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N-substituded thioacridones with five different structures were synthesized via a route involving Ull-man reaction, cyclization, N-alkylation and sulfurization. The structures of each thioacridone were identified with IR and MS. The results from UV-spectrophotometry show that the five N-alkythioacridones all have stronger absorption in the visible light region.

采用乌尔曼反应、酸催化环化、N-烷基化和代化四步反应路线合成了5种不同结构的N-取代代吖啶酮,利用IR和MS分析手段表征了其结构,UV分光光度计的测定结果表明5种代吖啶酮在可见光区都有较强的吸收。

Studied influence of sulphonated naphthalene formaldehyde condensates, polycarboxylic series(SR3), aminosulfonic acid-based series on rheology of sulphoaluminate cement paste. Adjusted setting time with setting retarder, and reduced water dilution, bleeding, segregation of fresh paste with viscosity-modifying admixture.

研究了萘系、氨基磺酸盐系和聚羧酸系高效减水剂与铝酸盐水泥的相容性问题,利用缓凝剂有效控制了铝酸盐水泥的凝结时间,利用浆体稳定剂成功解决了水泥净浆的板结、泌水问题,从浆体流变学角度研究了外加剂—铝酸盐水泥浆体体系稳定性。

The our company after relates in every way according to the above situation, already from overseas massively purchased the ZX-10 series desulphurization catalyst, has been able to coke with this catalyst technology the sulphonium compounds which the triphenyl contained, the nitrogen compound , the unsaturated compound and very many impurities, the fetid odor and so on removes, after the processing triphenyl always Sulfur content was lower than the petroleum benzene, the smell, the color, was consistent with the petroleum benzene.

目前焦化三苯在工业上使用范围小,销售价格也低于石油三苯。其主要原因是、噻吩等杂质含量高、气味重。而现在国际、国内焦化三苯、汽油、柴油等产品脱提纯去杂质的工艺均采用高压催化加氢法处理,该工艺设备投资巨大。根据以上情况我公司经多方联系,现已从国外大量购进ZX-10系列脱催化剂,用本催化剂技术已能将焦化三苯所含的化合物、氮化合物、不饱和化合物及很多杂质,臭味等脱除,处理后的三苯总含量低于石油苯,气味、颜色,均与石油苯一致。

The redox separation conditions were investigated in detail. It was indicated that TBAPI exhibited appropriate oxidation intensity and well selectivity, thiolethers can be oxidized into sulphoxide, but it cannot oxidize thiols.

详细考察了氧化还原分离条件,实验结果表明,TBAPI具有适宜的氧化强度和良好的选择性,它能将氧化成亚砜,且在同条件下,对噻吩不起作用。

The derivatives of the amino acids containing sulphur synthesizedfrom three sulphydry amino acids such as methione, cysteine and cystine play an important role on the methylation,sulphuration, detoxication and ,antioxidation and are very useful in pharmaceutic and food industry.

氨基酸衍生物主要由三个常见的含氨基酸——蛋氨酸,半胱氨酸,胱氨酸衍生转化而来,可以在体内参与转甲基,转基等生化过程,同时也具有抗氧化,清除自由基等功能,在医药和食品中具有重要的应用价值。

Ion nitriding+ion sulphurization duplex treatment can extend significantly the endurance life of sulphide layer, and improve very obviously the anti-scuffing behavior of surface at any speed.

喷丸处理在表面形成的大量缺陷促进了渗过程中向基体内部的扩渗,从而增加了渗层的厚度。

Based on the research results, the shot peening+ion sulphurization and ion nitriding+ion sulphurization duplex treatments were used to treat the steel surfaces, the effect of sulphide layer could be further developed.

依据研究结果,对钢铁表面进行喷丸+离子渗、离子渗氮+离子渗复合处理,以进一步发挥渗层的作用。

So the difficult sequence of cracking to remove the sulfur for different sulfur compounds is that thiophene, benzothiophene>alkyl side-chains of thiophenic compounds>mercaptan, sulfur ether.

总之,不同含化合物裂化脱的难度顺序为:噻吩、苯并噻吩>烷基噻吩>醇、醚。

On the condition of the existence of the buffer solution of ammonium acetate (PH5-6) and ammonium thiocyanate, quantitatively reduce Cu2+ into Cu+ by using sodium thiosulphate .

本文在PH5-6的乙酸铵缓冲溶液及氰酸铵存在下,用酸钠定量还原Cu~(2+)为Cu~+,Cu~+与SCN~-结合,形成稳定的氰酸亚铜白色沉淀,反应终点可由全自动电位滴定仪确定。

The chemical deposition method was applied to prepare bismuth sulfide through reaction of bismuth salt complexed by triethanolamine or EDTA with an aqueous solution containing a sulfur sourse such as thioacetamide, thiourea, sodium thiosulphate, geseous H2S.

化学淀积方法被提出申请准备化铋经过被和一个水溶液的三乙醇胺或乙二胺四醋酸合成物的铋盐反作用含有 sourse,像是代乙醯胺,,钠 thiosulphate , geseous H2S 。

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