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硅烷

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Methyltrichlorosilicane and phenyltrichlorosilicane are applied for the synthesization of the ladderlike polymethylsilsesquioxane and ladderlike polyphenylsilsesquioxane.

选用甲基三氯硅烷和苯基三氯硅烷为主要原料合成了梯形聚甲基倍半硅氧烷和梯形聚苯基倍半硅氧烷。

Monofilm of silane on the surface of the glass substrates is prepared via the method of self-assembled monolayers, Hf (SO4)24H2O and HCI are used as raw materials, HfO2 thin films are prepared on the active groups of the alkyl silane by the liquid phase deposition.

利用自组装单层膜技术,在玻璃基板上生长有机硅烷单分子膜层,以Hf(SO4)24H2O和HCI配制HfO2前驱液,通过液相沉积在硅烷的功能性官能团上诱导生成二氧化铪薄膜。

With heated water for extraction, DMSO,HMDS and C3H9 CLSI as derived reagent, the content of monose in Acanthopanax Senticosus tea is determined by capillary chromatography.

采用沸水提取,二甲基亚砜溶解,六甲基二硅氨烷和三甲基氯硅烷为衍生试剂,用毛细管气相色谱法测定了五加参茶中的糖含量,共测出6种单糖。

Finally the application of the homemade ODS for MSPD and the economical availability of the product was evaluated. Results show as the following: 1. It is a simple method for the preparation of a bonded octadecyl phase which has large particle and high extent of coverage of the bonded phase.

研究结果表明:①采用大粒径无定形硅胶为基质,选择十八烷基三氯硅烷硅烷化试剂,完整地合成了一种大颗粒、高表面积的ODS键合相,合成的ODS可作为基质固相分散MSPD的固相分散剂,用于样品的前处理。

Monolayer.2. A Novel Sensor Based on Layer-by-Layer Hybridized Phosphomolybdate and Poly on a Cysteamine Modified Gold ElectrodeA novel sensor have been constructed by layer-by-layer hybridizing phosphomolybdate and poly on a cysteamine modified gold electrode.

磷钼杂多酸和聚二茂铁硅烷多层组装膜修饰电极及其电化学行为采用层层组装法在金电极上组装多金属氧酸盐阴离子和聚阳离子聚二茂铁硅烷,交替沉积多层膜,构建了杂多酸-PFS多层膜修饰的金电极。

The gelatin-siloxane nano-particles are prepared from gelatin and 3-(2,3-epoxy propoxy )propyltrimethoxysilicane by performing chemical combination and hydrolytic reaction in acidic condition to obtain sol; and adjusting the pH value to slightly alkaline for performing polymerization reaction of silicane.

将明胶和3-(2,3-环氧丙氧)丙基三甲氧基硅烷在酸性条件进行化合、水解反应;将该溶胶的pH值调节至弱碱性,使硅烷发生聚合反应,即可得明胶-硅氧烷纳米颗粒。

The solid-liquid reaction method was used for the preparation of HPLC aryl-bonded silica gel stationary phases, including 3, 5-dinitrobenzyl, quinolinyl ether and 1, 1'-di(2-naphthol) ether bonded silica gel stationary phases by using N-(β-aminoethy1)-γ-aminopropylmethyldimethoxy silane and 3-glyci-doxypropyl trimethoxylsilane as coupling reagents, respectively.

采用固液相连续反应,以N--γ-氨丙基甲基二甲氧基硅烷和γ-丙基三甲氧基硅烷为偶联剂,分别制备了二硝基苯甲酰胺基、喹啉醚基和联萘酚醚基三种芳基键合硅胶固定相。

Methods:Purchased spherical silica particles (5 μm) were refluxed in anhydrous toluene with vinyl-triethoxysilane for 18 h, to modify the surface with vinylsilyl groups.

将商品球形硅胶颗粒(粒径5μm)与乙烯基三乙氧基硅烷通过在无水甲苯中回流18 h,进行硅烷化修饰。

The results indicate that the average permeability coefficient of 2 hours calculated by using the proposed method can effectively reflect the waterproofing effect of silicane.

结果表明,采用这种方法计算出的2h平均渗透系数可有效反映硅烷的防水效果。关键词:硅烷;防水;现场;评价;方法

In this paper, the effect of silicane coupling agent γ-aminopropyl triethy-oxysilane(A-1100) on interface properties of short glass fibre reinforced polycarbonate is report-ed.

针对短切玻纤增强聚碳酸酯体系,研究了硅烷偶联剂γ-氨丙基三乙基硅烷(A-1100)在上述复合体系中的界面偶联特性。

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