硅化处理

The water from cleaning silicon residue could be used as water-confected in refining epsom salt.

对于采用氟化物助浸所产生的氟化硅(SiF_4)气体环境问题，采用空心喷淋塔喷淋清水吸收方式处理。

A computer-aided local transient flow property measuring system was developed using a high speed CCD camera coupled with optical fibers in order to study the Gas-liquid-solid three-phase jet loop reactors. SnO2 crystal films were orientally deposited on the alkoxysilane molecule-coated hydroxyl glass substrates so as to prepare surface-marked particles as the tracers. An image analysis system was established to identify different phases. Stroboscopic photography was utilized to extend the measure range. The developed measuring and analysis system was capable of determining accurately the local transient flow property in a G-L-S jet loop reactor. Based on the above system, local transient flow properties of gas, liquid, and solid phase were measured and studied the influences of fluid property, operation and configuration parameters on the reactor.

以气液固三相喷射环流反应器为研究对象，将高速CCD和光纤束耦合制成局部瞬态流动特性微机数据采集及图象处理系统，利用MPS硅烷分子在带有羟基的玻璃基底上的自组装引导SnO2晶态膜层在功能化表面上进行沉积，以获得表面标记的示踪粒子，解决图象处理技术与相的识别的问题，利用频闪技术拓展了测量上限，得到可以准确测定气液固三相喷射环流反应器中局部瞬态流动特性的测试系统；采用上述测试技术进行喷射环流反应器中局部气相、液相与固相瞬态流动特性的实验研究，并考察物性参数、操作参数与结构参数的影响规律。

Its specific procedures are :first to treat the sample with hydrofluoric acid to convert the silica into a gas of silicon tetrafluoride to escape, and then at a PH value of 4 to 5 to treat the residual liquid with hydroxylamine hydrochloride to get the ferric ions reduced to ferrous ions.

其具体步骤为：首先用氢氟酸处理试样，使沉淀法白炭黑转化成四氟化硅气体逸出。

The state of soluble univalent ions of Na(superscript +) and K(superscript +) is very stable and almost unaffected by thermal oxidation treatment.

一价可溶性离子Na和K非常稳定，热氧化处理基本上不改变其在氮化硅颗粒表面的存在状态。

After several practical problems are resolved,the relation between contents of S,Si and Al has been disclosed.The ratio of Ca to Alin in steel is 1.26∶1 after calcium treatment,the nozzle clogging does not happen and the consumption of calcium is reduced.The recovery factor fluctuation of boron are 64% and ±5×10-6, respectively.

通过硼微合金化若干工艺问题的解决和工艺优化，明确了钢水硫含量、增硅、铝控制之间的内在关系；使SPHC钢成分合格的同时，实现硼收得率达到64%，硼的质量分数波动±5×10-6；钙处理达到钢水中w∶w为1.26∶1时，确保水口浇注顺利，同时节省钙线用量。

The leftover from bamboo processing was comminuted into bamboo fine powder, which was surface-treaded with a coupling agent of ethenyl tri (β-methoxyethoxy) silane; and then in the presence of initiator dicumyl peroxide, the powder was compounded with styrene-isoprene block copolymer/bromobutyl rubber blend to prepare a crosslinked vibration-absorbing rubber composite material.

将竹加工的边角料粉碎并用乙烯基三硅烷偶联剂处理，再与苯乙烯－异戊二烯嵌段共聚物和溴化丁基橡胶的共混物进行复合，在过氧化二异丙苯引发剂的作用下制得交联型橡胶吸振复合材料。

A computer-aided local transient flow property measuring system was developed using a high speed CCD camera coupled with optical fibers in order to study the Gas-liquid-solid three-phase jet loop reactors. SnO2 crystal films were orientally deposited on the alkoxysilane molecule-coated hydroxyl glass substrates so as to prepare surface-marked particles as the tracers. An image analysis system was established to identify different phases. Stroboscopic photography was utilized to extend the measure range. The developed measuring and analysis system was capable of determining accurately the local transient flow property in a G-L-S jet loop reactor. Based on the above system, local transient flow properties of gas, liquid, and solid phase were measured and studied the influences of fluid property, operation and configuration parameters on the reactor.

中文摘要：以气液固三相喷射环流反应器为研究对象，将高速CCD和光纤束耦合制成局部瞬态流动特性微机数据采集及图象处理系统，利用MPS硅烷分子在带有羟基的玻璃基底上的自组装引导SnO2晶态膜层在功能化表面上进行沉积，以获得表面标记的示踪粒子，解决图象处理技术与相的识别的问题，利用频闪技术拓展了测量上限，得到可以准确测定气液固三相喷射环流反应器中局部瞬态流动特性的测试系统；采用上述测试技术进行喷射环流反应器中局部气相、液相与固相瞬态流动特性的实验研究，并考察物性参数、操作参数与结构参数的影响规律。

Two times hydrolyzation of Fe~(3+) and Cr~(3+) was firstly pointed out in the process of pillar preparation with hydrothermal method. In order to improve the thermal stability, Fe/Cr-Si-pillaring agent solution was synthesized by hydrolyzing Fe~(3+) and Cr~(3+) solution on the surface of silica sol, and Fe/Cr-Si-pillared montmorillonite (Fe/Cr-Si-PILM) was prepared with conventional method and hydrothermal method. Because the technical innovation of preparation is the best way to improve the PILM properties, two novel methods (Microwave method and Ultrasonication method) have been studied to synthesize Fe/Cr-PILM.In order to expand PILMs new application in the field of coal conversion, catalytic activity of Fe/Cr-Si-PILM catalyst in LongKou lignite and ShenHua coal residue liquefaction was discussed and characterized in the last part of this paper.

研究证明：蒙脱石的预处理是可行的，我们以预处理后的Ca-M为原料，研究并优化了PILM的水热法制备工艺，提出了金属离子的二次水解法；为了提高PILM的热稳定性，我们自制了硅溶胶，合成了Fe／Cr-Si三元复合柱化剂，并制备了Fe／Cr-Si-PILM；在PILM合成中，制备技术的革新是改进PILM性能的重要方法，为此我们探索了微波合成法和超声波合成法在制备Fe／Cr-PILM中的应用；最后，我们选择龙口褐煤和神华煤液化残渣为研究对象，探索了Fe／Cr-Si-PILM催化剂在煤炭液化中的应用，希望能开拓PILM应用的新领域。

The conversion of the high-boiling components and low-boiling components of silane to valu- able methylchlorosilane by catalytic cracking and disproportionation catalyzed by acid treated active carbon andγ-Al_2O_3 was studied.

用酸处理的活性炭和γ-Al_2O_3组成双段催化剂，通过有机硅高沸物和低沸物的裂解歧化反应制备了甲基氯硅烷，考察了反应温度、质量空速等因素对反应的影响。

The results indicated that effect of silicon carbide or sodium silicate on inhibiting crystallization of fused quartz was not obvious,5wt% boric a.

以粒径。16mm的熔融石英颗粒为原料，以硼酸、碳化硅、氮化硅、水玻璃为晶化抑制剂，以聚乙烯醇(浓度1%)为结合剂，试样成型压强为20MPa，试样经1200℃保温2h烧成，对烧后试样进行1500℃保温1h的强化脱玻处理、RT～1300℃的差热分析以及RT-1300℃的热膨胀测定。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。