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Alkylamine reaction with dialkyl cyanodithioiminocarbonate was catalyzed by quaternary ammonium salts at room temperature to yield 3-alkylamine-5-amino-1,2,4-triazole in good quality and high yields. After imidization and reaction with an α,β-unsaturated acid derivative, the reaction intermediate was hydrolyzed in the presence of a Lewis acid to obtain the target product.

烷基胺与氰基亚胺硫代二甲酯在季氨盐催化作用下得到质量好、收率高的3-烷氨基-5-氨基-1,2,4-三氮唑,进一步经过亚胺中间体并与α,β-不饱和酸酯作用后,中间产物在Lewis酸催化作用下水解得到三唑嘧啶酮。

A reaction pathway for ammonolysis of O,O-dimethylphosphorochloridothioate without catalyst was proposed,based on the reaction mechanism of acyl halide ammonolysis ,and the pseudo-homogeneous reaction kinetics were founded.

模型表明:在反应前期,O,O-二甲基硫代磷酰氯浓度对速率影响很小,反应速率呈拟一级反应特征;但在反应后期,反应速率呈明显的二级反应特征。

Objective To observe the effects of Astragalus injection of different doses on TAA-induced acute liver injury in rats.

目的 观察不同剂量黄芪注射液对硫代乙酰胺所致大鼠急性肝损伤的影响。

The volunteers also swallowed 11 vegetables that are bitter but lack glucosinolates, including aubergine, bitter melon and spinach.

自愿者们还吃了 11 种有苦味但不含硫代葡萄糖苷的蔬菜,包括茄子、苦瓜、菠菜。

Methods The changes of brain tissue ET, malonicaldehyde and excitatory amino acids and possible actions of anti-ET serum in 7 neonatal rats with hypoxic-ischemia and 8 control rats were observed by RIA, TBA and amino acid autoanalysis.

应用放射免疫法、硫代巴比妥法及氨基酸自动分析法观察:(1)正常鼠(n=7)及低氧缺血新生鼠(n=8)不同脑组织内皮素的变化。

The synthesis of gold and platinum nanoparticles by the reduction of their salts with potassium bitartrate as the reductant and poly (N-vinyl-2-pyrrolidone) or 3. 3-thiodipropionic acid as the capping agent has been studied.

对以聚和3,3—硫代二丙酸为覆盖试剂通过酒石酸氢钾还原相应的金属盐制备金、铂纳米粒子作了研究。

The reaction of calcium L-threonate with hydrogen bromide in acetic acid readily yields (2S, 3S)-2, 4 -dibromo-3 -hydroxy butanoic acid which was further converted into methyl (2s, 3S)-2,4-dibromo-3-hydroxybutanoate by treatment of methanol.

在化合物12上引入氨基甲酰基可用二氯磷异氰酸酯、氯乙酰异氰酸酯或氯磺酰异氰酸酯,随之引入的二氯磷酰基、氯乙酰基或氯磺酰基可分别用碳酸氢钠、N-甲基二硫代氨基甲钠或亚硫酸钠脱去。

The results showed that the detract ratio of glucosinolates in rapeseed meal was about 50%~60%.

试验结果表明:菜籽粕中硫代葡萄糖甙的降解率约在50%~60%。

Methods Surface plasma resonance, circular dichroism and fluorescence experiments were conducted.

应用表面等离子体共振、圆二色散以及荧光光谱法对白蛋白与硫代寡核苷酸的结合行为进行了表征。

Objective:To determine glucosinolates in Draba nemorosa var.leiocarpa and provide the basic and science data for further development.

目的:测定光果葶苈全草中硫代葡萄糖苷的总含量,为进一步研究开发提供基础科学资料。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。