硝化的

We focused the study on the synthesis methods of quinoxaline, nitration of its aromatic ring and chlorination of its heterocycle. In this paper, we thought about environmental protection, the cost of material, the feasibility of industrialization, workup easily, and obtained 2,3(1H,4H)-quinoxalinedion, 6-nitro-2,3(1H,4H)-quinoxalinedion, 6,7-dinitro-2,3(1H,4H)–quinoxalinedion, 2,3-dichlo- roquinoxaline, 6–nitro-2,3-dichloroquinoxaline,and 6,7- initro-2,3-dichloro-quinoxaline. A more reasonable, easily, efficient and simple reactive route to synthesize above-mentioned compounds was developed by systematically investigating the yield, the purity and physical character of intermediates.

本文针对喹喔啉及其芳环硝化、杂环氯代的合成进行研究，主要考虑了环保性、原料成本、产业化的可行性、反应操作的简便性等问题，获得了2，3(1H，4H)-喹喔啉二酮、6-硝基-2，3(1H，4H)-喹喔啉二酮、6，7-二硝基-2，3(1H，4H)-喹喔啉二酮、2，3-二氯喹喔啉、6-硝基-2，3-二氯喹喔啉和6，7-二硝基-2，3-二氯喹喔啉等六个中间体，考察了反应产物的产率、纯度和性状等因素，得到了更为合理、方便、实用、简洁的可供产业化的合成路线。

Exploratory study was made on the Guanting reservoir influent treatment by using two-stage BAF at extreme low temperature.The results show that the removal of organics and ammonia nitrogen is seriously inhibited due to low temperature,and the conversion of nitrite into nitrate is no longer a limiting factor of complete nitrification.One possible hypothesis is that the activity of nitrobacter is hi gher than that of nitrosomonas at extreme low temperature.

摘 要：两级曝气生物滤池在极低温度下(1℃以下)处理官厅水库入库水的探索性研究试验结果表明，有机物和氨氮的去除受到了低温的严重抑制，亚硝酸盐转化成硝酸盐不再是完全硝化反应的限制步骤，这可能是在极低温度条件下硝酸菌的活性高于亚硝酸菌活性的缘故。

In addition,α-alkenoyl ketene--acetals mainly used as the synthons of 3C and 5C, theα-functionalized reactions of which just limited on some simple reactions, as bromination, nitration, acetylation. However, the understanding of the forming of C-C bond atα-position is far from enough.

另外，对于α-烯酰基二硫缩烯酮的研究则主要集中在其作为3C或5C合成子的研究上，其α-位的官能化研究只是停留在溴化、硝化、脱羧等简单的反应之上，而对α-位C-C键的形成还缺乏足够的认识。

In this dissertation, I will represent my studies on the nitration of Chalcone derivatives, reaction of epoxide ketone, and the aromatization of 3,5-disubstitued 2-isoxazolines with nitric oxide.

本文主要研究了：(1)NO与查尔酮及其衍生物的硝化反应，反应以较高的产率得到了a-硝基化合物；(2)NO对环氧酮的开环反应，反应生成了顺式羟基硝酸酯；(3)3，5-二取代的-2-异恶唑啉在NO作用下可以发生芳环化反应，生成了对应的2-异恶唑化合物。

O-MNT、 p-MNT and m-MNT are got by mononitrating toluene, and the quantity of p-MNT and m-MNT that are needed is increased greatly, there is a great economic benefit to improve their ratioes , so the objective of this study is to improve the ratioes of p-MNT and m-MNT in the mononitration of toluene respectively through changing temperature and mixed acid composition in industrial way.

甲苯一硝化生成邻硝基甲苯、对硝基甲苯、间硝基甲苯，其中对硝基甲苯和间硝基甲苯的用量明显增加，提高它们在产物中比例的研究，具有十分可观的经济价值，所以本文从工业化的角度出发，通过改变温度和硝硫混酸的组成，分别对提高一硝基甲苯中对、间位异构体的比例进行研究。

The RE of TP, COD and turbidity except NH4+-N in the aeration process by adding AS and PAM for enhanced chemical phosphorus removal increased by 7.3~59.2%, 5.0~20.3% and 10.9~34.7%, respectively. Given enough dissolved oxygen, the nitrification was not affected by adding AS and PAM in the dosage range of the study. The RE of TP, COD and turbidity by postpose coagulation were better than by simultaneous coagulation, however, coagulation and sedimentation equipments were needed in postpose coagulation process. Therefore simultaneous coagulation was more suitable for transformation of AB process for chemically enhanced phosphorus removal.

曝气过程中投加AS和PAM复配化学强化除磷，总磷、COD、浊度去除率分别提高了7.3～59.2%、5.0～20.3%、10.9～34.7%，但不能提高氨氮的去除率；在溶解氧足够时，本研究投加量范围的AS和PAM的加入对硝化作用无影响；后置混凝对TP、COD、浊度的去除效果优于同步混凝，但需增加混凝沉淀设备，因此同步混凝更适合于于AB工艺的化学强化除磷改造。

About 74.6% of soluble organic substance was degraded in the lower 40 cm of media, while most ammonia was nitrified in the upper media.

生物量和生物活性的大小对污染物的沿程去除率影响较大，74.6%的有机物在进水端40cm厚的填料层内得到降解，而氨氮（NH+4-N）的硝化集中在上层填料层内。

The use of the phosphorus uptake and denltrification of PAOs under anoxic conditions for the realization of the simultaneous removal of nltrogen and phosphorus is a method with practical prospect for munic－ipal sewage treatment,and the establishment of the mathematical models of denitrlfication and dephosphorization by activated-sludge process benefits the popularization and application of this technofogy.

利用聚磷菌在缺氧条件下的吸磷和反硝化作用，实现氮、磷的同时去除，是具有实用前景的城市污水处理方法，而建立活性污泥法脱氮、除磷的数学模型则有利于该项技术的推广应用。

Bromo-5-formyl -3-methylpyrrole is an important intermediate of tolyporohin. On the base of introducing the present research and development of tolypo- rohin and pyrroles ramification at home and abroad, an emphasis was made on synthesis of 2-Bromo-5-formyl -3-methylpyrrole and the technical conditions of all steps, which was described as follows. Diethyl 3,5-dimethylpyrrole-2,4-dicarboxylate was made by nitrification, reduction and cycle of ethyl acetoacetate.

由于2-溴-5-甲酰基-3-甲基吡咯是合成托尼卟吩的重要中间体，本文在阐述了当前托尼卟吩及吡咯衍生物的国内外研究和开发的基础上，重点研究了2-溴-5-甲酰基-3-甲基吡咯的合成，并对各步反应进行了工艺研究，具体合成步骤如下：本文通过对乙酰乙酸乙酯的亚硝化、还原、成环，反应生成吡咯单环衍生物2，4-二乙氧羰基-3，5-二甲基吡咯。

With the increase of establishment years, most of plant communities on the grasslands showed a "V" type change trend in their quantities, i.e., high-low-high, hut the forbs biomass had a "Λ" type change trend and the sedge biomass increased gradually. Soil nutrients presented a "V" type hut soil hulk density presented a "Λ" type change trend, bile soil pH presented a decreasing trend. Most of soil microbial physiological groups and microbial biomass carbon showed a "V" type change trend, phosphorus-dissolving bacteria showed a "Λ" type change trend, denitrifying bacteria decreased gradually, while cellulose-decomposing bacteria showed an increasing trend.

结果表明：随着人工草地建植年限的增加，植物群落的数量特征多呈高－低－高、杂类草生物量低－高－底、莎草生物量增加的趋势；土壤养分变化为高－低－高、容重为低－高－底、pH呈下降趋势；土壤中多数微生物的数量及微生物生物量碳含量的变化为高－低－高，纤维素分解菌数量逐渐升高，而反硝化菌数量逐年下降，溶磷菌数量呈低－高－低的动态变化。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。