硅的

Quinone methides, generated in situ from the reaction of 4-hydroxycoumarin with benzaldehyde, formaldehyde and pentanal, underwent the Diels-Alder reaction with silyl enol ethers to give a series of 3,4-dihydro-2H,5H-pyrano[3,2-c][1]benzopyran derivatives in high yields.

通过4-羟基香豆素与苯甲醛、甲醛和戊醛缩合产生的quinone methide与烯醇硅醚的Diels-Alder反应，以较高产率合成了一系列含有硅氧基的3，4-二氢-2H，5H-吡喃并[3，2-c][1]苯并吡喃-5-酮衍生物。

The purification-pretreatment technique of 8 kinds of solid phase extracting column stuffing (silica gel, acid silica gel, Florisil, siliceous magnesium sorbent, Al2O3, celite 545, acid celite, Al2O3+silica gel) for the prepared polluted soil containing 13 kinds of organochlorine pesticides (α-HCH,β-HCH,γ-HCH,δ-HCH, o,p'-DDT, o,p'-DDE, p,p'-DDT, p,p'-DDD, p,p'-DDE, a-endosulfan, dieldrin, endrin, hexachlorobenzene) was screened prior.

用製备的8种固相萃取柱填料（硅胶，酸化硅胶，氟罗里硅土，硅镁型载体，Al2O3，硅藻土载体545，酸性硅藻土，Al2O3+硅胶）对含有13种有机氯农药的污染土壤的纯化预处理技术进行了优化筛选。

Thiazolidiane-4-carboxylic acid was prepared and used as the aid catalyst that has strengthened the catalytic effect of chloroplatinic acid, greatly improved the yield of the hydrosilylation of methyldichlorosilane with allychloride, and made the yield get to 64.9%.

通过比较，选用自制的含硫化合物4-羧基-1，3-噻唑烷作助催化剂，大大增强了氯铂酸的催化活性，使甲基二氯硅烷与氯丙烯的加成反应以较高产率得到γ-氯丙基甲基二氯硅烷，产率可达64.9%。

In this research the necessary of desiliconization process which take precedence of dephosphorization pretreatment is studied, also the desiliconization experiment by charging desiliconization agent into iron runner of BF in Jiuquan Steel Plant is studied too.

对铁水脱磷处理前的铁水预脱硅处理的必要性及在酒钢高炉出铁沟内进行的投撒预脱硅实验进行了分析。

And it is because of this kind of "solvent effect" that the blends of diethyl silicone andmany lubricant oils show outstanding properties in ...

利用乙基硅油与不同油品调和时产生的&溶剂效应&可以说明乙基硅油调和油具有独特的粘度和粘温特性的原因。

Bis vinyl phenyl terminated polydimethylsiloxane was synthesized by the hydrosilylation of bis dimethylhydrogen siloxyl terminated PDMS with m divinyl benzene. The structure of the VTPDMS was characterized by 1H NMR.

通过双二甲基氢硅氧封端的聚二甲基硅氧烷与间二乙烯基苯的硅氢加成反应制备了双乙烯基苯封端的聚二甲基硅氧烷，用1H NMR对其结构进行了表征。

A method for the determination of ferrum content in cobalt based alloy dust by Air-C 2 H 2 flame atomic absorption spectrophotometry was set up.

建立了一种用空气-乙炔火焰原子吸收法测定钴基合金喷粉中铁含量的分析方法，探讨了硅对铁测定的干扰机理，对用氯化钙作为硅干扰铁测定的释放剂进行了试验。

Electronic gases are meant to become hyper-pure and hyper-clean, and market prospects of hyperpure silicon hydride are quite promising as relevant industries in China are growing fast.

超纯、超净是未来硅烷等电子气体发展的方向，随着国内相关产业的迅速发展和规模化，超纯硅烷的市场前景广阔。

From our experimental results, the porous c-Si and porous microcrystalline silicon films have the same luminescence mechanism.

我们对晶体多孔硅和多孔化微晶硅两类样品的比较表明两者的发光机制是一致的。

Three part of research works had been carried out in the dissertation. The first part: a kind of multidentate amine modified silica gel was synthesized through the following steps:(1) introduce the amino groups onto the surface of silica-gel by the treatment of surface silanol groups withγ-aminopropyl trimethoxy silane;(2) michael addition of excess trihydroxymethyl propyl triacrylate to amino groups on the silica gel surface;(3) amidation of the unreacted double bonds of TMPTA on the surface of TMPTA modified silica gel with diethylenetriamine;(4) the multidentate amine modified silica gel was finally obtained by the reaction of amino groups on the surface of DETA modified silica gel with double bond of butyl acrylate.

本论文进行了三部分研究工作，第一部分：通过多步反应对硅胶进行改性合成了一种多齿胺改性硅胶配体，合成过程如下：1通过γ-氨丙基三甲氧基硅烷与硅胶表面的硅羟基反应，使硅胶表面带有氨基；2利用硅胶表面氨基与过量的三羟甲基丙烷三丙烯酸酯发生Michael加成反应；3利用二乙烯三胺与TMPTA改性硅胶表面未反应的双键发生反应使硅胶表面氨基化；4最后用丙烯酸正丁酯与DETA改性硅胶表面氨基充分反应成功合多齿胺改性硅胶配体。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷