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Palmitic acid-silicon dioxide nano-composite phase change material was prepared by sol-gel process from tetraethyi orthosilicate and palmitic acid.

采用溶胶—凝胶法,以正硅酸乙酯和棕榈酸为主原料,制备了一种有机—无机纳米复合相变材料。

Nanu-SiO2 was syrtthesized though hydrolyzation-condensation of n- tetraethyl orthosilicate in organic solvent using sol-gel method.

西北工业大学理学院,西安710072摘要:采用溶胶一凝胶法,利用正硅酸乙酯在有机溶剂中的水解-缩合制备纳米SiO2。

A simple one-step procedure was described for the synthesis of mesoporous monolith and composite sphere, in which hydrolyzation of tetraethyl orthosilicate and polymerization of urea with formaldehyde occurred at the same time.

利用酸性条件下正硅酸乙酯的水解和脲醛树脂的聚合反应同时一步原位进行的方法合成了二氧化硅复合粉体(包括核壳微球结构和网状结构)和块体凝胶材料。

On such basis, a new porous structured heteropoly acid catalyst is obtained by salt-gel reaction, using tetraethyl orthosilicate as the silicon source.

在此基础上,以正硅酸乙酯为硅源,利用&盐—凝胶&法得到一种新型介孔结构的杂多酸催化剂。

Furthermore, tetraethyl orthosilicate was added to improve the structure of BMBSE film. A hydrophobic composite film of BMBSE/TEOS was successfully prepared on 0Cr18Ni9 stainless steels substrates.

并进一步采用正硅酸乙酯对BMBSE膜的结构进行改进,在不锈钢表面制备了具有一定疏水性的更加致密的BMBSE/TEOS复合膜。

Porous carbons were prepared with tetraethyl orthosilicate as the silica template and solube starch and β-cyclodextrin as carbon precursor by sol-gel method.

以正硅酸乙酯为模板硅源,β-环状糊精和可溶性淀粉分别为碳前驱体,运用溶胶-凝胶法制备了多孔炭材料。

Nanosize SiO_(2) particles were prepared using water-in-oil microemulsion method in polyether polyol with hydrolysis and condensation reactions of tetraethyl orthosilicate by means of controlling molar ratio of water to surfactant and selecting moderate hydrolysis temperature.

选择适当的乳化剂和水解温度以及控制水与乳化剂的摩尔比,采用W/O型微乳液法在聚醚多元醇中通过正硅酸乙酯的水解、缩合反应合成了纳米SiO2。

The sol-gel solution was prepared by mixing ethyl orthosilicate, absolute alcohol and 0.1molL^(-1) HCl in a definite proportion, and adding an appropriate amount of silicotungstic acid as active material, strring for 30min and then standing for 24h at room temperature.

溶胶-凝胶溶液系将正硅酸乙酯、无水乙醇及0.1molL^(-1)盐酸按一定比例混合后加适量的硅钨酸作为活性物质,搅拌30min混匀后在室温放置24h配成。

A kind of spherical microporous silica was synthesized by precipitation with the tetraethyl orthosilicate as a silica precursor and the block ploymer P_(123 as a template. The characterizations by the BET, FSEM and XRD showed that the spherical microporous silica has diameter of 3~4 μm, amorphous pore size of 0.9~1 nm and the specific area of 216±

以正硅酸乙酯作硅源,嵌段共聚物为模板剂,采用沉淀法合成均匀的实心球形二氧化硅微孔材料,BET、FSEM和XRD等表面分析手段表征表明,我们合成的二氧化硅微孔材料具有3~4μm的粒径和不规则分布的0.9~1nm的孔径以及216±3.5m2/g的比表面积。

Silica coating was prepared by atmospheric pressure chemical vapor deposition taking HP40 steel plate as substrate,tetraethyl orthosilicate as silica source,and air as carrier gas and diluent.

以正硅酸乙酯为硅源物质、空气为载气和稀释气,采用常压化学气相沉积法在HP40钢表面制备了SiO2涂层;采用扫描电子显微镜和能量色散能谱表征了SiO2涂层的组织结构和表面形貌;考察了在乙烯裂解的工艺条件下SiO2涂层的结焦抑制能力。

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