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Moreover, it was successfully linked with lactobionic acid through amine groups on the surface of particles, and used to recognize living liver cells successfully.(3) In order to simplify the proceeding of preparation of silica-coated qdots, a novel one-pot method using 3-mercaptopropyl-trimethoxysilane as a capping molecule was proposed for the first time. Furthermore, amine and phosphonate groups were also modified on the surface of silica-coated qdots simultaneously. This was the first time the synthesis and the surface modification of qdots were performed in the same system.

3在前一部分工作的基础上,进一步简化量子点的合成与包壳步骤,以MPS为稳定剂,制备了硅壳包被的CdTe量子点,并在硅壳外同步修饰氨基及磷酸基团,首次成功实现了量子点的合成与表面的功能化修饰在同一体系中进行,从而制得了水溶性的、表面带有氨基和磷酸基团的硅壳型CdTe量子点。

The rubber compound comprises a rubber which has at least two functional groups which can be cross-linked by hydrosilylation, a cross-linking agent consisting of hydrosiloxane or a hydrosiloxane derivative or a mixture of several hydrosiloxanes or derivatives, which comprise at least two SiH-groups per molecule in the centre, a hydrosilylation catalyst system, at least one filling material and a coagent which can be cross-linked by hydrosilylation.

为此该橡胶混配物包括:具有至少两个可通过氢硅烷化交联的官能团的橡胶;作为交联剂的氢硅氧烷或氢硅氧烷衍生物或者由数种氢硅氧烷或其衍生物组成的混合物,所述氢硅氧烷或其衍生物平均每个分子具有至少两个SiH基团;氢硅烷化催化剂体系;至少一种填料;和可通过氢硅烷化交联的助剂。

Silicon powders were mixed with pore-forming agent of 30wt% and agglomerant of 1wt% and shaped into discs of Φ70 mm×5 mm by mould pressing under pressure of 40 Mpa.

通过添加30wt%的成孔剂颗粒,制备出孔隙率在55%左右的具有宏观球形孔的多孔氮化硅陶瓷。反应烧结前,在低于硅熔点的温度下,对多孔硅坯体进行不同温度和不同时间的预烧。

Novel organic silane of 3,3′-dihydroxyldiphenoxydimethyl alkoxy silane and 3,3′,3-trihydroxyldiphenoxydimethylalkoxy silane triglycidyl ether for epoxy resin modification were synthesized.

研究了含酚羟基有机烷氧基硅烷及3,3′,3-三羟基苯氧基硅烷三缩水甘油醚两种新型有机硅改性剂对双酚F环氧树脂力学性能及热性能的影响。

This paper is studied on a new synthesis method of amino-modified organic silicone micro-emulsion of cationic style by one step with a silane-alkyl coupling,3-(2-aminoethyl)-aminopropyl methyl dimethoxy silane while opening-cyclo polymerization of the octa-methyl cyclo tetra siloxane,thus the optimal manufacturing conditions are determined by comparing test of their properties.

采用硅烷偶联剂氨乙基氨丙基甲基二甲氧基硅烷改性,八甲基环四硅氧烷开环聚合,探索一步合成阳离子型氨基改性有机硅微乳新方法,通过其性能测试得出其最佳工艺条件:反应温度:80℃,反应时间:3 h,十六烷基三甲基溴化铵用量:5%,脂肪醇聚氧乙烯醚用量:5%,预乳液滴加时间:2 h。

Use D4 or DMC, Divinyl tetramethyl disiloxane, Tetravinyl tetramethyl cyelo tetrasiloxane were used as raw materials and Tetramethyl ammonium hydroxide as catalyst to synthesize a high molecular weight of vinyl silicone oil. Concentrate hydrosilicone oil, tetramethyl dihydro disiloxane, hexamethyldisiloxane and D4 were used to synthesize the cross linker of low-hydro silicone oil required in experiments.

以D4或DMC,乙烯基双封头,乙烯基环体等为原料,四甲基氢氧化铵为催化剂合成了不同摩尔质量的乙烯基硅油;以高含氢硅油,含氢双封头,六甲基二硅氧烷,D4合成实验所需的交联剂低含氢硅油。

The concentration of liquid hydrocarbon B is 10%.the dosage of hydrophobe is 15%~20%. The condensation and used environment of defoaming agent were studied ,the experiments show that self-made defoamer can be the same with many bubbly systems,such as anion, zwitterions, Nonionic bubbly liquid et al.and it can be used from acidity to alkalescence conditions.the fitting dosage is 9‰~10‰to polyester,6‰to siloxane-polyester copolymer,and 3‰to mulriple defoamer.

对消泡剂的投加浓度、适用环境等作了相关应用研究,结论为:消泡剂适用的起泡体系较广,阴离子、两性离子、非离子型起泡液均可使用;适用PH值范围可从酸性至弱碱性,适宜加入量为(以占起泡体系的体积分数计):聚醚酯消泡剂9-10‰,有机硅改性聚醚酯消泡剂6‰,复配消泡剂3‰。

The experimental results shows, if the ratio between MS-1 and OP-10 rangs from 1:1 to 3:l,and the total dosage of them is about 20% of Octamethylcyclotetrasiloxane (D4 ) in quality, we can obtain a kind of stable seeded emulsion of organic silicone modified acrylic ester emulsion. At the same time, if the ratio between MS-1 and Tetramethylammonium Chlorideis l:1.7,the total dosage is about 50% of D4 in quality; the ratio between MS-1 and Cetyltrimethylammonium Chlorineis 7:1, the total dosage is about 25% of D4 in quality,we can also obtain stable seeded emulsions. But if the complex emulsifier system is made of TMAC and OP-10, MS-1 and Peregal O or CTAC and Span-80, we can not synthesize any kind of satisfactory seeded emulsions.

实验结果表明:当MS-1与OP-10的质量比为1:1~3:1,总用量为八甲基环四硅氧烷(D_4)的20%左右时,可合成稳定性良好的硅丙种子乳液;MS-1与四甲基氯化铵的质量比为1:1.7,总用量为D_4的50%左右,MS-1与十六烷基三甲基氯化铵的质量比为7:1,总用量为D_4的25%左右时,亦能得到稳定的硅丙种子乳液;而TMAC与OP-10、MS-1与Peregal O以及CTAC与Span-80的复合体系作为乳化剂时均不能得到满意的硅丙种子乳液。

In order to prevent this kind of pollution, often spreads the organosilicon water-repellent, the polymer cement mortar, the emulsion resin, the epoxy resin etc on the inside surface of the quartz stone , although it can have certain protection effect, but also has the following insufficiency: Uses organosilicon water-repellent processing, the quartz stone material, cement and the mortar cannot form a sealed surface layer, is unable to suppress the hoar frost separation and the rain spot effectively; Uses polymer cement processing, not only material itself includes the hoar frost ingredient, moreover the water permeability is big, the protection effect is also not ideal

为防止这类污染,常在石材内面涂上有机硅防水剂、聚合物水泥砂浆、乳液树脂、环氧树脂等,虽能收到一定的防护效果,但也存在以下不足:采用有机硅防水剂处理,石材与砼、砂浆被贴面不能形成密封层,无法有效抑制白霜析出物和润斑;采用聚合物水泥处理,不仅材料自身含有白霜成分,而且水渗透率大,防护效果也不理想

The results showed that the wheat-straw powder had little reinforcing effect on NR,but had good filling effect;when the wheat-straw powder was modified by sodium hydroxide solution,silane coupling agent KH-550 or its solution,the physical properties of wheat-straw powder/NR composite were improved;the silane coupling agent KH-550 solution possessed better modifying effect.

结果表明,小麦秸秆粉末对NR无明显补强作用,但具有良好的填充作用;采用氢氧化钠溶液、硅烷偶联剂KH-550或其水溶液对小麦秸秆粉末进行表面处理,均可改善复合材料的物理性能,其中硅烷偶联剂KH-550水溶液的效果较好。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力