石油醚

An aliquot of the alcohol solution was taken and further extracted with petroleum ether.

分取部分此乙醇溶液用石油醚萃取，使叶绿素溶入石油醚中。

Compareing with essential oil of the steam distillation method and the bensine solvent extraction method through GC-MS analysis .The result showed that:the essential oil principal constituent extracted by benzine is camphene,a-pinene,bornyl acetate, limonene, 1-methyl-4-(1-methylethyl)-1,4-cyclohexadiene, myrcene, caryophyllene, borneol.

对巴山冷杉针叶水蒸气蒸馏和石油醚萃取所得精油的GC-MS 分析对比研究结果表明：石油醚萃取精油主要成分为：莰烯，a-蒎烯，乙酸龙脑酯，柠檬烯，1-甲基-4-异丙基-1，4-环己二烯，月桂烯，石竹烯，龙脑。

Results: The extracts of ethanol, petroleum ether and ethyl acetate of Rhizoma Amorphophalli have inhibitory effect on the proliferation of cell SGC-7901, and the extract of petroleum ether has much more evident effect, showed a dose-effect curve.

结果：蛇六谷醇提取物、石油醚萃取物和乙酸乙酯萃取物均具有一定的抑制人胃癌SGC-7901细胞增殖的作用，以石油醚萃取物的抑制作用最为明显，呈现较好的剂量－效应曲线。

And the results of Friedman-test on these two correlation models of Ash,Nicotine,PEE,PEEN were 1.24,1.83,1.67,4.63 respectively,which indica...

两类近红外预测模型对灰分的预测没有显著性区别，而对尼古丁、石油醚提取物、石油醚提取物中性成分的预测有显著性区别。

Essential oil was extracted from the petroleum ether-soluble fraction of the leaves showed having antibacterial activity. It was demonstrated that the essential oil has significant antibacterial activity and the activity of the petroleum ether-soluble fraction is attributed to it. The constituents of the essential oil were analysized by GC-MS.10 relatively abundant components were identified on the basis of MS, among which Geranlgeraniol was found in the essential oil of Perilla frutescens leaves for the first time.

对具有抗菌活性的紫苏叶石油醚萃取物进一步精制，从中提取出挥发油，通过抗菌测试证明紫苏叶挥发油具有良好的抗革兰氏阳性菌和革兰氏阴性菌活性，是紫苏叶石油醚萃取物抗菌活性的来源；采用GC-MS对紫苏叶挥发油进行了成分分析，得到10种含量较高的主要化合物，其中的牻牛儿基牻牛儿醇首次在该植物挥发油中被发现。

objective to observe the antitumor activities of different solution extracts of plumbago zeylanica l.in vitro.method mtt method was used to detect the inhibitory effects on four kinds of cancer cells.results chloroform extracts had significant inhibitory effects on the breast cancer cell(bre-04),the nerve cancer cell(n-04) and the lung cancer cell(lu-04),ic50 were 0.2699mg/ml and 0.2634mg/ml,0.4961mg/ml respectively.ic50 of chloroform extract on the hepg2 was 0.9379mg/ml.ic50 of petroleum ether extracts on bre-04,n-04,lu-04 and hepg2 was 0.5902mg/ml,0.5725mg/ml,0.7938mg/ml,0.6374mg/ml;ethyl acetate extracts had fairly inhibitory effects on the lu-04,ic50 was 0.7343mg/ml;n-butanol extracts and water-solubility extracts had notsignificant inhibitory effects on the four kinds of cancer cells.conclusion the antineoplastic effective parts of plumbago zeylanica l.were chloroform and petroleum ether extracts.

目的 探讨白花丹体外抗肿瘤作用的活性部位。方法 mtt染色法对白花丹五种溶剂提取物体外抗肿瘤活性进行了初步的研究。结果氯仿提取物对乳腺癌细胞（bre-04）、神经癌细胞（n-04）、肺癌细胞（lu-04）有较好的抑制生长作用，ic50分别为0.269 9 mg/ml、0.263 4 mg/ml、0.496 1 mg/ml，对肝癌细胞hepg2抑制作用差， ic50为0.937 9 mg/ml；白花丹石油醚提取部位对乳腺癌细胞（bre-04）、神经癌细胞（n-04）、肺癌细胞（lu-04）、肝癌细胞hepg2的ic50分别为0.590 2 mg/ml、0.572 5 mg/ml、0.793 8 mg/ml、0.637 4 mg/ml；乙酸乙酯提取物对肺癌细胞（lu-04）有一定的抑制作用，ic50为0.734 3 mg/ml；水溶性提取物以及正丁醇提取物无明显抑制肿瘤作用。结论白花丹氯仿提取部位、石油醚提取部位体外抗肿瘤作用较好，值得对其提取部位进一步分离纯化并研究其抗肿瘤作用机制。

And Cucumis sativus L. were tested by bioassay-guided separation. The extracts from P. tomentosa flower with ethanol were extracted with petroleum ether, ethyl acetate and n-butanol. The inhibition rate of the ethyl acetate extract to growth of the 3 kinds of plant radicel were 99.89%, 63.53% and 32.74% respectively at 0.5 mg/mL concentration, and that of petroleum ether were 76.30%, 56.17% and 23.36%.

绒叶泡桐Paulownia tomentosa花乙醇提取物依次用石油醚、乙酸乙酯、正丁醇和水萃取后进行活性测定，结果表明，石油醚萃取物在浓度为0.5mg/mL时，对反枝苋、生菜和黄瓜种子胚根生长的抑制率分别为76.30%、56.17%和23.36%；乙酸乙酯萃取物在浓度为0.5mg/mL时，对反枝苋、生菜和黄瓜种子胚根生长的抑制率分别为99.89%、63.53%和32.74%。

Our results showed that the mortality from petroleum ether extract of Inula britanica; Ricinus communis methanol ether extract; Photinia serrulate petroleum ether extract after treatment, which showed significantly higher acaricidal activities than the other ones in the concentration of 2 mg/ml.

结果表明：当提取物浓度达到2mg/ml时，旋覆花石油醚提取物，蓖麻子甲醇提取物，石楠叶石油醚提取物的杀螨活性较高。

Solani. The extract was further separated into two parts and one part separated by ethyl acetate while the other was separated by petroleum ether. Based on the inhibition experiment against R. solani, ethly acetate extract has a rather strong effect on R. solani with 89.70% inhibition rate and 15.52 mgmL^(-1) EC 50.The effect of petroleum ether extract on R. solani is relatively weak. The former was again divided into five parts in silica gel column, of which the second part significantly inhibits R. solani. During the periods of 24 and 48 hrs, the inhibition rate of the second part on R. solan is respectively 89.58% and 80.36%.

结果表明：鸭粪乙醇提取物对水稻纹枯病菌有抑制作用，24h内最高菌丝生长抑制率和EC50分别为88.64%、26.11mgmL^(-1)；鸭粪乙醇提取物经萃取分离得到石油醚和乙酸乙酯两种组分，其中石油醚组分抑菌效果较弱，乙酸乙酯组分抑菌能力较强，其对水稻纹枯病菌抑制率为89.70%，EC50为15.52mgmL^(-1)；对乙酸乙酯组分进行硅胶柱层析分离得到5种流份，其中第2流份有显著抑菌活性，在24h和48h内对水稻纹枯病菌的抑制率分别为89.58%和80.36%。

The analysis methods for the determination of micro or trace elements in high moisture jellyfish were developed. The fatty acid compositions in difderent parts of fresh jellyfish were determined by GC/MS method. Thirty-five fatty acids were identified, and most of them were found in R. esculentum jellyfish for the first time. Especially, two unusual very long chain polyunsaturated fatty acids that were never detected in the other jellyfish also were determined. Amino acids were abundant in R. esculentum jellyfish, especially containing sulfur amino acids, and could be supplied for human diet. The polysaccharide in umbrella part of jellyfish was composed of glucose, galactose and uronic acid, and its molecular weight was 40,000, but the polysaccharide of the oral arms part consisted of glucose, mannose and glycuronic acid, and its molecular weight was 43,000. Above-mentioned data were never reported. The ethanolic extract of oral arms part of jellyfish were extracted by different polar solvents (petroleum ether, acetic ether, n-butanol), and antibacterial activity was tested to these extracts by four species of terricolous pathogenic bacilli and three species of botanic pathogenic fungi. The result demonstrated that the petroleum ether extract had certain bactericidal activity for two species of pathogenic bacilli, and n-butanol extract had certain inhibited activity on apple rot pathogenic fungus.

建立了 高含水量的海蜇产品中微量、痕量元素成分测定的分析方法；采用 GC/MS 方法测定了新鲜海蜇不同部位的脂肪酸组成，共鉴定出 35 种脂肪酸，其中大多数脂肪酸是首次在海蜇中被检测到，尤其是两种不常见的 C24：5 超长链多不饱和脂肪酸的分析和鉴定在其它水母种属中也从未见报道；海蜇三个部位中氨基酸成分齐全，含量丰富，含硫氨基酸含量较高，可与其它食物蛋白质的氨基酸互补；其中海蜇皮多糖是由葡萄糖、半乳糖和糖醛酸组成，分子量为 40，000，海蜇头多糖是由葡萄糖、甘露糖和糖醛酸组成，分子量为 43，000，以上工作均未见报道；利用石油醚、乙酸乙酯、正丁醇三种不同极性溶剂分别萃取海蜇头乙醇浸提物，用纸碟法和生长速率法分别对四株陆源病原菌和三株植物病原真菌进行了抑菌实验，结果表明海蜇头石油醚提取物和正丁醇提取物具有一定的抑菌活性。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。