and fuming sulfuric acid.

在实验室用发烟浓硫酸对环烷基油进行磺化反应,合成了一种新型的三次采油用表面活性剂:环烷基石油磺酸盐。

A novel sulphonate oil-displacement surfactant was made in laboratory using ester and fuming sulfuric acid and by hydrolysis and neutralization technologies.

摘要用发烟浓硫酸对油酯进行磺化,水解、中和后制成了磺酸盐驱油剂。

Through the analysis of szaibelyite ,the manufacture method of boric acid and magnesium carbonate from szaibelyite by sulfuric acid,CO_2 and ammonia water is determined.

对硼镁矿成分进行分析,从而确定了采用硼镁矿制取硼酸联产碳酸镁工艺路线———用硫酸分解硼镁矿制取硼酸,硼酸母液经处理后加入碳化氨水制取碳酸镁。

After more than ten years of development, has become a metal surface conditioning, phosphating solution, degreasing agents, rust agent, titanyl sulfate-led products, has an independent legal personality of the chemical products manufacturing enterprises.

经过十余年的发展,已成为一家以金属表面调整、磷化液、脱脂剂、除锈剂、硫酸氧钛为主导产品,具有独立法人资格的化工产品生产企业。

In the sensitive and simple method, the p-phenylenediamine dihydrochloride was oxided to diazotized products with the reaction of NaNO2 in H2SO4 medium.

色氨酸与重氮化的对苯二胺二盐酸盐在硫酸介质中生成粉红色化合物,该化合物最大吸光值为522nm;摩尔吸光系数为0.89×104L/mol·cm;偶合产物至少稳定存在1h;色氨酸浓度在0.30~12μg/ml范围内遵循朗伯比尔定律。

The yield was 47.3%. A series of21 azo-1,3,4-thiadiazole compounds were synthesized by diazotizing of2-amino-5-alkyl-1,3,4-thiadiazole with nitrosylsulfuric acid, then couplingwith phenol, substituted phenol or naphthol. The yields were 19.6~58.8%.16 of them were new compounds.

制得的2-氨基-5-烃基-1,3,4-噻二唑用亚硝酰硫酸进行重氮化,再与苯酚、取代苯酚或萘酚发生偶合反应合成了21个偶氮-1,3,4-噻二唑类化合物,其中16个为新化合物,收率为19.6~58.8%。

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