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Compound 1 and 2 are pure tungstosilicate cluster,the others are transition-metal tungstosilicate clusters All compound characterized by elemental analyses,IR,TG,and single-crystal X-ray diffraction..

其中,前两个化合物为纯钨簇,后三个化合物为含有金属的钨簇。所有的化合物都通过元素分析,IR,TG和单晶X-射线分析进行了表征。另外,对于化合物3、4和5,我们还对其电化学性质进行了研究。

Nickel oxide supported silica-pillared zirconium phosphates with high surface area have been prepared successfully by directly loading Ni〓 to uncalcined APS intercalate of α-ZrP followed by calcination.

1采用将金属盐直接负载到未焙烧的α-ZrP的胺丙基脂嵌入物上,然后再焙烧的方法,制备了大比表面负载氧化镍的柱磷酸锆。

The factors of temperature and humidity influenced on film thickness and order of layer were studied, in which pulling speed and pulling times were also included. It showed that the thickness of single dip-coating film reached 0.23 μm ~ 0.625 μm, and the degree of order of surface layer were still holding much higher.b Adopting calcined or uncalcined mesoporous silica membrane as matrix, nano zirconia particles were assembled through ion exchange method and ion-template exchange method.

结果表明,单次提拉膜膜厚0.23μm~0.625μm、8次提拉后表层膜仍有一定的有序性; b以自制的介孔氧化煅烧/未煅烧厚膜样为基体,采用离子交换法/离子模板交换法组装锆氧纳米粒子,选用DSC-TG、FT-IR、Uv-vis、SAXRD等对不同组装方法、锆源浓度、pH值等组装条件下ZrO_2/介孔氧化厚膜组装效果进行评价。

Sequential leaching experiments indicate fluorine in carbonate rock, phosphorite and Mo-Ni ore layer occurs principally in dissolvable forms: water-soluble, associated with carbonate or phosphorite, so fluorine in which rocks have high chemical mobility at surface conditions. Fluorine in siliceous rock, black shale and carbonaceous slate mainly occurs in undissolvable forms, which are inert at surface conditions.

氟在碳酸盐岩、磷块岩、钼、镍等多元素富集层及部分质岩中主要以水溶态、碳酸盐结合态等易溶形式存在,其在自然条件下的化学活动性强;而氟在碳质板岩、黑色页岩及大部分质岩中主要存在于难溶矿物中,其化学活动性较弱。

It has been warranted through experiments and practical application that rare-earths-high-aluminium heat-resistant nodular iron has some intrinsic properties which are worthy of reconimandation, namely,that it will not scale after long periods of use at 1050-1100℃, will hardly break while being hammered into castings, runners or risers as the high-temperature tensile strength reaches 14-19 kg/mm2 at 800℃ or≥l3.3kg/mm2 at 900℃, with the room temperature strength close to HT 30-50 and the unnotched impact str...

本文介绍了稀土高铝耐热球墨铸铁的生产实践、化学成分;探讨了稀土作用及其用量和控制;论述了稀土和铝加入方式以及冷却速度对金相组织的影响;并对铸造工艺、铸件缺陷及分析、耐热性能及使用效果作了阐明。试验和使用证明:稀土高铝耐热球墨铸铁在1050~1100℃长时间工作不起氧化皮,热强度800℃时,14~19kg/mm~2,900℃时≥13.3kg/mm~2,室温强度近于HT30—54,a_k≈2~6kg·M/cm~2,锤击铸件或浇冒口,很难碎裂,并能机械加工。可以认为是以我国富产资源为原料,能用各种炉子熔炼、耐热和综合机械性能均较高、中中铝球铁、高铝片墨铸铁为高的一种耐热铸铁,也是镍铬系耐热材料较好的替代品。

The Si-rich SiO2/p-Si structure has been fabricated with two-target alternative magnetron sputtering technique.After the Si-rich SiO2/p-Si sample having been scored by diamond tip on the front surface and annealed at 800℃ in N2 the photoluminescence spectrum is found quite different from that from the unscored one,which having been annealed in the same condition.

以磁控溅射方法于p-Si上淀积富二氧化,形成富二氧化/p-Si结构,用金刚刀在其正面刻划出方形网格后在N2气氛中退火,其光致发光谱与未刻划的经同样条件退火的对比样品的PL谱有很大不同。

NMOSFET devices are fabricated and measured in strained-Si and unstrained bulk-Si channels.

分别在应变和无应变的体沟道上制作了nMOSFET器件,并对它们进行了测量。

Furthermore,it is found that the stress in the strained Si cap layer is maintained even after the high thermal budget process.nMOSFET devices are fabricated and measured in strained-Si and unstrained bulk-Si channels.

分别在应变和无应变的体沟道上制作了nMOSFET器件,并对它们进行了测量。

The effect of electrolyte additive of vinylene carbonate on the SEI layer properties was investigated in details.

VC添加剂大大提高了薄膜的循环性能,薄膜的200次循环容量保持率在常规电解液中为25.6%,在功能电解液中提高到78.5%。

Wacker Silicones is a leading supplier of complete silicone-based solutions that comprise products, services and conceptual approaches.

瓦克有机是提供从产品、服务到理念的全球主要的有机解决方案的供应商。

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