硫酸化

METHODS Phase-transfer catalytic methylation and suitable method of aftertreatment were used.

采用相转移催化法以硫酸二甲酯为甲基化剂进行α-甲基化反应，并采用适当的后处理方法。

The chondrocytes of different generation were observed with light-microscope and transmission electron microscope for cellular growth and ultromicrostructure, with the method of MTT assay for grow curve and proliferation, with alcian blue test for GAG of ECM, with immuocytochemistry and RT-PCR (reverse transcript -polymerase chain reaction)for type Ⅱcollagen, with flow cytometry for cell life cycle ,histochemistry for S-A-β-galand so on by which to identify cataplasia and senescence of chondrocytes cultured in vitro.

对软骨细胞退变老化进行观察，采用相差显微镜观察其生长情况，透射电镜观察细胞结构，阿力新蓝染色检测胞外基质硫酸GAG含量和结构，免疫细胞化学法和RT-PCR方法检测Ⅱ型胶原鉴定软骨细胞，以MTT比色法描绘生长曲线、检测生长状态，组化法检测老化相关β-半乳糖苷酶，流式细胞仪分析细胞周期和增殖指数。3。

The results show that the yield of butyl acetate using the catalysts prepared with the concentration of H2SO4 by 0.5 mol·l-1 and the calcination temperature of 550℃ is the best,which is up to 52.5% when the molar ratio of butyl alcohol to acetic acid is 1:1.3 and without addition of entrainer in the hermetic reactor.

结果表明采用硫酸浸渍液浓度为0.5mol/L，焙烧温度为550℃时所制备的催化剂在正丁醇和乙酸的物质的量比为1.3及不添加任何带水剂的密闭条件下酯化效果最好，酯化率为52.5%。

Strong acids, such as sulfuric acid, hampered from the occurrence of the phenol hydroxylation.

过强的酸，如硫酸、硝酸和盐酸，对苯酚羟基化反应造成危害，使羟基化反应不能发生。

The propagation of non-sensitized IGC and the relation of IGC to potential values were investigated in sulfuric acid at ambient temperature.

用恒电位浸蚀方法在高压釜中研究了供货态316 L钢在尿素介质中发生非敏化态晶间腐蚀与电位区段的关系，并在常温硫酸溶液中研究了316 L钢非敏化态晶间腐蚀的发展过程及其与电位值的关系。

Difluorodiphenylsulfone and 4, 4"-difluorodiphenylketone are sulfonated by 50 % sulfuric acid. A new biphenol monomer containing six-membered ring imide is synthesized by reaction of 1, 4, 5, 8-naphthelenetetracarboxylic acid dianhydride with 3-aminophenol or 4-aminophenol sodium.

以50%发烟硫酸为磺化试剂，以4，4′-二氟二苯砜和4，4′-二氟二苯酮为原料反应得到双磺化的4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯砜和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯酮。

Various inorganic acid, such as ammonium chloride, copper sulfate, aluminum sulfate, mercury chloride, cerium sulfate and cerium chloride, have been evaluated for copper powder, zinc powder, or tin powder-mediated allylation reactions of carbonyl compounds with allyl bromide in aqueous medium.

结果表明：在同样的反应条件下，与铜粉或锌粉作用的此类反应相比，锡粉能更好的作用羰基烯丙基化反应，并且该反应的产率都比较高；在同样的金属促进剂存在下，硫酸亚铈的促进性能是所有无机酸中最好的。 2、研究了二氧化碳促进羰基化合物烯丙基化反应。

It can be use as an environment-friendly intermediate and starting material for organic synthesis substituting the poisonous phosgene and dimethyl sulfate in carbonylation and methylation reaction.

它可以代替剧毒的光气和硫酸二甲酯作为环境友好的有机合成中间体和起始物质，应用与羰基化和甲基化反应中。

It can be used as an environment-friendly intermediate and starting material for organic synthesis substituting the poisonous phosgene and dimethyl sulfate in carbonylation and methylation reaction.

它可以代替剧毒的光气和硫酸二甲酯作为环境友好有机合成中间体和起始物质，应用于羰基化和甲基化反应中。

This paper simulates the main component of biomass-cellulose with pledget and the filter paper .

以脱脂棉、滤纸模拟生物质的主要组分之一纤维素，在不同稀硫酸浓度、时间和温度反应参数下，进行纤维素水解糖化试验研究，以还原糖量为指标，考察纤维素糖化最佳反应条件。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。