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An effective procedure for the production of chromium yellow with nitric acid hydrolysis solution of Galena was studied.

应用方铅矿的硝酸酸解液可生产出多种铅产品,其中合成铅铬黄是比较便捷的一种。

First of all, this study will be multi-walled carbon nanotubes by chemical oxidation process purified so it can be modified to deal with than the purification of purity before the modified 5 wt%, more than 1.89 times the surface area to increase the surface potential decrease of about 10 ~ 20 mV and the surface functional base (-COOH and-OH) to increase 1.45 times, and then the control technology of electroless preparation parameters include: analysis of plating time, plating analysis of temperature, metal ions in solution than the (Fe2+/ Ni2+), bath pH and the added value of dispersion Agent and other research towards Fe-Ni particles to increase the iron content and Fe-Ni particles spread in the MWCNT upper fixed targets,the results found that when the parameters for the preparation of 50 ℃, pH10, do not add dispersant, metal ions than the solution (Fe2 +/ Ni2 +) 7, the highest iron content can be Fe = 40.55 at%(flat iron content 111.17 mg / g) of nanocomposites Fe-Ni/CNT, then for a series of the nature of its analysis, the final evaluation Fe-Ni/CNT nanocomposites were processed on the effectiveness of the application of mixed pollutants, the results showed that in 120 minutes at the same time when Adsorption of heavy metal ions lead nitrate 10 ppm, selenium heavy metal ion degradation of 1 ppm and orange azo dye AO7 50 ppm standard of effluents, and after a total Fe-Ni nano-particles to SEM / EDS analysis of more than 50% still remaining.

本研究首先将多壁奈米碳管以化学氧化法做纯化改质处理能使其纯度较纯化改质前提高5 wt%、比表面积提高1.89倍、表面电位下降约10~20 mV以及表面官能基提高1.45倍,再控制无电镀技术之制备参数包括:析镀时间、析镀温度,镀液中金属离子比(Fe2+/Ni2+)、镀液pH值及是否添加分散剂等,研究朝提高Fe-Ni粒子的含铁量与Fe-Ni粒子散布固定在MWCNT上等目标进行,研究结果发现当制备参数为50 ℃、pH10、不添加分散剂、镀液金属离子比(Fe2+/Ni2+)7时,可得到最高铁含量Fe = 40.55 at%(单位铁含量111.17 mg/g)之奈米复合材料Fe-Ni/CNT,接著对其作一系列性质分析,最后评估奈米复合材料Fe-Ni/CNT对共处理混合污染物之应用效益,结果显示其在120分钟时能够同时吸附重金属硝酸铅离子10 ppm、重金属硒酸根离子1 ppm及降解偶氮橘色染料AO7 50 ppm达放流水标准,且共处理后奈米Fe-Ni粒子以SEM/EDS分析仍剩余50 %以上。

On the 10th ,20th ,30th,40th and 50th day, cut the tail of each mouse to make blood smears, stained the smears by Wrights method, and counted the erythrocyte containing HowellJolly bodies, or containing basophilic stipplings, or showing polychromatophilia, or showing hypochromic.

昆明种成年雄性小鼠15只,随机分成两组,实验组10只饮用2g/L硝酸铅溶液(1251mgPb2+/L)染毒,共50d。每10d切尾涂片一次,分别镜检计数含HowellJolly小体RBC,嗜碱性点彩RBC,嗜多色性RBC及低色素性RBC的出现率。

Lead, arsenic, stibium and bismuth were determined by inductively coupled plasma atomic emission spectrometry in hydrochloric acid medium.

铜精矿经硝酸缓慢溶解,在氨性溶液中,以氢氧化铁和氢氧化镧作载体一次共沉淀铅、砷、锑和铋,并与铜等元素分离,在盐酸介质中用电感耦合等离子体原子发射光谱法测定铜精矿中的铅、砷、锑、铋杂质元素。

Products available:strontium chloride,strontium nitrate,high purity strontium carbonate,strontium hydroxide,strENDS UNION ENTERPRISE LTD.

提供产品:氯化锶,硝酸锶,高纯碳酸锶,氢氧化锶,半水醋酸锶,高纯氯化钡,氢氧化钡,高纯碳酸钡,醋酸钡,氯化锰,硝酸锰,醋酸锰,碱式碳酸铅,硫磺。

Lead zirconate titanatenanopowder with a composition in the vicinty of morphotropic phase boundary (Zr/Ti=52/48) is prepared by optimizing the technology process of chemical coprecipitation method .

以四氯化钛、硝酸铅、氧氯化锆等为原料,采用化学共沉淀技术,通过优化工艺条件制备了组成在准同型相界点附近的钙钛矿相PZT纳米粉。

It is found that the concentration of nitric acid has great effect on reclaiming rate of lead in the processing of nitric acid leaching-lead deposition after investigating the preparation of tribasic lead sulphate from bismuth waste residue by ammonium hydrogen carbonate transformation method.

通过对铋冶炼浸渣采用碳酸氢铵转化法合成三碱式硫酸铅的工艺研究,得出在硝酸浸出—硫酸沉铅工艺过程中影响铅回收率的主要因素为硝酸质量浓度。

The processing principle for the preparation of tribasic lead sulphate from bismuth hydrometallurgy waste residue by ammonium hydrogen carbonate transformation-nitric acid leaching-lead deposition with sulphuric acid-sodium hydroxide synthesis is introduced.

介绍了铋冶炼浸渣采用碳酸氢铵转化—硝酸浸出—硫酸沉铅—氢氧化钠反应合成三碱式硫酸铅的工艺原理。

The research used microwave power 600W,and S/L is 1/10, with the suitable microwave operation condition (nitric acid concentration 9.0 mole/L, digesting time 8 minute, and digesting temperature 140 ℃), by microwave digestion lead leaching rate is 94.11%, if it used microwave power 600W,and S/L is 1/10, with the best microwave operation condition (nitric acid concentration 0.8 mole/L, digesting time 6 minute, and digesting temperature 120 ℃), by the result of study, after Microwave Digestion Treatment, the TCLP leachate of lead in reaction ash might could be reduce to 4.83 mg/L from 7.10 mg/L, and the TCLP leachate could keep under the regulation control standards.

本研究以微波功率600W、固液比1/10,在最适微波条件下(硝酸浓度9.0M、消化时间8分钟、消化温度140℃),铅的微波消化溶出率为94.11%。在微波功率600W、固液比1/10,以微波最佳条件(硝酸浓度0.8M、消化温度120℃、消化时间6分钟),经微波消化处理后,其铅TCLP 溶出量由7.10 mg/L降为4.83 mg/L,已能符合法规管制标准值。在此最佳微波条件下,对於铅TCLP 削

I plant perennial supply of chemical plating material: nickel sulphate, chloride nickel, nickel nitrate, ammonium chloride, sodium hypophosphite, sodium citrate, ammonium citrate, potassium citrate, chromium oxide, red Lead oxide, palladium chloride, SnCl2, crystal tin tetrachloride, the resistance of fuse, lithium fluoride, sulfuric acid cadmium, Na2HPO4, bismuth chloride, bismuth oxide, oxide Thallium sulfate Cobalt, cobalt nitrate, cobalt chloride, barium hydroxide, calcium hydroxide, fine chemical products.

我厂常年供应化学镀材料:硫酸镍、氯化镍、硝酸镍、氯化铵、次亚磷酸钠、柠檬酸三钠、柠檬酸三铵、柠檬酸钾、三氧化铬、红色氧化铅、氯化钯、氯化亚锡、结晶四氯化锡、电阻熔断剂、氟化锂、硫酸镉、磷酸氢二钠、氯化铋、三氧化二铋、三氧化二铊、硫酸钴、硝酸钴、氯化钴、氢氧化钡、氢氧化钙等精细化工产品。

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