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In addition a series compounds of thiazole glycosides (17a~17f) were synthesized through 1-benzoyl-3-aryl-thioureas by phase-transfer catalysis method under mild condition.

另外,本文以1-苯甲酰基-3-芳基硫脲为原料通过相转移合成法合成了一系列噻唑类糖苷的衍生物(17a~17f)。

Two methods were taken to synthesize the tris(4-aminophenyl)thiophosphate: One is amide-hydrolyzing process, the other is one-step reaction.

采用酰胺水解法和催化反应法两种方法来合成硫代磷酸三(4-氨基苯)酯。

O-(1-Arylseleno-3-azido)isopropyl-O-2-(N3-tegafur)alkyl thiophosphate (3a~3f) were obtained via nu-cleophilic ring-opening of sodium azide to 2a~2f in dry DMF at room temperature, and their antitumor activities were tested.

以无水N,N-二甲基甲酰胺作溶剂,室温下,叠氮化钠中对2a~2f进行亲核开环,得到O-(1-芳硒基-3-叠氮基)异丙基-O-2-(N3-替加氟)乙基硫代磷酯。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明,在分析出的21种香气成分中,分别有脂肪酸类8种,酯类5种,醛类2种,氮硫杂环类2种,烃类、醇类、酮类、内酯类各l种,其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯,其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

The voltammetric behavior of Pb facilitated by dithizone (DzH2) across the water/acetylacetone interface was investigated by cyclic voltammetry.

用循环伏安法研究了双硫腙络合推动Pb2+在水/乙酰丙酮界面迁移的伏安过程。

Quantum chemical and molecular mechanical methods were employed to study the acylation in the acetylthiocholine hydrolysis catalyzed by acetylcholinesterase.

应用量子化学和分子力学方法研究乙酰胆碱酯酶催化硫代乙酰胆碱水解反应中的乙酰化反应,计算了反应物、过渡态、产物及中间体的几何结构及电子结构。

New sulfonyloxadiazolones have the formula, in which A stands for hydrogen, sulphur,-SO-,-SO2- or a group, in which R stands for hydrogen or alkyl; R stands for optionally substituted cycloalkyl, cycloalkenyl or aryl; and R stands for optionally substituted alkyl, alkenyl, dialkylamino or aryl.

本发明涉及式新的磺酰基__二唑酮,其中,A代表氧、硫、-SO-、-SO 2 -或基团,其中R 3 代表氢或烷基;R 1 代表任选被取代的环烷基,任选被取代的环烯基或任选被取代的芳基;和R 2 代表任选被取代的烷基,链烯基,二烷基氨基或芳基。

The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.

报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物,邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证

This experiment adopted lipoic amido dehydrogenase histochemistry method and image pattern analysis technique to investigate the relationship between nitric oxide synthase neurons and activity of NOS and auditory threshold, and to explore the possible role of NOS neurone in cochlear nuclei of guinea pigs after exposed to white noise.

采用硫辛酰胺脱氢酶组织化学方法及图象分析技术,研究白噪声暴露后豚鼠耳蜗核一氧化氮合酶神经元及NOS活性的变化与听阈的关系,探讨豚鼠耳蜗核NOS神经元在白噪声损伤过程中可能的作用。

This experiment adopted lipoic amido dehydrogenase histochemistry method and image pattern analysis technique to investigate the relationship between nitric oxide synthase neurons and activity of NOS and auditory threshold, and to explore the possible role of NOS neurone in cochlear nuclei of guinea pigs after exposed to white noise.

提要 采用硫辛酰胺脱氢酶组织化学方法及图象分析技术,研究白噪声暴露后豚鼠耳蜗核一氧化氮合酶神经元及NOS活性的变化与听阈的关系,探讨豚鼠耳蜗核NOS神经元在白噪声损伤过程中可能的作用。

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