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Ten benzoylthiourea s containing substituted pyrimidine ring were synthesized,among them seven are new compounds.

合成了10种含不同取代嘧啶环的苯甲酰硫脲类化合物,其中7个为未见文献报道的新化合物。

E-44 epoxy resin,"¨" PF2A2-131, PF2A2-141 Brand Bakelite powder,"Golden Harvest card" 40 percent different, such as rice blast net EC was namedproducts, o-toluene sulfonamide amide, sodium benzoate eight product quality by the title of Zhejiang Province; 25% quinalphos National New Product by Product Jinlong Award.

熊猫牌"E-44环氧树脂、"熊猫牌"PF2A2-131、PF2A2-141牌号酚醛塑料粉、"嘉禾牌40%异稻瘟净乳油等被评为部优产品,邻甲苯磺酰胺、苯甲酸钠等八个产品获浙江省优质产品称号;25%喹硫磷产品获国家新产品金龙奖。

Methods The lymphocytes of rats were isolated from the peripheral blood and cultured with sodium arsenite under 37 ℃.The ROS content was detected by DCFH-DA;The content of LPO was detected by fluoresce method.

体外分离大鼠外周血淋巴细胞后,施加处理因素,在37℃条件下恒温培养,用2'7'-二乙酰二氯荧光素染色法检测细胞内的ROS水平,用硫代巴比妥酸荧光法测定细胞内LPO含量。

The results show that it only takes 8 min for the reaction, when the initiator is potassium persulfate/sodium thiosulfate which forms an oxidation-reduction initiator system; N,N-methylene diacrylamide is as cross-linker; neutralization degree is 70%, under the microwave power of 360 W.

结果表明,在360W的微波辐射功率下,采用过硫酸钾与硫代硫酸钠的氧化还原引发体系,N,N-亚甲基双丙烯酰胺为交联剂,接枝单体的中和度为70%时,只需8min就可以完成纤维素基高吸水树脂的接枝共聚合成。

The method applied is in accordance with that of the PRC National Standard for the determination of urease activity in soya bean products.

参考了中华人民共和国国家标准大豆制品中尿素酶活性测定方法,进行了正丁基硫代磷酰三胺活性的测定。

The traceless Staudinger ligation of azides and phosphines is an effective method to produce an amide bond.

叠氮化合物和膦硫酯的无痕施陶丁格连接反应是一种有效生成酰胺键的方法。

Effect of several reaction factors on the yield of the synthesis of methane sulfonyl chloride is discussed.

阐述了利用二甲基二硫在相转移催化剂作用下,于盐酸介质中经氯气直接氧化,一步合成甲烷磺酰氯的工艺过程,讨论了几个主要反应因素对产物收率的影响,确定了适宜的工艺条件。

Methods 42 Wistar male rats of hepatic fibrosis were induced by TAA and divided into 7 groups randomly (n=6). The rats of 1 model group were sacrificed every 2 weeks.

60只雄性 Wistar大鼠应用硫代乙酰胺饮用水喂养,制备肝纤维化模型。42只大鼠模型制备成功后,随机分为 7 组,每组6只。

Methods: FHF was developed by subcutaneous injection of TAA.

采用硫代乙酰胺皮下注射复制大鼠暴发性肝衰竭动物模型。

Methods Naloxone was synthesized starting from oxidation of thebaine, followed by hydrogenation, acylation, cyanidation, O-demethylation, hydrolyzation and N-allylation. The alternative method of O-demethylation, methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

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