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Methods Cyclohexane, ethyl acetate and glacial acetic acid (8∶8∶0.8) were used as the developing solvent. Samples were analyzed on a layer plate of silica gel G thin by using 20% phosphomolybdic acid as chromogenic agent.

以环己烷乙酸乙酯冰醋酸(体积比8∶8∶0.8)为展开剂,以羧甲基纤维素钠为黏合剂自制硅胶G薄层板,20%磷钼酸溶液为显色剂,进行薄层色谱分析。

A traditional acidification method incorporated with an ether extraction technique was used to prepare silicotungstic acid and phosphotungstic acid with Keggin structure.

采用盐酸酸化-乙醚萃取法制备了Keggin型硅钨酸、磷钨酸,并分别以活性炭和硅胶为载体,采用不同的制备方法制备出一系列负载型杂多酸。

Due to its large surface area, mesoporous structure, pure anatase structure and high adsorption capacity, the photoactivity of 31%TiO〓/SiO〓 was much higher than that of the pure titanium dioxide.

多孔硅胶抑制了高温时TiO〓晶型由锐钛矿向金红石型的转变,并且对TiO〓具有很好的分散能力。

IC(50)=25.02 μg/ml was detected, The compound came from n-butanol extract of Plantago asiatica L. via silica column chromatography.

实验结果表明,车前子正丁醇提取物经硅胶柱层析所得到的第二段收集物中所含物质对DU145细胞生长具有很强的抑制活性,其IC_(50)值为25.02μg/ml。

C18 esterified silica monolithic column emerging from chromatogram realm was made by use of solid-phase extraction medium material in μ-TAS. Several simple solid-phase extraction pretreatment units were set up to preconcentrate dobutamine hydrochloride which was detected by dobutamine hydrochloride-KMnO4-Luminol chemiluminescence system.

以改性C18反相硅胶整体柱为微流控芯片分析系统中固相萃取介质材料,构建不同功能单元的样品预处理微分析系统,实现了血清样品中痕量盐酸多巴酚丁胺的富集。

Their pure products of the six compounds were obtained by silica gel column chromatography and recrystallization in propanone solution.

通过硅胶柱色谱分离和重结晶对所得的六种化合物纯化后获得它们的纯化合物。

Insulate the tube type series:Dian tube Pyrocondensation, silicone tube, yellow wax tubes, high temperature casing, waterproof cable connector, environmental conservation rubber coil, beam lines ring, beam lines Block.

三、绝缘管类系列:热缩佃管、硅胶管、黄腊管、高温套管、防水电缆接头、环保橡胶护线圈、束线环、束线座。

Key words: breast implants;N-vinyl pyrrolidone;CT

硅胶乳房假体;N-乙烯基吡咯烷酮;CT

Methods N-vinyl pyrrolidone, the hydrophilic monomer, was grafted onto the surface of silicone breast implants by 60Co radiation.The implants were buried in the bilateral subcutaneous layers of the back of rabbits.The unchanged implants were used as the control group.

利用钴60共辐射的方法把亲水性单体 N-乙烯基吡咯烷酮接枝到硅胶乳房假体表面,改变其表面特性后植入兔的背部,以未经改性的正常假体作为对照组,隔一定时间通过组织切片及CT扫描的方法观察假体周围纤维囊壁的形成情况。

The solid-liquid reaction method was used for the preparation of HPLC aryl-bonded silica gel stationary phases, including 3, 5-dinitrobenzyl, quinolinyl ether and 1, 1'-di(2-naphthol) ether bonded silica gel stationary phases by using N-(β-aminoethy1)-γ-aminopropylmethyldimethoxy silane and 3-glyci-doxypropyl trimethoxylsilane as coupling reagents, respectively.

采用固液相连续反应,以N--γ-氨丙基甲基二甲氧基硅烷和γ-丙基三甲氧基硅烷为偶联剂,分别制备了二硝基苯甲酰胺基、喹啉醚基和联萘酚醚基三种芳基键合硅胶固定相。

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