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Effect of Common Goldenrod Herb on rats Gastrelcosis Caused by Indocin;2. Animal Model of Helicobacter pylori Infection in BALB/c Mice with Gastrelcosis ;3. AIM To study the synthesis of zinc chlorin e 4 (1), its experimental antigastrelcosis activity as well as the protection against acute liver injuries.

蚕沙叶绿素粗品经酸碱降解反应制得二氢卟吩e6(3),3经吡啶回流降解制得二氢卟吩e4 (2 ),2与醋酸锌络合制得 1;并测定 1对消炎痛诱发的大鼠胃溃疡的保护作用及对硫代乙酰胺、四氯化碳所致小鼠急性肝损伤的防治作用。

Objective:To observe the effect of Jiawei Zhenwu Tang on rat model of hepatorenal syndrome.

目的:研究加味真武汤对硫代乙酰胺所致肝肾综合征模型大鼠肝肾功能的影响。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

Methods: The rats were injected with thioacetamide 600mg/kg twice at same time for two days to induce the model of acute hepatic failure rat except the normal group injected with the normal saline hypodermically.

按600mg/kg的剂量经皮下注射硫代乙酰胺1次,24小时后按相同剂量重复注射1次,造成大鼠急性肝衰竭模型,于实验前3天至实验结束分别给予各组大鼠生理盐水,不同剂量丹黄方及促肝细胞生长素,观察造模后48小时内大鼠病死率,并于造模48小时后经腹主动脉采血测定ALT、AST、TBil、TNF-α、IL-6,取肝组织作病检。

Another method for determining primary structure is to employ Edrnan's , which reacts quantitatively with the free amino group of a peptide to yield the corresponding pheny lthiocarbamoyl peptide, leaving the rest of the peptide chain intact.

另一种可以决定初级结构的方法是用埃德曼降解法,它们能与肽键上的游离氨基定量反应,产生相应的苯氨基硫代甲酰肽,而其余的肽链保持不变。

Mainly engaged in sodium azide, barium azide, three phosphorus nitride Friday, phenyl isothiocyanate, 1 - phenyl -5 - mercapto-tetrazole, 4 - dimethylamino-pyridine, 2 - mercapto--5 -- methyl-1,3,4 thiadiazole, N-hydroxy phthalimide, anhydrous betaine and betaine hydrochloride, such as fine chemical raw materials and medicine, pesticide intermediates of the development, production and sales.

主要从事叠氮化钠,叠氮化钡,五氮化三磷,异硫氰酸苯酯,1-苯基-5-巯基四氮唑,4-二甲氨基吡啶,2-巯基-5-甲基-1,3,4噻二唑,N-羟基邻苯二甲酰亚胺,无水甜菜碱及甜菜碱盐酸盐等精细化工原料及医药、农药中间体的开发、生产和销售。

Chapter III We try to synthesizing pyrazole by hydrazine and thiourea in alkaline conditions, we found we can not get the acyl pyrazole in the conditions of synthesizing succinylthydrazine and ferrocenyl chalcone, pyrazole was got instead.

第三章我们尝试以酰肼及氨基硫脲作为氮源在碱性条件下来合成吡唑类化合物,并取得了理想的结果。

Two novel pyrazolone derivatives 2-ethylamino-6H-5-(1-phenyl-3-methyl/phenyl-5-pyrazolone-4-ylene)-1,3,4-thiadiazine (PMCP-ETSC/DPCP-ETSC) containing NNS six-membered heterocycles were synthesized by the condensation reaction of 1-phenyl-3-methyl/phenyl-4-chloroacetyl-pyrazolone-5 with 4-ethyithiosemicarbazide. The title compounds were characterized by elemental analysis, IR, 1H NMR, 13C NMR and single-crystal X-ray diffraction.

利用1-苯基-3-甲基/苯基-4-氯乙酰基-吡唑啉酮-5与4-乙基氨基硫脲发生缩合反应,生成了2个新的双杂环化合物2-乙氨基-6H-5-(1-苯基-3-甲基/苯基-5-吡唑啉酮-4-基)-1,3,4-噻二嗪(PMCP-ETSC/DPCP-ETSC),并对其进行元素分析、红外光谱、核磁共振表征和晶体结构分析。

The Schiff base of O-ethylthonophosphoryl-dihydrazine with salicylaldehyde and its Ni, Cu, Zn complexes was synthesized.

合成了O-乙基硫代磷酰二肼的双水杨醛席夫碱(H2L)及以它为配体分别与Ni、Cu、Zn离子形成的配合物,所合成的席夫碱配体及配合物均为未见文献报道的新化合物。

Using silicotungstic acid as catalyst with the catalyst supported on active carbon,2-methyl-2-ethyl-acetic-1,3-oxathiolane(targeted compound I,an aroma compound with apple flavor )was synthesized by the reaction of ethyl aceto-acetate and 2-mercapto-ethanol.

以活性炭固载硅钨酸作为催化剂,用乙酰乙酸乙酯与巯基乙醇缩和合成了具有浓郁苹果香气的香料化合物2-甲基-2-乙酸乙酯基-1,3-氧硫杂环戊烷。

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