相量

The mixture of corn and wheat bran were good food bases. Inoculation proportion and water content were key factors affecting conidial production.

结果表明：蛭石和稻壳均可作为固相培养的优良载体，以蛭石为载体的产孢量稍高于稻壳。

In order to investigate the succession of soil microbial community with ecosystem development, soil samples of three successional stages (i.e., barren stage, cryptogamic crust stage and herbaceous vascular plant community stage) from two tailings wastelands (Yangshanchong tailings wasteland discarded in 2001 and New Tongguanshan tailings wasteland discarded in 1991) were collected and soil microbial biomass was determined by methods of typical plate culture' and molecular biology.

该研究以2处（即，铜陵杨山冲尾矿废弃地和铜官山新尾矿废弃地）不同时期弃置的、处于3个演替阶段（原生裸地阶段、隐花植物结皮阶段和草本维管植物群落阶段）的铜尾矿废弃地为研究对象，利用传统培养法和分子生物学法相结合的手段对土壤微生物量和土壤微生物群落结构变化及其影响因素进行了调查。

Their thermotropic phase behavior was investigated by differential scanning calorimetry and POM. It was found that T(subscript S-N) w and T(subscript N-I), of PMMAZO was slightly increased with the increased of the mass ratio of liquid crystal block segments. PEO and PMMA block affected the liquid cystal behavior of PMMAZO. Meanwhile, PMMA and PMMAZO obviously influenced the crystals property of PEO segments3 which was decreased as the increase of molecular weight of PMMA and PMMAZO segments.

以差示扫描量热仪和偏光显徽镜研究了ABC三嵌段共聚物PEO-b-PMMA-b-PMMAZO的热力学相转变行为，发现随着PMMAZO链段的质量百分比的增加，三嵌段共聚物中PMMAZO链段的T和T逐渐提高；同时，PMMA和PMMAZO链段的长短影响PEO链段的结晶性，随着液晶段PMMAZO和PMMA链段分子量的增加，PEO链段的结晶性减弱。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

DSC and dilatometry were carried out to determine the phase transformation temperature of a high speed steel used for centrifugal cast rolls.

采用差式扫描量热法及热膨胀法测定了离心铸造轧辊用高速钢的相变点，根据高速钢的临界转变温度，进行了退火、淬火和回火实验。

The crystal structure, phase transition, cross-section morphology and thermal expansion coefficient of the samples were investigated by X-ray diffraction, thermogravimetric and differential scanning calorimetry, scanning electron microscope and dilatometry respectively.

通过X射线衍射仪、热重-差示扫描量热、扫描电子显微镜、热膨胀仪等分析手段对样品的晶体结构、物相转变、断面微观形貌和热膨胀性能进行表征。

Using diphase emulsion to make bovine albumin microcapsuals with hydroxy proprl methyl celluloxe phthalate and CMC-Na,Gelatine,chitosan as dispersed phase;Designing test with single factors method and studying effection of the wrap material,reagent of emulsification,hydrophilic colloid of protection...

分别用羧甲基纤维素钠、明胶、壳聚糖作分散质，复相乳液法制备HPMCP的BSA微胶囊；采用单因子设计试验，研究了壁材、乳化剂、分散质浓度对微胶囊包裹量的影响。

Using diphase emulsion to make bovine albumin microcapsuals with hydroxy proprl methyl celluloxe phthalate and CMC-Na, Gelatine, chitosan as dispersed phase; Designing test with single factors method and studying effection of the wrap material, reagent of emulsification, hydrophilic colloid of protection on the methods for testing the protein envelopment quantum of HPMCP Microcapsuals.

分别用羧甲基纤维素钠、明胶、壳聚糖作分散质，复相乳液法制备HPMCP的BSA微胶囊；采用单因子设计试验，研究了壁材、乳化剂、分散质浓度对微胶囊包裹量的影响。

The movement and volatilization ofthe small molecular which produced by the discomposing of the SBS as well as thecontinuous degradation of SBS is also retarded. The thermo-stability and anti-thermooxidative aging properties of the composites are enhanced.

磨盘剪切力场增加了PP与有机蒙脱土的界面结合，由塑料包覆粘土片层的复合分散相具有模量梯度和结构梯度，能较好地传递应力并阻碍裂纹的扩展，提高了材料的强度。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新