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Second, aminolysis of polystyrene and poly prepared by reversible addition-fragmentation chain transfer polymerization was investigated. The product of the former contains predominantly double molecular weight species by the formation of disulfide bond, whereas the latter formed coupled species which consequently cleaved to unimolecular weight species.

由RAFT聚合的机理可知,聚合最终得到的聚合物的结构包含双酯基团,它是聚合物链保持活性特征的重要体现,同时它为聚合物的端基官能化提供了一个重要的途径,其中氨解反应是一个被人们广泛采用的方法,它在很温和的条件下将端基去掉,同时还能将双酯端基变成醇端基。

The experimental result shows that sulfuring rate from coke to hot metal reduces with witherite and CaCl2 addition in coke making, but the sulfuring rate increased with lime stone.

结果表明,在实验条件下,加入毒重石和CaCl2的焦炭能降低焦炭向铁水渗率,减少进入铁水中的含量;而加入石灰石的焦炭中进入铁水中含量较多。

A new catalytic kinetic spectrophotometric method for the indirect determination of trace sulfide has been studied. The method was based on the inhibition of sulfide on the iron catalyzed oxidation of xylenol orange by hydrogen peroxide in NH3 medium.

在氨水介质中,离子可阻抑Fe催化过氧化氢氧化二甲酚橙褪色,并且催化体系和阻抑体系在570nm处吸光度的差值与离子浓度呈线性关系,据此建立了阻抑动力学光度法间接测定痕量离子的新方法。

Process of flotation of acture ore is the following: firstly, adding Na_2CO_3, ZnSO_4, CSU-1 to the pulp while grinding, and thus in this condition of low Eh, marmatite is inhibited; Secondly, adding CSU-1 to the pulp out of grinding machine, then amesonite and iron sulfur mineral can be flotated using diethyldithiocarbamate as collector; High quality lead and antimony concentrate can be got by adding CSU-1 and calcareousness; Lastly, marmatite is flotated by adding calcareousness, CuSO_4, xanthe, and D-250 to get zinc concentrate.

小型试验研究表明,首先在脱粗选作业只加入适量的Na_2CO_3、ZnSOO_4、和CSU-1至磨矿机,利用磨矿机的研磨和磨机中的低电位环境,使铁闪锌矿受到抑制,而最容易浮的脆锑铅矿和黄铁矿、磁黄铁矿等化矿物则依然具有可浮性;在磨机出来的矿浆中分别加入CSU-1进一步抑制易浮的铁闪锌矿,然后加入乙氮将脆锑铅矿和化铁矿快速浮净,加入石灰和CSU-1,浮选分离出高质量的铅锑精矿;接着添加石灰、CuSO_4、黄药及2~#油选别铁闪锌矿。

Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamides(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,与氰酸钾反应生成α-萘乙酰基异氰酸酯,再与芳基酰肼进行加成反应,合成8种新型N,N′-萘乙酰基取代芳乙酰胺基脲类化合物(Ⅱ1~Ⅱ8)。

Occurring commonly in lead-zinc pyrite orebodies and near-ore skarn, it is associated with spessartine, pyrite and alabandite.

在对辽宁建昌县八家子矿区吴家屯铅锌黄铁矿-锰矿矿床进行研究的过程中,首次发现三斜锰辉石,它与锰铝榴石、锰矿、黄铁矿等共生,主要产出在铅锌黄铁矿体、锰矿体和近矿矽卡岩中。

Similar to S-adenosylmethionine decarboxylase(B26),S-adenosylmethionine methyl-transferase(B70), allene oxide synthase(B38),ethylene receptor(B96),cytochrome P450(B58) and methionine synthase (B77) were found in ovaries of Pingyi Tiancha at 1d before the blossom day,which related to plant hormone and could participate in metabolic pathways of ethylene,polyamine,jasmonate acid and gibberellin,et al.,as well as had close relationship with maturity and senescence of plants.

在平邑甜茶开花前1d的子房中发现的S-腺苷甲氨酸脱羧酶(B26)、S-腺苷甲氨酸甲基转移酶(B70)、丙二烯氧化合酶(B38)、乙烯受体(B96)、细胞色素P450酶(B58)、甲氨酸合酶(B77)等相似基因片段与植物体内的生长素有关,将会参与乙烯、多胺、茉莉酸、赤霉素等的代谢途径,与植物的成熟和衰老具有密切的关系。

The quality and inhibition efficiency of thiourea, allylthiourea and phenylthiourea self-assembled films were studied by electrochemical impedance spectroscopy and polarization curves, respectively.

利用电化学阻抗谱和极化曲线研究了脲、烯丙基脲、苯基脲在金属铜表面上的自组装膜的质量和缓蚀效率,并通过量子化学计算进一步研究了各种分子和金属铜的相互作用。

These coordination compounds mostly have group ⅡB metals as center ions. The complexes are classified with ligand as three types: thiourea type, allylthiourea type and thiosemicarbazone type.

这类配合物大都以ⅡB族金属为中心离子,根据配体不同可分为脲类、烯丙基脲类及缩胺基脲类3种类型。

Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a~3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a~7c) in the presence of triethyl phosphite.The compounds 7a~7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中,在亚磷酸三乙酯存在下,采取高度稀释的方法,使4,5-二氰基-1,3-二杂环戊二烯-2-酮分别和多缩杂冠醚进行交叉偶联反应,成功地得到了不对称的2,3-二氰基四富瓦烯衍生物。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。