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The study shows that, under the conditions of the concentration of sodium silicic acid being 4%-8%,the pH<4, and the reaction time being about 5 hour, the stable polysilicic acid is made.

以水玻璃、废盐酸为原料,制备聚硅酸,研究表明:在硅酸钠浓度为4%~8%,pH小于4的条件下,室温熟化5h左右,可制得稳定的聚硅酸

They are liquid sodium silicate, sodium metasilicate pentahydrate , quick-resolving sodium silicate and silica sol.

详细介绍了联产法生产硅酸钠系列产品新工艺及其特点,对工业液体硅酸钠、五水偏硅酸钠、粉状速溶硅酸钠、硅溶胶 4种产品的原材料规格、质量标准、工艺原理、工艺流程等方面进行了论述。

The problem from sodium tripolyphosphate,4A zeolite,sodium metasilicate and phosphorous prohibition was summarized and the various performances and effect of δ-layered crystal disodium silicate as detergent were analyzed.

分析了现用助洗剂三聚磷酸钠、4A沸石、偏硅酸钠存在的问题及禁磷的重要性,重点论述了δ-层状结晶二硅酸钠用作助洗剂的各种性能及效果,认为δ-层状结晶二硅酸钠是一种良好的无磷助洗剂,它具有其他助洗剂所不具备的优良性能;对δ-层状结晶二硅酸钠的制备工艺作了简要介绍,并作了市场及在国内工业化生产的可性行分析。

By using the silicomolybdic yellow colorimetric method, the paper determines not only the existing form of soluble glass in the newly made-up, being used, and discarded cooling liquid,but also the relation of the stability of cooling liquid to the concentration and standing time of monosilicic acid and total silicic acid. The relation of the concentration of polysil...

本文采用硅钼黄比色法测定新配制、使用中和报废冷却液中的水玻璃存在形态和研究冷却液的稳定性与单正硅酸、总硅酸的浓度和放置时间的相关性;用四氢呋哺萃取比色法测定冷却液中的高聚硅酸含量与放置时间的相关性;研究用超声波、磁场等物理方法处理废冷却液的再生可行性及水玻璃的形态变化。

Through lots of tests, the new technology of preparing the polymeric ferric aluminum silicate sulfate by using the waste-acid of Ti02-industriy and the coal fly ash has been designed. The highest Al-acid stripping rate can be achieved by the waste sulfate acid under boiling degree for 1. 5h when the mass ratio between NaCl and Coal Fly ash is 0. 05:1, as well as that between Coal Fly ash and Waste Acid ratio is 1:10. By means of the oxidation-polymerized reaction under 40-50*C and normal pressure, using NaNCkas catalyst and air as oxidation, the polymeric ferric aluminum sulfate can be obtained. The poly-silicic acid is polymerized with soluble glass in the optimum conditions of pH=5-6 and the concentration of Si02 is about 3%. The inorganic high molecule coagulant of PFASS is synthesized with the poly-silicic acid into the solution of polymeric ferric aluminum sulfate.

本论文通过大量的试验,研究开发出了用粉煤灰及钛白废酸制取聚合硫酸硅酸铁铝的新工艺,其最佳工艺条件为:于沸点温度,以NaCl为助溶剂(NaCl与粉煤灰质量比为0.05:1),以钛白废酸浸取粉煤灰(固液比为1:10)中的铝1.5小时,最大浸取率可达40%;经过滤洗涤后,调节滤液pH至2.0左右,以NANO_2为催化剂(NaNO_2用量为滤液中FeSO_4·7H_2O量的3%),空气为氧化剂,于40-50℃进行常压催化氧化反应,制取聚合硫酸铁铝,催化氧化时间为2小时;将工业水玻璃稀释至3%左右,调节其pH于5-6,室温下制备活性聚硅酸;将活性聚硅酸与聚合硫酸铁铝按照一定比例复合,经熟化,即制得新型无机高分子混凝剂PFASS。

SiO2 causes early decomposition of CaSO4 due to the formation of calcium silicate and dicalcium silicate during the reaction of CaO and SiO2 at high temperature, and the formation of calcium sulphosilicate above 1200℃ helps to retard CaSO4 decomposition.

SiO2在高温下易与CaO发生固相反应形成硅酸二钙和硅酸钙使得CaSO4的初始分解温度降低,在1200℃以后硫硅酸钙的形成对CaSO4的分解有一定的延缓作用。

The main products are inorganic fluoride, with the integrated capacity of 150 thousand tons per year, our main products are: synthetic cryolite, aluminium fluoride, sodium fluoride, silica white, hydrofluoride, potassium fluoroborate, potassium fluotitanate, potassium aluminium fluoride, magnesium fluoride, barium fluoride, lithium fluoride ,potassium fluoride, magnesium fluorosilicate, potassium fluorosilicate, potassium fluorosilicate etc.

多氟多公司生产区多氟多化工股份有限公司,公司注册资本8000万元,为河南省高新技术企业,是中国最大的无机氟化盐生产基地之一。综合产能15万吨/年,主要产品有冰晶石、氟化铝氟化钠、白炭黑、氢氟酸、氟硼酸钾、氟钛酸钾、氟铝酸钾、氟化镁、氟化钡、氟锆酸钾、氟化氢铵、氟化铵、氟化钾、氟化锂、氟硅酸钠、氟硅酸钾、氟硅酸镁等。

And it is expected to replace the expensive organic polymer coagulants which were often suspected of being dangerous to human.The preparation technique of HSPSAS was introduced in this paper. The parameters of the process were discussed by the method of orthogonal design, such as molar ratio of Al/Si, the pH of polysilicate, the aging time of polysilicate, the pH of PSAS, the aging time of PSAS, intake of PSAS, and so on, and then an optical technology was obtained.

本文介绍了聚硅酸硫酸铝絮凝剂的制备工艺,并利用正交设计的方法,对其中Al/Si摩尔比、硅酸熟化pH值、聚硅酸熟化时间、药品熟化pH、药品熟化时间、投药量等制备参数进行了分析和讨论,得到优化的制备条件,确定了更为合理的制备工艺。

This further indicated that when the acetic acid compound existed it could slow the growth rate of the particles of polysilicic acid, but total species distribution and its transformation model of polysilicic acid did not change.

乙酸化合物的存在,能够有效减缓硅酸溶液中聚硅酸颗粒物的生长速度,但聚硅酸的总体形态分布与转化规律的模式并没有因为乙酸的存在而发生根本的改变。

The species distribution and transformation characteristics of polysilicic acid in the presence of acetic acid were investigated by chemical Si-Mo assay analysis.

针对聚硅酸金属盐絮凝剂因硅酸聚合胶凝而失活的问题,依照Si-Mo比色法的原理,对乙酸存在时的聚硅酸形态及其转化规律进行研究。

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