石墨的

In reaction-injection moldinga mixture of two or more reactive fluids is forced under high pressure into the mold cavity.Chemical reactions take place in the mold rapidly and the polymer solidifies.Various fibers such as glass,graphite,or boron may also be used to reinforce the materials.Structural foams are also produced by a similar methodusing an inert gasand resin mixture.The product consists of a rigid cellular(closed-cell)structure with a continuous solid skin as muchas 0.080 in.(2mm)in thickness.There are several methods for forming structural foams with density reductions as much as 40% from the solid structure.Because stiffness is proportional to the third power of the thickness of a part,for the same weight of material used,cellular structures are stiffer than solid plastics or metals.

在反应注射成型所夹杂的两个或两个以上的接触过程中，被迫在高压下进入模具cavity.chemical反应发生在模具迅速和聚合物solidifies.various纤维如玻璃，石墨，或硼可能也可以用来加强materials.structural泡沫也产生类似的方法利用惰性气体和树脂mixture.the产品构成的一个硬性蜂窝的结构与连续性固皮肤作为留言Muchas 0.080英寸（ 2毫米），在thickness.there有几种方法，形成结构性的泡沫密度减少了四成之多，从固体structure.because刚度成正比第三力量厚度的一部分，为同样重量的使用材料，蜂窝结构更为严厉的比硬塑料或金属。

The dispersion of particles are also related to the interactionbetween nanosilver and polymer. Nanosilver dispersed well in PS, while form larger branchedclusters in PMMA, and polymers could prevent nanoparticles from aggregation. The interaction between nanosilver and polymers depends on the properties of polymers and treatment. XPS results indicated that no obvious interaction between nanosilver and PS was foundbefore and after heat treatment; for AS matrix, there exists a interaction between nanosilver and AN,moreover AN on the nanosilver surface could cyclize and lose N after heat treatment at 150℃ for1h; for PMMA matrix, there exists a interaction between nanosilver and O atoms, heat treatment at150℃ for 1h could lead to the reaction between Ag, S and O in the interlayer of composite andchange the interface interaction.

纳米银粒子的加入改变了聚合物体系对激光能量的吸收和转换方式，导致其激光离解方式的变化，通常此种粒子会促进聚合物的炭化，且在界面可能有诱导石墨化的作用；而银粒子自身的离解及其对基体激光离解的作用都受两相的界面相互作用的影响，即与聚合物基体的性质、后处理等有关，热处理后两相界面的变化对PS和AS体系的炭化影响不大，但PS体系中银团簇的最大原子聚集数减小；而对PMMA体系则基本上消除了激光炭化。

Both overlong or overshort bottom duration and overlong or overshort fluctuation period are unfavorable for reduction of non-diamond content. Only moderate ones have optimal effects on it.3 Compared with a smooth microwave, a fluctuating one can reduce the diamond nucleation density slightly.4 In fluctuating microwave, even if a higher CH〓 concentration chosen, diamond films with quality better than that of those deposited at a lower CH〓 concentration and in smooth microwave can be obtained.In smooth microwave, the influence of O〓 upon the diamond films＇MWPCVD was investigated. It is found that:1 In the range of lower O〓 concentration, its increase is beneficial to improvement of quality of diamond films, but in that of higher one, its increase conversely deteriorates the quality of diamond films.

在脉动微波下进行了沉积金刚石膜的研究，得到下述结果：1）采用合适的脉动微波，能使金刚石膜的沉积质量显著提高，并能使金刚石膜中的微晶石墨得到几乎完全的抑制。2）过长或过短的平底时间或脉动周期均不利于金刚石膜中非金刚石相碳含量的降低，只有适中的平底时间或脉动周期才有最佳的降低非金刚石相碳含量的效果。3）脉动微波会使金刚石的形核密度有所下降。4）脉动微波下，即使选用较高的CH〓浓度，也能得到沉积质量比在平稳微波下采用较低的CH〓浓度所制备的金刚石膜的沉积质量要明显提高的金刚石膜。

In fluctuating microwave, deposition of diamond films was investigated and some significant results were obtained:1 An appropriate fluctuating microwave can distinctly improve the quality of diamond films, and can grow diamond films almost without microcrystalline graphite.2 Both overlong or overshort bottom duration and overlong or overshort fluctuation period are unfavorable for reduction of non-diamond content. Only moderate ones have optimal effects on it.3 Compared with a smooth microwave, a fluctuating one can reduce the diamond nucleation density slightly.4 In fluctuating microwave, even if a higher CH〓 concentration chosen, diamond films with quality better than that of those deposited at a lower CH〓 concentration and in smooth microwave can be obtained.

在脉动微波下进行了沉积金刚石膜的研究，得到下述结果：1）采用合适的脉动微波，能使金刚石膜的沉积质量显著提高，并能使金刚石膜中的微晶石墨得到几乎完全的抑制。2）过长或过短的平底时间或脉动周期均不利于金刚石膜中非金刚石相碳含量的降低，只有适中的平底时间或脉动周期才有最佳的降低非金刚石相碳含量的效果。3）脉动微波会使金刚石的形核密度有所下降。4）脉动微波下，即使选用较高的CH〓浓度，也能得到沉积质量比在平稳微波下采用较低的CH〓浓度所制备的金刚石膜的沉积质量要明显提高的金刚石膜。

In this paper, two assemblies of special test equipments have been designed and fabricated by authors in our laboratory: namely Catalyst Molding Process Analyzer and Catalyst Mechanical Process Tester. These new skills are developed for the dynamic studies on whole mold forming process and crushing process of Fe-Cr WGHS catalyst pellet. Based on the orthogonal experimental design, the effects of some factors during the forming process of solid catalyst, such as predensification proportion, calcination time, calcination temperature and content of graphite on the mechanical strength of catalyst pellets are systematically examined, and the molding conditions have been optimized. Based on the experimental data, the relationship between catalyst density and forming pressure are educed, and the physical significances of some related parameters are described. The parameter of macro scopic elastic moduls has been suggested to character the mechanical properties of molding catalyst. The effects of molding pressure on mechanical properties of catalyst pellets are discussed, and results show that there exists a optimal molding pressure for the ideal mechanical properties: when over-high or over-low pressure is applied, the specific surface area and side crushing strength of catalyst pellets will decreased. The "rebound effect" will be undermined by the unsuitable pressure maintain process, resulting in the apparent decrease of mechanical strength of catalyst pellets.

本研究通过自行设计制造的催化剂模压成型过程分析仪（Catalyst Molding Process Analyzer， CMPA）和催化剂力学性质测试仪（Catalyst Mechanical Properties Tester， CMPT），以Fe-Cr系高温变换催化剂片剂为研究对象，对成型过程和受压破碎过程提供了全过程动态研究的新手段；本研究利用正交实验设计方法考察了固体催化剂成型过程中诸因素（包含预密致比例、煅烧时间、煅烧温度和石墨含量等）对催化剂成型体强度的影响，并对成型条件进行了优化；根据实验结果，关联确定了固体催化剂成型过程中的密度－压力关系式，并对方程中诸因子的物理意义进行了描述；提出了一种利用宏观弹性模量来表征成型催化剂的力学性质的方法；研究讨论了成型压力对催化剂成型体强度性质的影响，结果表明：对于催化剂成型体的强度和比表面性质，成型压力存在着一个最佳值，过高的成型压力会导致比表面积和侧压强度的降低；不适当的成型压力的维持时间会破坏&压力回弹&作用，造成催化剂成型体的机械强度明显降低。

A direct method to prepare nanometre catalyst of positive electrode for methyl alcohol fuel battery is to add strong oxidant to a mixed solution of manganese nitrate and some other metal nitrate, to coat them on the graphite electrode to have catalyst precursor produced, then to prepare the non-platinum nanometre catalyst of metal ion-doped manganese dioxide with carbon as a carrier by thermolytic reaction of the in-situ precursor. The prepared catalyst has the advantages of high electrical catalytic activity of methyl alcohol, high performance to protect against CO poison and low price, and it can lower the battery manufacturing cost effectively as well as can raise the entire electrical property of the battery so that the price performance and the market competitive edge of the battery are enchnaced effectively.

一种直接甲醇燃料电池阳极纳米催化剂的制备方法是在硝酸锰和其它金属硝酸盐的混合溶液中加入强氧化剂，涂抹于石墨电极上制成催化剂先驱体，通过先驱体在原位的热分解反应来制备以碳为载体的金属离子掺杂二氧化锰非铂纳米催化剂；制得的催化剂具有高的甲醇电催化活性、高的抗CO毒化性能以及低廉的价格等优点，可以有效地降低电池的制造成本，提高电池的整体电性能，从而有效地提高直接甲醇燃料电池的性能价格比及市场竞争能力。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。