硅剂

Titanium incorporated mesoporous molecular sieves Ti-MCM-41, Ti-HMS, and Ti-MSU were synthesized through S〓I〓, S〓I〓, and N〓I〓 pathways using cetylpyridium bromide, tetredecylamine, and polyoxyethylene (10) stearyl ether as the structure-directing agents, respectively. The framework structure and the titanium coordination environment of these materials were characterized by XRD, N〓 adsorption/desorption, TG, TEM, FT-1R, DR UV-Vis, and ICP-AES. It was confirmed that the titanium was highly dispersed in the silica-based framework positions, and all samples were free of extra framework titanium impurities. The catalytic performance of these titanium containing mesoporous materials was investigated in the oxidation of styrene with aqueous H〓O〓 as the oxidant.

以TEOS和TBOT为硅源和钛源，分别以溴代十六烷基吡啶、十四胺和十八烷基聚氧乙烯基醚为模板剂，通过S〓I〓、S〓I〓和N〓I〓方式合成了含钛的介孔分子筛Ti-MCM-41、Ti-HMS和Ti-MSU，用XRD、N〓吸附/脱附、TEM、FT-IR、DR UV-Vis和ICP-AES等方法对它们的骨架结构、孔道结构以及钛原子的存在方式等进行了系统表征，结果表明钛原子以高分散的形式存在于以SiO〓为基本单元的介孔分子筛的骨架结构中，制备过程中未形成聚集态的骨架外金属氧化物物种。

Based on seed-emulsion polymerization, the stable silicon-acralyte core/shell latex with little coagulum were synthesized at lower temperature with potassuim persulphate, sodium formaldehyde sulfoxylate and V-044 as composite initiators.

选用过硫酸钾、甲醛合次亚硫酸氢钠和2， 2'-偶氮二[2-（2-咪唑啉－2-代）丙烷]二氢氯化物(V-O44)为复合引发剂，在低温下通过种子乳液聚合技术合成了生成凝聚物少的硅－丙核／壳乳液。

Water samples were extracted and purified and collected by solid-phase extraction LC-18 column. Soil samples were extracted by ethyl acetate/petroleum ether (2:1, by vol) and purified by sulphonation. Wheat sample was extracted by acetonitrile/water (4:1, by vol) and purified and collected by SPE- Florisil column.

水样直接用LC-18固相萃取小柱分离、净化和富集；采用乙酸乙酯／石油醚（体积比2：1）振荡提取，磺化法净化，测定土壤中氯氟吡氧乙酸残留量；以乙腈／水（体积比4：1）为提取剂，氟罗里硅土固相萃取小柱分离、净化，测定小麦样品中氯氟吡氧乙酸的残留量。

Objective To evaluate the therapeutic effect and safety of heavy silicone oil used as internal tamponade to treat complicated retinal detachment.

目的 评价重硅油作为眼内填充剂治疗复杂性视网膜脱离的有效性和安全性。

A series of tri-block copolymers of styrene/tetradecyl methyl acrylate/3-methacryloxyl-propyl thimethoxyl silane was synthesized by atom transfer radical polymerization. The structures of those copolymers were characterized by means of gel permeation chromatography, infrared spectrum, and nuclear magnetic resonance (1H-NMR). Effect of tri-block copolymers on the mechanical properties of glass fiber/polypropylene composites was also investigated.

采用原子转移自由基聚合法合成了一系列新的三嵌段共聚物大分子偶联剂聚苯乙烯－b-聚甲基丙烯酸十四酯－b-聚3-甲基丙烯酰氧基丙基三甲氧基硅烷，通过凝胶渗透色谱、红外光谱和核磁共振(1H-NMR)证实了其结构，并研究了其对玻璃纤维／聚丙烯复合材料力学性能的影响。

Mercaptopropyl methyldimethoxysilane was synthesized by thiourea in the presence of tetramethylammonium iodine as a catalyst and mixed liquid containing ethylenediamine and trichloroethylene as a neutralizer, without solvent, in which the reaction temperature, catalysts ,neutralizer and their amounts were optimized.

以四甲基碘化铵为催化剂，乙二胺和三氯乙烯的复合液为中和剂，在无溶剂体系中，用硫脲法合成了甲基巯丙基二甲氧基硅烷。

The chemical adsorption model of titanite on the surface of finely calcium carbonate was established according to the properties of finely calcium carbonate and titanite and the mutual action mechanism.

硬脂酸钠、钛酸酯和铝酸酯对重质碳酸钙的改性与钛酸酯对硅灰石的改性导致改性剂在矿物表面的反应吸附，吸附以化学吸附为主，物理吸附为辅。

A series of modified polyurethane elastomer materials with different amino siloxane content were synthesized,which were based on polyoxypropylene glycol,aminoethyl aminopropyl poly,toluene diisocyanate and the curing agent dimethylsulfide toluylenediamine.

以聚氧化丙烯二醇或聚氧化丙烯三醇、氨乙基氨丙基聚二甲基硅氧烷、甲苯二异氰酸酯为原料在无溶剂条件下制备预聚体，利用二甲基硫甲苯二胺为固化剂合成一系列氨基硅油改性聚氨酯弹性体材料，并对材料的力学性能、耐热性、表面水接触角等性能进行了测试。

The company mainly produces surfactant, triethanolamine, printing and dyeing auxiliaries, silicone defoamers.

公司主要生产表面活性剂、三乙醇胺、印染助剂、有机硅消泡剂。

Using trimeric surfactant C_(14-2-14-2-14) as templating agent, the low cost and facile inorganic species sodium aluminate and sodium silicate as inorganic precursors, highly ordered 2D hexagonal aluminosilicate MCM-41 with high Al content were successfully synthesized.

利用廉价易得的硅酸钠和偏铝酸钠作为无机前驱体，以低聚季铵盐表面活性剂C_(14-2-14-2-14)为模板剂合成了高铝含量，高有序性的二维六方结构介孔硅铝酸盐材料，并对材料的结构、表面性质、形貌以及酸性进行了研究。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。