石油醚

From Cacalia deltophylla (collected from Luqu County, Gansu Province), 22 compounds were isolated, of which 15 compounds have been identified. Among them, two compounds are new. They are named as 3-methyl-4-hydro-8-acetyl-furanonaphth-9-one and 1hydroxy-2-methoxy-3-acetyl-4, 8-dimethyl-5, 8-dihydro-naphthalene.

从采自甘肃省碌曲县的三角叶蟹甲草全草的甲醇提取物的石油醚部分和乙酸乙酯部分中，采用同样方法分离得到22个化合物，鉴定了其中的15个化合物，其中有2个为新化合物，分别命名为3-甲基-4-氢-8-乙酰基-呋喃萘-9-酮（2）和1-羟基-2-甲氧基-3-乙酰基-4，8-二甲基-5，8-二氢-萘（3）。

Methods Using petroleum ether to extract crude fat from the Capparis spinosa fruit and identify separately with GC-MS method after methanolysis.

方法］用石油醚提取刺山柑果实中的粗脂肪，甲酯化后，用GC-MS法进行分离鉴定。

Wax ester was synthesized from soybean oil and cetyl alcohol in a packed-bed reactor with petroleum ether as solvent and immobilized lipase Candida sp.99-125 as catalyst.

以大豆油、十六醇为原料，在石油醚体系中，使用实验室自制的固定化Candida sp.99-125为催化剂。

Chondrus ocellatus was extracted by methanol, ethanol, ethyl ether, ethyl acetate, petroleum ether and acetone, respectively.

采用甲醇、乙醇、乙醚、乙酸乙酯、石油醚、丙酮6种溶剂分别对角叉菜进行冷浸提取。

The anti-microbial activity of active materials against valsa mail,fusarium oxysporum,coniothyrium diplodieua and aspergillus nidulans were measured in vitro.the results showed that active materials extracted using acetone,aether and petroleum ether presented fungistasis to different extent on the four pathogenic fungi and had the best effect to coniothyrium diplodieua.active material extracted using ethanol presented certain anti-microbial effect to fusarium oxysporum.the results also showed there were anti-microbial active material in the leaves of cichorium intybus and founded a base on the research and application.

然后以提取液为供试药剂，对苹果腐烂病菌、棉花枯萎病菌、葡萄白腐病菌、构巢曲霉病菌4种植物病原真菌进行离体活性测定。结果表明：丙酮、乙醚、石油醚的提取液对4种病菌均有不同程度的抑制作用，其中对葡萄白腐病菌抑制效果最好；乙醇的提取液对枯萎病菌具有一定的抑制作用。表明菊苣叶中存在抑菌活性成分，补充了菊苣抑菌活性的研究内容，为该种植物抑菌活性成分的研究和应用奠定基础。

Methods Two sesquiterpenoids were isolated from the resinous exudates of Commiphora opobalsamum.

方法没药石油醚提取部分经硅胶柱层析分离得到二十多个倍半萜类化合物。

The invention discloses a method for extracting polysaccharide from chiretta and an application, which comprises breaking dry chiretta via a breaker into powder, arranging into an extraction pot, adding ligarine to reflux and defat, adding distilled water into defatted residues to extract, processing alcohol precipitation and centrifugation to obtain deposits, removing protein, processing acid hydrolysis and gel chromatography separation, freezing and drying to obtain active chiretta polysaccharide.

本发明公开了一种从当归中提取多糖的方法及应用。干燥当归用粉碎机粉成粉末，置入提取罐中，加入石油醚回流脱脂，向脱脂后的残渣中加入蒸馏水提取，醇沉、离心得沉淀，除去蛋白、酸解、凝胶色谱分离、冷冻干燥得到活性当归多糖。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂，甲醇为溶剂的回流提取法来提取植物多酚，用显色反应检识酚羟基；采用紫外分光光度法对多酚粗体物进行总多酚含量的测定；选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌，采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验，并测定其最低抑菌浓度；采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析，根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

Methhods:1:The chemical components of Chinese herbal medicines extracted with petroleum ether,chloroform, ethyl acetate,ethenol and water respectively were analyzed and compared.2.The specimens were analyzed with ultraviolet-visible absorption spectrophotometry.

(1)按中药多分子体系的脂溶性差异，分为石油醚、氯仿、乙酸乙脂、乙醇和水的溶出性成分集合，然后进行&对药&与非&对药&的对比分析；(2)用紫外-可见光光度计测定吸收光谱曲线。

The hypha growth-inhibiting method and the virulence determination method were used to investigate the inhibition effects of the petroleum ether fraction, chloroform fraction, ethyl acetate fraction, n-butanol fraction and water fraction in the alcoholic extracts from the aboveground of Peganum harmala L.

采用抑制菌丝生长法和毒力测定法，研究了骆驼蓬地上部醇提物的石油醚、氯仿、乙酸乙酯、正丁醇和水5个极性部位对南瓜枯萎病菌、西瓜枯萎病菌Fusarium oxysporum f。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了