硅酸化

Study on continuous production of silica by hypergravity sulfuric acid precipitation method was conducted.

对超重力硫酸沉淀法生产白炭黑进行了连续化实验研究，通过改变硫酸的质量分数、旋转床转子的转速和硅酸钠的流量，探索出了这些工艺条件对白炭黑粉体性能的影响。

The influence of phosphorous slag on the setting time of Portland cement and improvement by some additives such as sodium sulphate,calcined gypsum and calcined alunite and synthesized additive were studied.

磷渣是电炉制取黄磷工业的一种工业废渣，在用电炉法制取黄磷时，所得到的以硅酸钙为主要成分的熔融物，经淬冷为粒化电炉磷渣，简称磷渣[1，2]。

Arsenic containing wastewater from gallium arsenide production was treated by coagulation process using self made polyferric metasilicate.

用自制的聚合硅酸铁对砷化镓生产中的含砷废水进行混凝处理。

The paper discusses the process conditions of producing synthetic cryolite by carbonation method and the main factors affecting the yield rate of sodium fluosilicate.

本文探讨了碳酸化法合成冰晶石的工艺条件，确定了影响氟硅酸钠纯碱分解率的主要因素，试验结果表明：NaF溶液的精制和〔6F-〕/〔Al〕、反应温度等对冰晶石性能有显著的影响。

In the aspects of research method, we took the method of preparing sol at first and then impregnating the wood to obtain ceramic-wood composite; this method made the wood use efficiently and increased the wood's weight gain percent. The ceramic-wood composite with performances of well decay resistance, dimensional stability, effloresce resistance and high strength was obtained by importing the cymene to the net of gel as the result of co-hydroxylation between MTES and TEOS. Making use of XPS ,we found that the apex of Si2p、O1s、C1s had evident chemical shift , which validated the existence of Si-O-C bonding.Key Words: Sol-gel, Ceramic-wood composite, Modified sol, Ecomaterials

在工艺方法上，采用先制备溶胶，然后浸注木材的工艺方法具有原料利用率高、提高增重率的优点；采用甲基三乙氧基硅烷和正硅酸乙酯共水解的方法，将甲基引入陶瓷化复合木材的凝胶内部，所制备的材料具有尺寸稳定性好、具有耐风化和耐腐朽性，强度高的特点；首次利用X射线光电子能谱，发现了Si2p、O1s和C1s谱峰发生了明显的化学位移，证实了Si－O－C键合作用的存在。

DS and distribution of DS were improved. The optimized technology was gotten as follows: sodium borate was 8wt%,alkalization temperature 20 alkalization time 90min.The heat-resistance of CMC was also enhanced by adding sodium silicate in alkalization, and adding sodium borate in etherization in the synthesis of CMC. ra was decreased, but the viscosity was significant increased.

综合考 虑对水溶液粘度和取代度及其分布的影响，得到优化了的工艺配方：硅酸钠的加入量浙江人学硕士学位论文为纤维素的10叭%左右，碱化温度为20℃，碱化时间为90min，采用两次加碱法工艺(Zmol%和1 。1 smol%)，醚化阶段加6wt%的四硼酸钠。

Isobutyl butyrate was synthesized from butyric acid and isobutyl alcohol using tungstosilicic acid as catalyst.

以钨硅酸为催化剂，通过桂酸和戊醇酯化反应合成桂酸戊酯，研究了各有关因素对产品酯化率的影响。

Hybrid mesoporous molecular sieve materials with hexagonal mesoporous structure and covalent bonded polyoxometalates were synthesized based on tetraethoxysilane anti lacunary polyoxometalate, SiW11, via sol-gel method in the presence of triblock copolymers P123 as the structure-directing agent. The influences of molar ratio of inorganic precursors and aging temperature on the structure and the loadings of SiW11 in the hybrid materials were investigated. Some reaction details in the synthesis were revealed.

用嵌段共聚物P123为模板剂，正硅酸乙酯和缺位结构的多金属氧酸盐SiW11为无机前驱体，由溶胶－凝胶法合成了具有六方结构和SiW11共价键联的介孔分子筛杂化材料SiW11/SBA-15，着重考察了无机前驱的配比和老化温度对杂化材料结构及SiW11负载量的影响。

Polyimide/silica (PI/SiO2) nano-hybrid films of different solid content were prepared based on pyromellitic dianhydride and 4, 4'-oxydianiline using tetraethoxysilane as the inorganic precursors.

以均苯四甲酸二酐和4，4'-二氨基二苯醚为有机单体，正硅酸乙酯为无机前驱体，制备了SiO2含量一定，PAA杂化胶液固体含量不同的PI/SiO2纳米杂化薄膜。

The results indicate that aluminum fluoride product will be returned about 140 t,sodium silicofluoride and cryolite are 238 t and 206 t,and neutralization residue is 375 t,if the mother liquor output of aluminum fluoride product is 4000 t per year.The annual economic benefit will reach 1,400,000 yuan RMB.

半工业化实验结果表明：计算年产4 000 t氟化铝产品的母液，企业可回收产品氟化铝140 t，生产副产品氟硅酸钠238 t、冰晶石206 t、中和残渣375 t，每年可获效益140万元人民币。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。