硫

Species of metallic deposits are quite complicated: Besides commonly-seen pyrite ,chalcopyrite and bornite, there exist varied copper-bismuth sulfosalt minerals(sandber}erite, Bi-tennantite, Bi-tetrahedrite, aikinite, wittichenite),tungsten-tin sulfidesand polymetallic sulfides.

金属矿物种类复杂，除常见的黄铁矿、黄铜矿、斑铜矿外，还有多种铜铋硫盐矿物（锌砷黝铜矿、铋砷黝铜矿、铋锑黝铜矿、针硫铋铅矿、硫铋铜矿）、钨锡硫化物（硫铁锡铜矿、硫钨锡铜矿）及多金属硫化物。

ABSTRACT nine fitted with rumen fistula proximal duodenum and the Inner Mongolia Cashmere Goats Jieyang (about 2 years old) were randomly divided into 3 groups, respectively fed nitrogen and sulfur than the same sulfur different sources (for sulfur, sulfide sodium and sodium sulfate), three kinds of diet, digestion and metabolism test and determination of chyme liquidity to explore different inorganic sulfur and nitrogen and sulfur deposition of sulfur circulation.

选用9 只装有瘤胃和十二指肠近端瘘管的内蒙古白绒山羊羯羊(2 周岁左右)，随机分成3组，分别饲喂氮硫比相同而硫源不同(分别为硫磺、硫化钠和硫酸钠)的3 种日粮，进行消化代谢试验和测定食糜流通量，以探讨不同无机硫对氮和硫的沉积量以及硫的流通规律。

The external scale of cobalt sulfide and yttrium oxide-surfide particles in the inner scale were found respectively after corrasion in Pa .!$+ lo-'' Pa Q. Beneath the external scale, a region of internal sulfidation-oxidation of yttrium was also present. The comion pduct in lo-' Pa .!$+ 10-l5 Pa Q was only a very thin surface layer of yttrium oxysulfide and an internal oxidation zone of yttrium.

并有助于降低纯Co的腐蚀速率，10＾02Pa硫压下，合金表面形成的腐蚀产物为多层、以为硫化钴，中间层为由两金属化合物怕成分复杂的混合物层，最内层是由氧和硫引起的Y的内腐蚀区；在10＾－3Pa硫压下，合金没有形成外层硫钴，仅在表面形成较薄的Y的硫氧化物，其下为Y的内氧化区。

Diallyl trisulfide was synthesized with a yield of 76.4% based on sodium thiosulfate, allyl bromide and sodium sulfide. And diallyl tetrasulfide was synthesized by the reaction of sulfur monochloride with ally1 mercaptan with a yield of 81.0%.

以硫代硫酸钠、烯丙基澳和硫化钠为原料，合成了二烯丙基三硫，产率为76.4%；以一氯化硫和烯丙硫醇为原料合成了二烯丙基四硫，产率为81.0%。

The pyrolysis characteristics and sulfur release characteristics during coal pyrolysis of three different coals, which include high volatile, were studied by TG-GC-MS(Thermal gravimetry-Gas Chromatography-Mass spectrum), tube furnace of pyrolysis reactor and intelligent fixup sulfur equipment.

本文应用热重—质谱—色谱联用系统、管式炉热解反应器和快速智能定硫仪，研究三种高挥发分煤种的热解特性和热解硫析出特性，对热解硫析出的两种主要产物(H_2S和COS)进行了监测分析，得到硫的赋存形态、粒径大小以及矿物质对各种形态含硫气体析出的影响规律。

In this thesis, we used this principle coupled with flow injection solid phase reactor on-line oxidation, solid phase extract and dialysis separation technology to establish the on-line oxidizing fluorometric method for determination thioridazine hydrochloride and methotrexate in table and plasma samples, respectively.

第二章：研究报告一、流动注射在线氧化荧光法盐酸硫利达嗪分析体系研究流动注射在线氧化荧光法测定药物中盐酸硫利达嗪含量本方法根据盐酸硫利达嗪的氧化产物具有强荧光这一性质，在磷酸介质中利用二氧化铅固相反应器在线氧化盐酸硫利达嗪并通过乙醇对其的增敏作用，建立了流动注射在线氧化荧光法测定盐酸硫利达嗪含量的新方法。

According to the fluorescence measurement results from mixed solution, the association constant estimated for thioridazine hydrochloride-BSA binding and the number of the binding site with Scatchard analysis were 1.2×104 L/mol and 0.98, respectively.

将盐酸硫利达嗪与牛血清白蛋白以不同比例混合并在37 ℃下培养，以流动注射透析采样技术从混合液中分离出游离盐酸硫利达嗪，在线氧化为强荧光化合物后测定其浓度；应用Scrathard方程分析所测数据，求得盐酸硫利达嗪和牛血清白蛋白的结合常数为1.2×104 L/mol，结合位点数为0.98；根据热力学参数推断，盐酸硫利达嗪与牛血清白蛋白之间以疏水作用力为主；进一步基于荧光猝灭现象和Fster非辐射能量转移理论，得到盐酸硫利达嗪小分子与牛血清白蛋白之间的能量转移效率( E =0.497)和结合距离( r 0=3.27 nm)。

Rhodococcus erythropolis TJQ can use both organic and inorganic sulfur as vegetal sulfide. The strain growing with sodium sulfate can effectively desulfurize benzothiophene DBT and its derivatives 4,6-dimethyldibenzothiophene (4, 6-DMDBT).

实验结果表明，该菌既可以利用有机硫源又可以利用廉价的无机硫源作为生长硫源，以硫酸钠作为硫源培养的菌株可专一性脱除苯并噻吩和DBT及其甲基衍生物4，6-二甲基二苯并噻吩(4，6-DMDBT)中的硫。

During temperature-programmed combustion, the evolution sequence of different sulfur forms is aliphatic sulfur, aromatic sulfur and pyritic sulfur, thiophenic sulfur and sulfatic sulfur.

2大同煤各形态硫燃烧逸出的基本顺序为：脂肪硫，芳香硫和黄铁矿硫，噻吩硫和硫酸盐硫。

The results show that stable organic sulfur is the main s9lfur form in ZY coal. Pyrite can be removed under all the atmospheres in the tests, except for nitrogen at 500℃ 1% O2-N2 atmosphere has strong reactivity to remove the stable organic sulfur in ZY coal, especially at 700℃. Under 1% O2-N2 atmosphere, not only a part of stable organic sulfurs can be decomposed, but also more stable organic sulfur-containing structure can be broken down into less stable one.

结果表明，对于ZY煤而言，黄铁矿和不稳定有机硫除在氮气气氛下500℃时热解不能全部分解外，在其他条件下热解时都可以分解。1%氧气对ZY煤中稳定的有机硫的分解有很强的促进作用，不仅可以脱除稳定的有机硫，还可以使更稳定的有机硫断裂生成次稳定的有机硫，在随后的AP-TPR-MS实验过程中，这部分硫在较低的温度下逸出。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。