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For the strong activity of Nano-Si02, the conglobation will happen easily. It is modified and dispersed with KH-570 and the ultra dispersing agent by means of mechanical and ultrasonic dispersion.

针对nano-SiO_2在涂料中不易分散且分散稳定性差,易发生一次团聚的问题,加入硅烷偶联剂KH-570和超分散剂,采用机械分散为主、超声波分散为辅的方法,对其进行改性和分散。

The basic function of emulsified asphalt modified with silane coupler was studied in this paper.

研究了硅烷偶联剂改性乳化沥青的基本性能。

In the aspects of research method, we took the method of preparing sol at first and then impregnating the wood to obtain ceramic-wood composite; this method made the wood use efficiently and increased the wood's weight gain percent. The ceramic-wood composite with performances of well decay resistance, dimensional stability, effloresce resistance and high strength was obtained by importing the cymene to the net of gel as the result of co-hydroxylation between MTES and TEOS. Making use of XPS ,we found that the apex of Si2p、O1s、C1s had evident chemical shift , which validated the existence of Si-O-C bonding.Key Words: Sol-gel, Ceramic-wood composite, Modified sol, Ecomaterials

在工艺方法上,采用先制备溶胶,然后浸注木材的工艺方法具有原料利用率高、提高增重率的优点;采用甲基三乙氧基硅烷和正硅酸乙酯共水解的方法,将甲基引入陶瓷化复合木材的凝胶内部,所制备的材料具有尺寸稳定性好、具有耐风化和耐腐朽性,强度高的特点;首次利用X射线光电子能谱,发现了Si2p、O1s和C1s谱峰发生了明显的化学位移,证实了Si-O-C键合作用的存在。

Increasing the modified time from 0 day to 4 days, the surface contact angle indicated by glycerol increased from 88.7° to 99.0°, indicated by water from 54.2°to 69.1° and indicated by diazomethane declined hum 40.0° to 31.9°.

结果表明,改性0-10d的木材吸水率从138.4%下降到111.1%;木材分别经过1d、2d和4d的硅烷化改性,甘油表面接触角从未改性时的88.7°上升到99.0°,蒸馏水表面接触角从54.2°上升到69.1°,二碘甲烷则从40.0°下降到31.9°。

The rubber composition for covering a carcass cord of the present invention comprises 25 to 80 parts by mass of silica, 1 to 15 parts by mass of a silane coupling agent and 3 to 30 parts by mass of an organic vulcanizing agent represented by the following general formula (1):- n - wherein R is -(CH 2 -CH 2 -O) m -CH 2 -CH 2 -; x is an integer of 2 to 6; n is an integer of 10 to 400; and m is an integer of 2 to 5, based on 100 parts by weight of a diene rubber, and a tire prepared by using the rubber composition.

以100重量份的二烯橡胶为基准,本发明的用于包覆胎体帘线的该橡胶组合物包含25~80质量份的二氧化硅、1~15质量份的硅烷偶联剂和3~30质量份的由如下化学式(1)表示的有机硫化剂:- n -,其中R是-(CH 2 -CH 2 -O) m -CH 2 -CH 2 -;x是2~6的整数;n是10~400的整数;并且m是2~5的整数,以及使用该橡胶组合物制备的轮胎。

Of anhydrous dioxane was then added dropwise in 30 minutes.

0.15摩尔甲基二氯硅烷)在150厘米。无水二氧3滴加当时在30分钟内。

At this stage, the solid pyrolyzed products of polysiloxane and polycarbosilane were amorphous silicon oxycarbide and nonstoichiometric silicon carbide containing excess carbon, respectively At higher temperature, structure of the amorphous pyrolyzed products started to rearrange and experienced a disorder →order transformation, even crystallized Cristobalite crystallized from SiO〓C〓, and β-SiC also crystallized from SiO〓C〓 provided carbon content of the starting polysiloxane was high enough, while β-SiC crystallized from SiC〓.

当热解温度达1000℃时,聚合物先驱体的无机化过程已基本完成,其陶瓷转化率值趋于稳定,此时聚硅氧烷的热解产物为非晶态的氧碳化硅,聚碳硅烷的热解产物则为含过量碳的非化学计量比的非晶态碳化硅;随着热解温度的升高,非晶态热解产物的结构逐步调整,发生无序→有序的相变,以至析晶。

The relationship between molecular modification of erythromycin and NMR chemical shifts was summarized. It's noticeable that downfield of shifts of H-3 (△δ 0.2) after silylation and upfield of shifts (△δ-0.4) after methylation. No changes were observed after methylation.

分析总结了红霉素分子修饰与核磁共振化学位移变化之间的关系,并且发现大环上H-3硅烷化后由高场移至低场(△δ为0.2),甲基化后又由低场移至高场(△δ为-0.4),变化均较大;而且一旦甲基化后H-3化学位移在高场几乎不再变化。

The process of both photoluminescence and electroluminescence,and the property of photoluminescence and electroluminescence on polysilane were introduced.

介绍了光致发光和电致发光的过程及聚硅烷的光致发光和电致发光性的研究进展。

SiC thin films of large area were prepared successfully in a plasma-enchanced CVD reactor at room temperature, with silane and ethene used as raw materials and Ar as carrier gas.

采用射频等离子体增强的气相沉积法,以硅烷和乙烯为原料,在常温下成功的合成了碳化硅薄膜。

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