硫

Properties of sulfur passivated GaAs (100) surfaces are studied by using photoelectron spectroscopy and photoluminescence measurements. Some practical applications of the sulfurizing technique are carried out and very promisingt results are obtained.

本文通过光电子能谱的手段和光荧光谱的方法分析了硫钝化GaAs(100)的性质并在此基础之上对硫钝化的实际应用进行了初步的尝试取得了较好的效果。

Two series of polyurethane acrylate grafted acrylic resins (Acr-g-TPU-PETA and Acr-gPPU-PETA) self-emulsifying systems are obtained by grafting -NCO group modified polyurethane acrylates with acrylic copolymer prepared from n-butyl acrylate, styrene,βhydroxyethyl methacrylate and acrylic acid The self-emulsifying systems showed Newtonian fluidity with viscosity closed to that of water, the solid contents were around 30% The T〓 of 15～4℃ for dried film before photocuring favored film formation at room temperature DSC and DMA results showed that PU-PETA is compatible with acrylic resin in the grafted resin The TG and dTG curves for Acr-g-PU-PETA samples were substantially different from the corresponding blends, and the brodened dTG peaks for photocured grafted resin suggest that there might be multiple interactions among chain segments The photocued film of the grafted resins self-emulsifying system exhibited good overall properties with polyurethane acrylate grafts ranging from 30% to 50%, and Acr-g-TPU-PETA series showed better properties than Acr-gPPU-PETA series The adhesion of the photocured film was 1～2 grade, impact strength was 50kg-cm and flexibility was 1mm The Shore hardness and the adhesion of the film decreased markedly if PETA was replaced by HEMA as photoactive group due to the lower C=C double bond content in the grafted resin The polyhydroxy amine-linked thioxanthones photoinitiators can be evenly dispersed in self-emulsifying system without color spot appearing in the dried film The films photocured with IV〓～IV〓 generally exhibited higher Shore hardness, gloss and solventresistance than that cured with Irgacure 2959 and did not induce the rusting of the iron substrate Pigmenting with titanium oxide had no effect on the photocuring The polyhydroxy amine-linked thioxanthone IV〓 and IV〓 can be new candidates for the formulation of titanium oxide pigmented photocurable water-borne coatings for their pale-yellow appearance and slight interference with the color of the coatings WB 4759 with high water-solubility coalesced and separated from the dried resin film, and even induced the rusting of iron substrate.

以丙烯酸丁酯，甲基丙烯酸-β-羟乙酯，丙烯酸及苯乙烯合成厂丙烯酸共聚树脂，并与含-NCO端基的聚氨酯丙烯酸酯接枝反应，经水性化后，得到两个系列（Acr-g-TPU-PETA和Acr-g-PPU-PETA）各5个不同配比的丙烯酸树脂接枝聚氨酯丙烯酸酯自乳化体系，粘度与水相近，为牛顿流体，固含量30％左右。光固化前干燥涂膜的玻璃化转变温度在-15℃～4℃之间，有利于室温下成膜。DSC及DMA谱表明两种树脂基本相容。Acr-g-PU-PETA的热失重行为明显不同于共混材料，接枝样dTG峰明显宽化，表明接枝样中链段之间的相互作刚有多重性，丙烯酸树脂与聚氨酯之间有一定的相容性。接枝树脂自乳化体系光固化涂层的综合性能以聚氨酯丙烯酸酯成分为50％～30％者相对较好，且以Acr-g-TPU-PETA系列更理想。光固化膜的附着力为1～2级，冲击强度为50kg·cm，柔软性多为1mm。以HEMA代替PETA作为接枝树脂的活性基团，碳—碳双键密度太低，光固化膜交联点太少，硬度和附着力均较差。多羟基胺连硫杂蒽酮光引发剂能均匀分散于树脂自乳化体系和接枝树脂干膜中，不出现色斑，光固化膜肖氏硬度一般高于以Irgacure 2959为光引发剂的光固化膜，光泽度及耐丁酮溶剂性能均有所提高，不会诱导铁基生锈，钛白着色对光固化结果几乎没有影响。本论文所合成的多羟基胺连硫杂蒽酮光引发剂IV〓与IV〓为浅黄色，对光固化涂层的颜色干扰较小，为配制钛白着色光固化水性涂料提供了新的光引发剂。水溶性太强的WB 4759在干膜中易聚结析出，且对所附着的铁基有诱导锈蚀作用。

In this research, B2 gene of HCV was highly expressed as a fusion protein (Trx-B2) by cloning into pThioHisA, and induced specific anti-HCV antibody in higher titer than unmodified B2 protein after immunize mice or rabbit.The results showed antigen Trx-B2 has obvious immunogenicity and induced specific antibody,which might be able to serve as diagnosis HCV. Consequently, this PcAb of rabbit was used to coated Immulon plate, and a method of both antibodys sandwiching antigens was developed to detect 32 HCV positive serum and 32 nomal serum.Results show that ratio of positive are 87.5%and 43.75% respectively.

但缺点是该抗原所诱导的抗体滴度较低，可能是由于其分子量较小，所以本课题将人工合成的HCV复合多表位抗原基因B_2克隆到表达载体pThioHisA中，利用硫氧还蛋白融合方式对该抗原进行修饰，并在大肠杆菌中表达融合蛋白(Trx-B_2)，纯化该蛋白后免疫小鼠及家兔，结果表明用硫氧还蛋白修饰后的融合蛋白免疫小鼠和家兔后，得到的抗体滴度均高于未经修饰过的复合多表位抗原合成肽所诱导的抗体滴度，并从免疫后的兔血清中提取IgG包被酶联板，利用双抗夹心法分别检测了32份HCV阳性血清和32份正常人的血清，结果阳性率分别为87.5%和43.75%，符合率为71.88%。

The worn surface of the sulfurized steel disc was observed with a scanning electron microscope, while the chemical states and phase structure of carbon-nitrided carbon steel and of the sulfurized one were examined by means of X-ray photoelectron spectroscopy and X-ray diffraction.

采用MPX-200型摩擦磨损试验机考察了碳氮共渗及室温电解硫化处理后的20#碳钢的摩擦学性能，探讨了在干摩擦条件下载荷、渗硫处理时间和滑动摩擦时间对渗硫层摩擦系数的影响。

The worn surface of the sulfurized steel disc was observed with a scanning electron microscope, while the chemical states and phase structure of carbon nitrided carbon steel and of the sulfurized one were examined by means of X ray photoelectron spectroscopy and X ray diffraction.

采用MPX-200型摩擦摩损试验机考察了碳氮共渗及室温电解硫化处理后20^#碳钢的摩擦学性能，探讨了在干摩擦条件下载荷、渗硫处理时间和滑动摩擦时间对渗硫层摩擦系数的影响。

Sulphurized-nitrided compound layer is prepared on the surface of drilling pipe joint material 35CrMo steel by the application of ion nitriding and ion sulfurizing technology.

中文摘要：应用离子渗氮与离子渗硫技术，在钻杆接头材料35CrMo钢表面制备了硫氮复合处理层。

The method of acidothioureation leaching (with 732 resin) for the extraction of gold from ore Containing Sulfurs and concentrate of gold was Studied.

本文报导了在硫酸酸性介质中以Fe~(3+)离子为氧化剂，用硫脲浸出，732型离子交换树脂吸附回收含硫金精矿中金的方法。

The results showed that the sulfur recovery ratio declined along with the increase of NH3 content.NH3 in acid gas should be burnt up to decompose into N2 and H2O in the burner of acid gas,or it would form crystalline of ammonium salt to obstruct the following equipments,even make production shut down.

结果表明，随着酸性气中氨含量的增加，硫回收率下降；酸性气中的氨必须在制硫燃烧炉中完全燃烧分解为N2和H2O，否则会形成铵盐结晶而堵塞下游设备，严重时将导致停产；根据酸性气中氨含量的不同，可选择不烧氨和烧氨2种工艺流程。

Based on discussion of industry environment of pyrite mine,sulfuric acid,phosphate fertilizer industry the position of enterprise strategy of pyrite mine enterprise was defined and new development was for the pyrite mine enterprises were put forward.

分析了硫铁矿企业所处的矿、酸、肥行业环境，明确了企业战略定位及发展方向，对我国硫铁矿企业的生存与发展提出了新的思路。

Summarize: XGN15-12 is a new metal-enclosed switchgear which whole air-insulated is assembly composed with SF6 loading switch as the main switch ,suitable for auto-electric-power distribution , both compacted and extensible metal-enclosed switch equipments.

XGN15-12型户内交流高压六氟化硫环网开关设备是新一代以六氟化硫负荷开关作为主开关而整柜采用空气绝缘的，适用于配电自动化的、既紧凑又可扩充的金属封闭开关设备。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。