硝氨基

The synthesis method comprises the following steps: adding 2-( 5-(dimethylamino methyl- 2- furyl methyl sulpho ethylamine and 1- methylthio- 1- methylamino- 2- nitro ethylene with a molar ratio of 1.04: 1 into water, heating to 48- 52 Deg. C, reacting 4.5 hours with a vacuum degree of 0.02- 0.05 MPa, cooling, adding sodium-hydroxide of concentration of 10% to regulate the PH value to 11.0- 11.4, filtrating and cooling the filtrate to 0- 2 Deg. C, crystallizing for 12 hours, centrifugally filtrating, and rinsing filter cake with purity water to prepare wet ranitidine alkali; dissolving ranitidine alkali in alcohol and reacting with chlorhydric acid to prepare ranitidine hydrochloride.

合成方法包括：将摩尔比为1.04∶1的2-(5-(二甲氨基甲基-2-呋喃基甲基硫代乙胺与1-甲硫基-1-甲胺基-2-硝基乙烯加入水中，升温至48-52℃，于真空度0.02～0.05MPa反应4.5小时，反应完毕降温，用10％氢氧化钠溶液调pH＝11.0-11.4，抽滤，滤液降温至0～2℃，结晶12小时，离心甩滤，用纯化水漂洗滤饼，得雷尼替丁碱湿品；将雷尼替丁碱溶于乙醇中与盐酸反应，制备得到盐酸雷尼替丁，产品符合欧洲药典标准。

With the catalyst TiO2/SO(superscript 2- subscript 4), 2, 4, N-trinitroanilinoacetic acid was synthesized from chlorobenzene and glycine with yield of 71.6%.

以纳米固体酸TiO2/SO(上标 2-下标 4)为催化剂，氯苯和氨基乙酸为原料直接合成了2，4，N-三硝基苯胺基乙酸，收率为71.6%。

Objective To evaluate relationship between urine NAG isoenzyme and acute cerebrovascular disease. Methods The activity of urine NAG isoenzyme, NAG/Cr and blood NAG isoenzyme in 47 patients with acute CVD (15 patients with brain hemorrhage and 32 patients with brain infarction) were examined by p-nitrobenzene chronometry.

目的 探讨尿液N-乙酰-β-D-氨基葡萄糖苷同工酶与急性脑血管病的关系方法采用对硝基酚比色法，分别测定了47例急性脑血管疾病患者（其中脑出血15例，脑梗死32例）的尿液NAG同工酶谱、尿NAG与尿肌酐的比值、血清NAG活力。

The UV-Vis absorption spectra, steady-state fluorescence spectra and the fluorescence decay curve of 4--4′--azobenzene in chloroform solution were measured.

采用紫外可见吸收、稳态荧光光谱和荧光衰减测量技术，观察了4-硝基-4′-氨基偶氮苯在氯仿溶液中的光致变色现象及分子的跃迁能级和能级寿命。

Dinitrophenol, Wetted with not less than 20% water, by mass

2-氨基-4，6-硝基苯酚，湿的，按质量含有不少於20%的水 2-Amino-4， 3317

That is to say it has some advantages of fast burning velocity, more gases products, lower burning temperature, little solid draff, low toxicity.

研究发现，3-硝基-1，2，4-三唑-5-酮氨基胍具有良好的产气性质，表现为燃烧速度较快、产气量较大、燃烧温度低、固体残渣少、所释放的气体毒性小等优点，而且它还具有较低的感度和较好的热稳定性。

Here we found the optimum situation to determine LAP: the concentration of Tris-HCl is 125 mmol L^(-1) and the optimum pH is 7.2, temperature is 37℃, under this condition, Michaelis constant is 0.15 mmolL^(-1), ground substance concentration is 6.0 mmol L^(-1), with 157 health people serum samples (81 from male, 76 from female),x± s=35.7 UL^(-1)±8.2 UL^(-1), we established the method and reference value for clinical application and automatic analysis.

测定亮氨酰氨基肽酶的最适条件：选用浓度为125mmolL^(-1)的Tris-Hcl缓冲液，最适pH为7.2，温度取37℃，得出在此实验条件下的米氏常数Km为0.15mmolL^(1)，亮氨酰对硝基苯胺浓度取6.0mmolL^(-1)，取健康体检者血清157例（男81例，女76例），测得x±s为35.7UL^(-1)+8.2UL^(-1)，建立了适合于临床应用及有动生化分析仪的方法和参考值。

The standard molar special heat capacity of 1,1-diamino-2,2-dinitroethylene (FOX-7) was determined with two continuous Cp modes of a mircocalorimeter to be 176.56 and 176.02 J·mol－1·K－1 at 298.15 K, respectively.

应用Micro-DSCⅢ微热量仪的两种连续比热容测定模式对1，1-二氨基-2，2-二硝基乙烯(FOX-7)比热容进行了测定。

A new spectrophotometric method for the determination of chromium has been developed. In HCl medium, the chromium oxidizes hydroxylammonium chloride to form nitrite, which produces a pink azo dye when reacting with p-aminobenzene sulfonic acid and α-naphthylamine.

基于铬在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根，而亚硝酸根与对氨基苯磺酸重氮化后可与α-萘胺偶联产生粉红色偶氮染料，提出了分光光度法测定铬的新方法。

With the occurrence of H2/Pd-C and ethyl formic ester,the reduction of the nitro group and the formylation of the amino group could be finished in one step.

但是在甲酸乙酯存在下，用H2/Pd-C对Ⅶ的硝基进行还原，得到的Ⅷ中的氨基可当即被甲酰化，使由Ⅶ到Ⅳ的两步反应一步完成。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。