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Xi'an Dongfang Mech Group Company Abstract : A high precision data collection system is designed by using 24 bits ADC which has the function of self - calibration and signal processing.

扩散硅压力传感器及变送器参数测试系统:采用具有自校验和信号调理功能的24 位ADC ,开发设计了一种高精度数据采集系统。

In this study, the CPE processes of four different kinds of polyaromatic hydrocarbons, acenaphthene, anthracene, phenanthrene a...

今利用两种聚醚型有机硅表面活性剂DC-193和DC-190,对蒽、菲、芘和苊四种多环芳烃进行浊点萃取研究,分别使用加热、加盐、离心和搅拌等辅助方法改变相分离过程的速度。

Effects of three feeding methods on siloxane modified acrylate emulsion polymerization stability and properties of emulsion were studied.

研究了3种单体投入方式对有机硅改性丙烯酸酯乳液聚合稳定性及性能的影响。

The effect of the substrate on the surface properties of organosilicon polymer and acrylate polymer blend films was investigated.

研究了成膜基材对有机硅聚合物-聚甲基丙烯酸甲酯溶液共混物薄膜表面性能的影响。

Calcium carbonate and soluble glass and so on were confected as alkaline antifouling agent. The Infrared Spectrometry results showed that 2275-2250 cm~(-1) diagnostic absorb wave crest in part A and 3390-3200 cm~(-1) in part B and 1730 cm~(-1) in coating film strongly proved polymers reacted just as the reacting mechanism, that means polysiloxane which offer low-surface-energy property linked Polyurethane system by —OH groups reacting with —NCO groups. Relative molar mass of part A and part B was determined by Gel Permeation Chromatography and the results were appropriate. Surface-energy was determined and results were between 33.6-47.17 mN/m and it increased when alkaline antifouling agent was put into the coating. Alkaline antifouling agent was releasing steadily when the coating film was dipped in seawater. As time gone, the pH value of seawater was increasing. Solubility parameter and results showed that there was no corrasive phenomenon between the polyethylene strand and the coating.

红外光谱分析结果表明,出现在A组分中的2275~2250cm~(-1)处的异氰酸酯特征吸收峰、B组分中的3390~3200cm~(-1)处硅羟基的特征吸收峰及出现在固化后涂膜中的1730cm~(-1)处氨基甲酸酯基团的特征吸收峰证明了涂料成膜物质交联固化符合本文的设计要求,即赋予涂膜低表面能特性的有机硅组分通过—OH基团与—NCO基团的反应已经链接到聚氨酯体系中;凝胶渗透色谱结果表明,成膜物质的A、B组分均为低分子量,符合预聚物的要求;涂膜表面能的测算结果表明,涂膜的表面能在33.6~47.17mN/m之间;加入碱式防污剂后涂膜的表面能略有升高;碱式防污剂的释放平稳,随着涂膜在海水中浸泡时间的增长,pH值有增加的趋势;用溶解度参数原则来评价涂料与网绳的涂装,结果表明,本试验研制的防污涂料对聚乙烯网绳无溶蚀作用。

Steelmaking Plant can be reduced to 20ppm by increasing argon flow of RH degasser and controlling vacuity According to the above results, the main efforts to develop IF steels have been made at No 3 Steelmaking Plant.

研究结果表明:钢水增碳主要在大包中发生,影响钢水增碳的主要因素是钢液与包壁接触面积与钢水体积之比,在高温下,耐火材料中CO的压力和钢水中Als的含量对钢水增碳也有一定的影响;钢水脱氧后将增硅,钢水的增硅量主要受大包渣的碱度、中包绝热板材料和中包保护渣碱度的影响;通过增大RH真空处理装置的氩气流量和控制真空度,能将三炼钢厂大包钢水的碳含量降到20ppm左右。

The results show that the SAPO–5 has a pillar-like morphology with the size of about 20 μm×5 μm×5 μm.The ratio of P:Al:Si is 1:1.19:0.67 in its crystal structure, the content of Si is high. The total acidimety fo the SAPO–5 is 578.0 μmol/g , hihger than that of prepared by one step crystalline hydrothermal method.And its initial catalysis character performance on normal butane isomerization reaction reach 24.8 %, higher than that of prepared by one step crystalline hydrothermal method.

实验结果表明:产物为柱状的磷酸硅铝分子筛,其晶粒尺寸大约为20 μm×5 μm×5 μm,其晶体结构中P:Al:Si=1:1.19:0.67,硅含量较高;采用分段晶化方式制备的SAPO-5分子筛的总酸量为578.0 μmol/g高于一段晶化方式制备的SAPO-5分子筛的总酸量;采用分段晶化生成的SAPO-5分子筛的催化正丁烷异构化反应初始活性可达到24.8 %,远高于一段晶化制备的SAPO-5分子筛的初始活性14.1 %。

The preferred organometallic compounds of the present invention are of the formula (R1)m M(PR23)x, where M is a metal selected from the group consisting of manganese, technetium, rhenium, iron, cobalt, nickel, ruthenium, rhodium, palladium, osmium iridium and platinum wherein m is 0, 1, 2, 3 or 4; x is 2, 3, 4 or 5 and m+x are 2, 3, 4, 5, 6, 7 or 8, m and x selected according to each metals appropriate valence; each R1 is independently selected from the group consisting of hydrogen, deuterium, N2, H2, D2 and a variety of substituted alkyl groups; each R2 is independently selected from the group consisting of lower alkyl, aryl, arylalkyl, and alkyl-Z, aryl-Z and arylalkyl-Z where Z is selected from the group consisting of oxy, silyl, siloxy, oxysilyl, siloxy, oxysiloxy, silyalkyl, oxysilylalkyl, siloxyalkyl, oxysiloxyalkyl, silylalkoxy, silylalkoxy, siloxyalkoxy and oxysiloxyalkoxy; and wherein when M is cobalt and one group R1 is selected to be N2, then m is 2 and the second group R1 is hydrogen or deuterium.

有机化合物的首选本发明的配方是米(R1代)米×(pr23)、那里是一米的金属挑选出来,第一组由锰、锝、铼、铁、钴、镍、钌、铑、钯、锇、铱铂其中M是0、1、2、3或4; X是2,3, 4或5米×+有2,3,4,5,6,7或8 米和X挑选合适的价按每个金属; R1的是每一组由独立选自氢、氘、氮、氢气、 D2和各种烷基取代群体; R2中的每个组由独立选自烷基低、芳、芳基烷基、烷基的Z、芳基、芳基烷基的Z-那里的ZZ是选自组风、含硅、氧、oxysilyl、硅、oxysiloxy,silyalkyl, oxysilylalkyl,siloxyalkyl,oxysiloxyalkyl,silylalkoxy,silylalkoxy,siloxyalkoxy和oxysiloxyalkoxy;其中,M是当钴一派R1的选择是氮气、然后是2米,第二组R1的氘是氢或者。

New reactions found in this program include: photoinduced regioselective free radical addition to aromatic imines;photoinduced Dielse-Alder reactions of aromatic imines for synthesis of tetrahydroquinoline derivatives;Photoinduced radical cation mediated selective ring opening reaction of epoxides;Formation of novel macrocyclic crown ethers by photoinduced reaction of diazonaphthaquinones;photoinduced selective desilylation of silyl ethers.

用这种方法成功的发现了下列在有机合成中有意义的新反应:(1)光诱导产生的自由基正离子诱导的自由基对芳香亚胺的区域选择性加成反应;(2)用光诱导的芳香亚胺的Diels-Alder反应合成四氢喹啉衍生物;(3)经光诱导产生的自由基正离子基诱导的环氧化物选择性开环反应;(4)重氮萘酮在环醚中经光诱导反应形成新奇的大环冠醚;(5)硅醚的光诱导选择性脱硅基反应。

It is considered in this paper that the light and heat oxygen resistance ageings of silicone acrylate resin are better than those of normal acrylic and polyurethane resins, through the theoretic investigations into the reaction mechanisms of the light and heat oxygen ageings of high molecular polymer and contrasting, when exposed to light and under a high temperature, the changes in colour,shape, tensile strength and elongation of Silicone Acrylate Resin DX 8501 to the normal acrylic and polyur...

本文通过对高分子聚合物的光氧老化、热氧老化的反应机理的理论探讨和对DX8501硅丙树脂、普通丙烯酸树脂、普通聚氨酯胶膜在紫外光照射下和高温条件下的颜色、形态、抗张强度、伸长率的变化情况对比,认为硅丙树脂的耐光氧老化和耐热氧老化的性能优于普通的丙烯酸树脂和普通的聚氨酯。表3,参考文献8

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