硫

The sodium dithiobenzoic acid was oxidized with potassium ferricyanide to obtain di disulfide.The influences of raw materials mole ratio,stirring method and reaction time on the yield were studied with orthogonal test.

用铁氰化钾溶液氧化二硫代苯甲酸钠，得双二硫代苯甲酰，采用正交实验探讨了4，4'-偶氮双(4-氰基戊酸)与双二硫代苯甲酰反应的投料比、搅拌方式、反应时间对反应收率的影响。

Subcordiformis in Huanghai Sea near Dalian, it can be able to evolve H〓 photosynthetically. Comparing with Chlamydomonas reinhardtii in our lab, the H〓 productivity is same. By the elementary macro regulation of H〓 production with 2, 5-dibromo-3-methyl-6-isopropyl-p-benzoquinone , N, N'-dicyclohexylcarbodiimide , 3-(3, 4-dichlorophenyl)-1, 1-dimethylurea , sodium dithionate, sulfur-deprivation and cell immobilization, the results show that DCCD, immobilization and sulfur-deprivation has a positive effects on the H〓 production.

利用DCCD（质子泵抑制剂N，N'-dicyclohexylcarbodiimide）、DBMIB（光合电子传递抑制剂2，5-dibromo-3-methyl-6-isopropyl-p-benzoquinone）、DCMU[PSⅡ光合放氧抑制剂3-（3，4-dichlorophenyl）-1，1-dimethylurea]、连二亚硫酸钠、无硫调控及固定化扁藻等手段，对该扁藻产氢进行初步的宏观调控，发现DCCD的加入、扁藻的固定化和无硫调控对产氢均有正效应，其中无硫调控使扁藻产氢时间延长，总产氢量提高了近10倍。

The diffusion of ethanethiol in MFI and MOR was investigated by Molecular Dynamics.

采用分子动力学方法模拟计算了乙硫醇分子在MFI和MOR两种拓扑结构沸石中的动力学性质，比较了乙硫醇不同负载量和沸石晶格原子刚性和柔性两种状态下乙硫醇分子在沸石孔道中扩散系数的大小。

Adsorption kinetics of ethanethiol and thiophene on 13X molecular sieves loaded with Ag+ was investigated in static state system.

在成品油中的硫主要是硫醇、硫醚、二硫化物和唾吩等有机硫化物。

For the product 〓, the signal for n=2 is much smaller than that for n=1, which may due to the large steric hindrance by the ethanethiol ligands.

其原因很可能是乙硫醇分子体积比较大，所以金属离子结合第二个乙硫醇时，就有很大的空间位阻，以致比结合第一个乙硫醇要难得多，结果n=1～2之间出现明显的强度突变。

Study on removal rate of methyl mercaptan and ethanethiol by bio-trickling filter;2. The deodorizing effect of tea functional ingredients on methyl mercaptan (CH3SH) was studied in this investigation.

就茶叶功能成份对主要恶臭成分甲硫醇的去除效果进行了研究，结果表明：绿茶水提取物，儿茶素，EGCG对甲硫醇的去除效果不明显，而茶黄素则表现出较强的活性；在pH10的碱性条件下，1mg含量为40%的茶黄素对甲硫醇的最大去除量为0。

The topology models of MFIand MOR were built and the method of Configurational-bias Monte Carlosimulation was used for investigating the adsorption and distributions of ethanethiolas adsorbate in MFI and MOR type zeolites. The diffusion of ethanethiol in MFI andMOR type zeolites was studied by molecular dynamics simulation.The results show, the concentration of Zn2+ is the most important factor of theloading quantity of zeolite 13X and alumina, and the temperature secondly. The pHvalue which range from 2 to 3 effects on the loading quantity faintly.

构建了MFI 和 MOR 两种拓扑结构沸石的数学模型，以乙硫醇分子作为被吸附的目标物，采用偏倚蒙特卡罗方法模拟乙硫醇在MFI和MOR沸石上的吸附行为及分子分布密度，并利用分子动力学模拟乙硫醇在这两种拓扑结构的扩散行为，为实现面向硫化物进行吸附剂的微观结构设计作初步探索。

Bunte salt was first prepared by α-furfuryl chloride and sodium thiosulfate. Then under the reaction of Bunte salt with 2-methyl-3-furanthiol in the presence of sodium hydroxide, furfuryl 2-methyl-3-furyl disulfide was prepared.

首先以α-糠基氯和硫代硫酸钠反应制备Bunte盐，然后Bunte盐与2-甲基－3-呋喃硫醇在碱性条件下反应合成了产品糠基2-甲基－3-呋喃基二硫醚。

This method can be used to detect 16 pesticides in 30 minutes, including organophosphorus (parathion-methyl, phorate, isofenphos-methyl, malathion, chlorpyrifos, fenthion), organochlorine (dichlororos, heptachlor, chlorothalonil,α-hexachlorocyclohexane,γ-hexachlorocyclohexane,δ-hexachlorocyclohexane, p, p'-DDE, p, p'-DDD), pyrethroids and triadimefon in vegetables.

采用选择离子－气相色谱－质谱联用方式，依据保留时间和特征离子丰度比，可以在30 min之内检测有机磷（甲基对硫磷、甲拌磷、甲基异柳磷、马拉硫磷、毒死蜱、倍硫磷）、有机氯（敌敌畏、七氯、百菌清、α-六六六、γ-六六六、δ-六六六、p， p'-DDE、p， p'-DDD）、除虫菊酯、三唑酮等16种农药。

The charge transfer salts with second order nonlinear optical properties have been synthesized based on hexamethylenamine and the heteropoly acids,H 3PMo 12 O 40 ·nH 2O,H 4SiMo 12 O 40 ·nH 2O and H 4GeMo 12 O 40 ·nH 2O and characterized by elemental analysis,IR spectra and UV spectra.

本文研究了一系列不同富硫有机配体的配合物以及富硫有机分子修饰的硫化物；合成了两个系列的7个富硫配合物和2个电荷转移盐，运用元素分析、红外、紫外-可见光谱对配合物进行了表征，并且通过单晶四圆X-衍射测定了C_5H_6S_5CuI(1)、(C_5H_6S_5)2PdI_2(6)、C_(10H_(10)S_8[(C_4H_4S_4)AuCl_2](8)、C_(10H_(10)S_8Hg_2Cl_6(9)四个化合物的晶体结构。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。