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The method includes steps:(1) dropping triethoxy - 3 - propyl silicane isocyanic acid to ethanol solution of pH sensitive reagent to obtain reaction fluid A;(2) mixing siloxane, acid, and water to obtain reaction fluid B;(3) mixing reaction fluid A, reaction fluid B and solution of calcium chloride according to proportion to obtain solution C;(4) coating solution C on micropore base of micropore plate, using sealing tape to seal micropores, and using needle to perforate each micropore at center, and protecting from light; after placing it a period of time, the method adds distilled water to micropores, keeping the back up.

本发明公开了一种微孔板pH传感器的原位制备方法,其步骤是首先将三乙氧基-3-异氰酸丙基硅烷滴入pH敏感试剂的乙醇溶液中,得反应液A;其次是将硅氧烷、酸和水混合,得反应液B;第三是取反应液A、反应液B及氯化钙溶液,按比例混合,得溶液C;第四是取溶液C涂于微孔板的微孔底部,用密封带将微孔封住,并用针在每个微孔中央刺孔,避光保存。

A novel polyurethane dispersion with high gloss and excel le nt mechanical properties was prepared with polyether glycol and isophorone diiso cyanate as raw materials and castor oil and 3-aminopropyl-triethoxysilane as cross-linking agents.

探讨了胶膜光泽度与亲水基团及蓖麻油含量的关系,同时研究了氨丙基三乙氧基硅烷的加入对材料的机械性能和耐水性产生的影响。

Effect of percutaneous penetration ,including influence of different formulations on penetration,and lipolytic activity of Siloxanetriol alginate were studied using the techniques of percutaneous penetration in vutro and adipose tissue incubation in vitro.

利用体外经皮渗透和脂肪组织体外培养技术,探讨了硅烷醇C 经皮渗透和配方的促渗透,以及对脂肪组织的脂解作用。

The performance of the WD-10 and its main component dodecaalkyl trimethoxysilane were introduced in this article,and the application in the surface protection of the lithoid cultural relic was also brief described.

本文介绍WD - 10及其主体成分十二烷基三甲氧基硅烷的性能,并介绍了在石质文物表面封护中的应

The synthesis of methyl mandelate catalyzed by dodetungstophosphoric acid supported on modified silica gel with 3-aminopropyltriethoxysilane (HPW/M-SiO2) has been studied.

γ-氨丙基三乙氧基硅烷修饰的硅胶负载磷钨酸(HPW/M-SiO2)催化剂催化合成扁桃酸甲酯。

Taking zinc oxide and phosphoric acid as raw materials and silane coupling agent as modified agent,the micro-size zinc phosphate is prepared by wet-process mechanicochemical method and its modification is carried out.

以氧化锌和磷酸为原料,以硅烷偶联剂为改性剂,采用机械力化学湿法制备微细磷酸锌并进行表面改性。

Because of the strong interaction between the trimethychlorosilicane and surface hydroxy groups of mordenite, silylation is used to modify mordenite.

本文旨在通过硅烷化、脱铝改性丝光沸石,以提高丝光沸石疏水性能,为疏水沸石的开发利用提供一些基本数据和实验依据。

Sequence tests showed that when the SiO2 tubes were treated in 10% aminosilane solution and 3% glutaraldehyde solution for 3 hours and 2 hours, respectively, the HCV monoclonal antibody had high immobilization efficiency and low nonspecificity, and the HCAg was detected to 1 ng/mL.

结果显示,通过条件优化实验,发现以10%的氨基硅烷水溶液处理玻璃试管3 h后,再用3%的戊二醛水溶液交联丙肝单克隆抗体2 h,可以得到固定效果较好,非特异性较低的玻璃载体,对HCAg可测至1 μg/L。

Methods used in other high-performance liquid chromatography for determination of active ingredients, octadecyl silane for the bonded silica filler; methanol - water (55:45) as mobile phase, detection at 254nm.

采用高效液相色谱法对方中有效成分进行含量测定,用十八烷基硅烷键合硅胶为填充剂;甲醇-水(55:45)为流动相,检测波长为254nm。

Scanning electron microscopy,transmission electron microscopy,circular dichroism and small-angle X-ray diffraction were used to analyze the aggregation mode of CSG in the organogel phase.A hierarchical self-assembly model was proposed to explain the transition from molecular to primary and secondary structure.It is shown from our results that CSG can aggregate into a micellar fibril nanostructure with high length-to-width ratio which is bundled and entangled to form a three-dimensional(3D) network that immobilize the fluid component probably by surface tension.Moreover,sol-gel polymerization of tetraethoxysilane was carried out using CSG in the gel phase.

通过扫描电镜(ScanningElectron Microscopy,SEM)、透射电镜(Transmission Electron Microscopy,TEM)、圆二色谱(Circular Dichroism,CD)和小角X—射线衍射仪(Small-angle X-rayDiffraction,SAXRD)考察CSG分子自组装行为结果表明,CSG形成的聚集体具有多级结构:首先CSG通过手性堆叠自组装形成直径在9—10nm的细纳米纤维,这些细的纳米纤维再以不规则的六方堆积的方式进行排列,构成直径在40—100nm的粗纳米纤维(即细纳米纤维的&捆束&),最后粗纳米纤维互相粘连形成三维网络状结构,使有机溶剂&固定&,从而形成凝胶;以CSG有机凝胶为模板,四乙氧基硅烷为前体,通过溶胶—凝胶聚合的方法制备了直径大约为100nm的二氧化硅纳米管。3。

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