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The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域,涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料,用偏硅酸钠的水溶液在30~60℃反应10~300分钟,使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片,加入模板剂十六烷基三甲基溴化铵,然后调节母液pH值为10~12,老化1~8小时,然后加入高压釜于80~130℃进行水热合成反应。反应24~72小时后,分离出固体,水洗、干燥,然后于500~600℃焙烧5~10小时,得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料,所合成的材料经过质子交换可以具有较强的酸性,在吸附和催化领域具有广泛应用前景。

From the pyrolyzed product at 200℃ of Gephyrocapsa oceanica a group of C〓 dicycle terpenoids were firstly identified. They were highly instable and sensitive to temperature because they can only generate at 200℃ and segregate or transform at higher temperature. Therefore they can not only be an indicator of special temperature of organic matter originated from G. oceanica, but can be used to distinguish organic matter from G. oceanica before the hydrocarbon generation peak.

在近海颗石藻Gephyrocapsa oceanica 200℃产出的饱和烃中首次检出了一组C〓二环萜类化合物,这一组特殊的C〓二环萜类化合物在颗石藻来源的有机质中是高度不稳定和温度敏感的,因为它们只在200℃时才形成,更高的温度条件下便解离或转化了,因此,它们既可以是近海颗石藻Gephyrocapsa oceanica来源有机质的特定温度条件的指示,又可以被用于判识该藻类在成烃高峰到来前所形成的有机质。

By way of description of those unfortunate women's fate, Isikawa Tatsuzo makes a severe disclosure and critique about the cultural tradition of male hegemonism in Japanese society. Furthermore, he also expresses heartfelt sympathy for those women in difficult position. Isikawa Tatsuzo knows that women face a dilemmatic condition between family and society, he also wants to look for a way for women to exist. All of these express his positive view on women.

石川达三通过对其笔下女性不幸命运的描写,深刻地揭露与批判了日本社会中普遍存在的男性霸权主义文化传统,并对那些身陷困境的女性寄予了深切的同情;石川达三看到了女性被困于家庭及社会中的两难地位,而且积极地想要为她们寻找一条生存之路,这些都表明了石川本人的女性观中需要肯定的积极一面。

LREE depleted spinel lherzolite xenoliths are the 2%~15% partial melting residues of spinel lherzolite with 2 times REE concentration of chondrite. LREE enriched spinel lherzolite xenoliths are the prodiuct that 1% partial melting of garnet lherzolite derived melts mix in ratio of 2% with most LREE depleted spinel lherzolite.

轻稀土亏损的尖晶石二辉橄榄岩包体,是2倍球粒陨石稀土元素丰度的尖晶石二辉橄榄岩地幔经过2%~15%部分熔融后的残留体;而富集型尖晶石二辉橄榄岩包体可能为,来自深部石榴石二辉橄榄岩源区1%熔融形成的熔体以约2%的比例隐交代轻稀土元素最亏损的包体代表的幔源区后形成的。

The signals look like noncontinuous beads on the DNA fiber,which consist of multi-copy and arrange tandemly.Fiber-FISH results with 45S rDNA probe showed that an average signal length is about 3~11μm in many tandem copy sequence(measure number,n=8),so we estimated the size of each copy to be approximately 11~30kb in cotton genome.There are dual signals on each end of the mitosis metaphase chromosomes and pachytene chromosomes hybridized with telomere DNA probe.The signals also look like non-continuous beads on the DNA fiber,the length is about 1~9μm,so we estimated the size is about 4~27kb.The signals almost covered the whole mitosis metaphase chromosomes and pachytene chromosomes of G.arboretum Shixiya 1 hybridized with gDNA probe,the euchromatin zone and heterochromatin zone were identified clearly on pachytene chromosomes,and the signals also look like non-continuous beads.Two BAC clones 150-D-24 and 182-F-9 in DNA BAC library of Pima90 were selected as probe to hybridize with mitosis metaphase chromosomes,pachytene chromosomes and DNA fiber of G.raimondii.

棉花FISH技术系统的应用研究。45S rDNA在亚洲棉石系亚1号中期和粗线期染色体上有两对大的信号,在DNA纤维上信号为非连续的念珠状,多个拷贝串联排列,每个拷贝长度大约在3~11μm,推测每个拷贝的实际长度为11~30kb;端粒序列在亚洲棉石系亚1号中期和粗线期染色体端部都有双点信号,在DNA纤维上信号也为非连续的念珠状,不同染色体上信号长度大约在1~9μm不等,推测实际长度为4~27kb;gDNA信号几乎布满整个亚洲棉石系亚1号中期和粗线期染色体,在粗线期染色体上能明显区分出常染色质区和异染色质区,DNA纤维上的信号均为非连续的念珠状。

Under optical microscope,the observational result indicates that the peach blossom stone samples from Gao Mountain contains transparent and distransparent minerals which forms pealike and red spots.

光学显微镜的观察结果表明,高山桃花石样品中存在透明和不透明矿物,其中不透明矿物形成了艳丽的红色斑点;XRD测试表明,样品的矿物组成为地开石、赤铁矿、石英以及少量的叶腊石;拉曼光谱测试结果表明,样品的基质部分为地开石,结晶形态完好的红色矿物颗粒与呈浸染状的红色部分均为赤铁矿,无色透明的矿物颗粒为石英。

Under optical microscope, the observational result indicates that the peach blossom stone samples from Gao Mountain contains transparent and distransparent minerals which forms pealike and red spots. The XRD testing result indicates that the mineral compositions in the samples are dickite, hematite, quartz and a little pyrophyllite. LRM testing result shows that the basic part of the samples is dickite, the red minerals with both well crystal shape and dip dye shape are hematite, and colourless and transparent mineral grains are quartz.

光学显微镜的观察结果表明,高山桃花石样品中存在透明和不透明矿物,其中不透明矿物形成了艳丽的红色斑点;XRD测试表明,样品的矿物组成为地开石、赤铁矿、石英以及少量的叶腊石;拉曼光谱测试结果表明,样品的基质部分为地开石,结晶形态完好的红色矿物颗粒与呈浸染状的红色部分均为赤铁矿,无色透明的矿物颗粒为石英。

Co-firing characteristics of corn stalk and stone coal in different proportion were investigated by thermal gravimetric analysis. The results showed that corn stalk can improve the ignition and combustion of stone coal. The agglomeration experiments on corn stalk were made in a bench-scale bubbling fluidized bed with quartz sand as bed material and stone coal ash as additive. The results indicate that stone coal ash can inhibit agglomeration of bed material particles at temperature of 900℃. Agglomerate of blends was analyzed by means of scanning electron microscopy, energy-dispersive X-ray, and the bed materials were analyzed by means of X-ray fluorescence. Analysis showed that aluminum element and iron element in stone coal ash can react with alkali compounds and eutectics with low melting point, form a covering layer with high melting point on the surface of biomass and quart sand particles, thus inhibit the forming and transfer of low melting compounds.

以玉米秸秆与石煤按不同比例组成的混合物为研究对象,在TG-DTG热分析仪上进行了燃烧特性分析,结果表明玉米秸秆有利于石煤的着火和稳定燃烧,对石煤有一定的助燃作用;在小型鼓泡流化床实验装置上,以石英砂为床料、石煤灰为添加剂,进行了玉米秸秆成型燃料流化床燃烧的床料黏结实验,结果表明:石煤灰能够在生物质流态化燃烧过程中有效地抑制流化床床料黏结现象的发生;通过对实验中形成的结团进行扫描电子显微镜X射线能谱(scanning electron microscopy/Energy-dispersive X-ray- SEM/EDX),对床料进行X射线荧光光谱(X-ray fluorescence,XRF)分析,结果表明石煤灰中的Al和Fe能够与生物质灰中的碱金属化合物以及低熔点共熔物发生化学反应生成高熔点物质,并且覆盖在生物质碳颗粒与石英砂颗粒表面形成隔绝层,从而阻止低熔点物质的生成与迁移。

Diversity of soil surface, stone gully and stone pit is 1.199, 1.592 and 1.962; evenness index of soil surface, stone gully and stone pit is 0.616, 0.989 and 1.095; dominance of soil surface, stone gully and stone pit is 0.545, 0.353 and 0.245 in soil macrofauna community structure.

土面生境土壤动物的多样性指数为1.199,石沟的为1.592,石槽的为1.962;均匀性指数为0.616,石沟的为0.989,石槽的为1.095;土面生境土壤动物的优势度为0.545,石沟的为0.353,石槽的为0.245。

Diversity of soil surface, stone gully and stone pit is 1.199, 1.592 and 1.962; evenness index of soil surface, stone gully and stone pit is 0.616, 0.989 and 1.095; dominance of soil surface, stone gully and stone pit is 0.545, 0.353 and 0.245 in soil macrofauna community structure.

土面生境土壤动物的多样性指数为1.199,石沟的为1.592,石槽的为1.962;土面生境土壤动物的均匀性指数为0.616,石沟的为0.989,石槽的为1.095;土面生境土壤动物的优势度为0.545,石沟的为0.353,石槽为0.245。

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